Extraction of green coffee oil using supercritical carbon dioxide

Detalhes bibliográficos
Autor(a) principal: Azevedo, Álvaro Bandeira Antunes de
Data de Publicação: 2008
Outros Autores: Kieckbusch, Theo Guenter, Tashima, Alexandre Keiji, Mohamed, R. S., Mazzafera, P., Melo, Silvio Alexandre Beisl Vieira de
Tipo de documento: Artigo
Idioma: eng
Título da fonte: Repositório Institucional da UFBA
Texto Completo: http://www.repositorio.ufba.br/ri/handle/ri/6356
Resumo: Acesso restrito: Texto completo.p. 186-192.
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spelling Azevedo, Álvaro Bandeira Antunes deKieckbusch, Theo GuenterTashima, Alexandre KeijiMohamed, R. S.Mazzafera, P.Melo, Silvio Alexandre Beisl Vieira deAzevedo, Álvaro Bandeira Antunes deKieckbusch, Theo GuenterTashima, Alexandre KeijiMohamed, R. S.Mazzafera, P.Melo, Silvio Alexandre Beisl Vieira de2012-07-06T13:08:14Z20080896-8446http://www.repositorio.ufba.br/ri/handle/ri/6356v. 44, n. 2Acesso restrito: Texto completo.p. 186-192.Supercritical CO2 extraction was used to refine coffee oil obtained by mechanical pressing. Extractions were carried out using 50–70 ◦C and pressures ranging from 15.2 to 35.2MPa, with a CO2 flow rate of 1 standard L/min using a semi-continuous high-pressure extraction apparatus. Green coffee oil fractions were collected at fixed time intervals and the composition of each fraction was determined by HPLC analyses. Caffeine and traces of chlorogenic acid were detected in the first fractions while waxes remained in the extraction vessel. Compared with the original oil the triglyceride composition remained almost unchanged in the fractions. The results also indicate an increase of triglyceride and caffeine extraction with pressure. An increase in extraction temperature results in a retrograde behavior over the pressure range of 15.2–28.3MPa. At pressures higher than 30MPa the solubility behavior of coffee oil was apparently independent of the temperature. A good correlation of the solubility data of green coffee oil was obtained using the Chrastil equation.Submitted by JURANDI DE SOUZA SILVA (jssufba@hotmail.com) on 2012-07-06T13:08:14Z No. of bitstreams: 1 CONFIG~1...-S0896844607004366-main-1.pdf: 406145 bytes, checksum: b939f07398c5bf5c5dae92bd5bead1c1 (MD5)Made available in DSpace on 2012-07-06T13:08:14Z (GMT). No. of bitstreams: 1 CONFIG~1...-S0896844607004366-main-1.pdf: 406145 bytes, checksum: b939f07398c5bf5c5dae92bd5bead1c1 (MD5) Previous issue date: 2008http://dx.doi.org/10.1016/j.supflu.2007.11.004reponame:Repositório Institucional da UFBAinstname:Universidade Federal da Bahia (UFBA)instacron:UFBACaffeineChlorogenic acidCoffeeCoffee oilTriglycerideExtraction of green coffee oil using supercritical carbon dioxideJournal of Supercritical Fluidsinfo:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/article10000-01-01enginfo:eu-repo/semantics/openAccessORIGINALCONFIG~1...-S0896844607004366-main-1.pdfCONFIG~1...-S0896844607004366-main-1.pdfapplication/pdf406145https://repositorio.ufba.br/bitstream/ri/6356/1/CONFIG~1...-S0896844607004366-main-1.pdfb939f07398c5bf5c5dae92bd5bead1c1MD51LICENSElicense.txtlicense.txttext/plain1762https://repositorio.ufba.br/bitstream/ri/6356/2/license.txt1b89a9a0548218172d7c829f87a0eab9MD52TEXTCONFIG~1...-S0896844607004366-main-1.pdf.txtCONFIG~1...-S0896844607004366-main-1.pdf.txtExtracted texttext/plain26131https://repositorio.ufba.br/bitstream/ri/6356/3/CONFIG~1...-S0896844607004366-main-1.pdf.txte67d93c498880de409d1a585bc9c5a59MD53ri/63562022-08-08 13:17:34.657oai:repositorio.ufba.br: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Repositório InstitucionalPUBhttp://192.188.11.11:8080/oai/requestopendoar:19322022-08-08T16:17:34Repositório Institucional da UFBA - Universidade Federal da Bahia (UFBA)false
dc.title.pt_BR.fl_str_mv Extraction of green coffee oil using supercritical carbon dioxide
dc.title.alternative.pt_BR.fl_str_mv Journal of Supercritical Fluids
title Extraction of green coffee oil using supercritical carbon dioxide
spellingShingle Extraction of green coffee oil using supercritical carbon dioxide
Azevedo, Álvaro Bandeira Antunes de
Caffeine
Chlorogenic acid
Coffee
Coffee oil
Triglyceride
title_short Extraction of green coffee oil using supercritical carbon dioxide
title_full Extraction of green coffee oil using supercritical carbon dioxide
title_fullStr Extraction of green coffee oil using supercritical carbon dioxide
title_full_unstemmed Extraction of green coffee oil using supercritical carbon dioxide
title_sort Extraction of green coffee oil using supercritical carbon dioxide
author Azevedo, Álvaro Bandeira Antunes de
author_facet Azevedo, Álvaro Bandeira Antunes de
Kieckbusch, Theo Guenter
Tashima, Alexandre Keiji
Mohamed, R. S.
Mazzafera, P.
Melo, Silvio Alexandre Beisl Vieira de
author_role author
author2 Kieckbusch, Theo Guenter
Tashima, Alexandre Keiji
Mohamed, R. S.
Mazzafera, P.
Melo, Silvio Alexandre Beisl Vieira de
author2_role author
author
author
author
author
dc.contributor.author.fl_str_mv Azevedo, Álvaro Bandeira Antunes de
Kieckbusch, Theo Guenter
Tashima, Alexandre Keiji
Mohamed, R. S.
Mazzafera, P.
Melo, Silvio Alexandre Beisl Vieira de
Azevedo, Álvaro Bandeira Antunes de
Kieckbusch, Theo Guenter
Tashima, Alexandre Keiji
Mohamed, R. S.
Mazzafera, P.
Melo, Silvio Alexandre Beisl Vieira de
dc.subject.por.fl_str_mv Caffeine
Chlorogenic acid
Coffee
Coffee oil
Triglyceride
topic Caffeine
Chlorogenic acid
Coffee
Coffee oil
Triglyceride
description Acesso restrito: Texto completo.p. 186-192.
publishDate 2008
dc.date.issued.fl_str_mv 2008
dc.date.accessioned.fl_str_mv 2012-07-06T13:08:14Z
dc.type.status.fl_str_mv info:eu-repo/semantics/publishedVersion
dc.type.driver.fl_str_mv info:eu-repo/semantics/article
format article
status_str publishedVersion
dc.identifier.uri.fl_str_mv http://www.repositorio.ufba.br/ri/handle/ri/6356
dc.identifier.issn.none.fl_str_mv 0896-8446
dc.identifier.number.pt_BR.fl_str_mv v. 44, n. 2
identifier_str_mv 0896-8446
v. 44, n. 2
url http://www.repositorio.ufba.br/ri/handle/ri/6356
dc.language.iso.fl_str_mv eng
language eng
dc.rights.driver.fl_str_mv info:eu-repo/semantics/openAccess
eu_rights_str_mv openAccess
dc.source.pt_BR.fl_str_mv http://dx.doi.org/10.1016/j.supflu.2007.11.004
dc.source.none.fl_str_mv reponame:Repositório Institucional da UFBA
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reponame_str Repositório Institucional da UFBA
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