Application of full factorial design and Doehlert matrix for the optimisation of beef tallow methanolysis via homogeneous catalysis

Detalhes bibliográficos
Autor(a) principal: Mendonça, Daniel Ribeiro de
Data de Publicação: 2011
Outros Autores: Andrade, Heloysa Martins Carvalho, Guimarães, Paulo Roberto Britto, Vianna, Regina Ferreira, Meneghetti, Simoni Margareti Plentz, Pontes, Luiz Antônio Magalhães, Teixeira, Leonardo Sena Gomes
Tipo de documento: Artigo
Idioma: eng
Título da fonte: Repositório Institucional da UFBA
Texto Completo: http://www.repositorio.ufba.br/ri/handle/ri/5472
Resumo: texto completo: acesso restrito. p.342–348.
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spelling Mendonça, Daniel Ribeiro deAndrade, Heloysa Martins CarvalhoGuimarães, Paulo Roberto BrittoVianna, Regina FerreiraMeneghetti, Simoni Margareti PlentzPontes, Luiz Antônio MagalhãesTeixeira, Leonardo Sena GomesMendonça, Daniel Ribeiro deAndrade, Heloysa Martins CarvalhoGuimarães, Paulo Roberto BrittoVianna, Regina FerreiraMeneghetti, Simoni Margareti PlentzPontes, Luiz Antônio MagalhãesTeixeira, Leonardo Sena Gomes2012-02-29T18:12:35Z20110378-3820http://www.repositorio.ufba.br/ri/handle/ri/5472v. 92.texto completo: acesso restrito. p.342–348.The transesterification of triglycerides by means of alkaline catalysts is the most widely used route for biodiesel production and reaction optimisation by multivariate methods has been used for biodiesel production from different vegetable oils.However, the application of simultaneous optimisation for biodiesel production frombeef tallow has received little attention. In an effort to optimize the beef tallowbiodiesel production, a combination of the full factorial design and the Doehlert matrix was applied, and the effects of temperature, reaction time, catalyst concentration and alcohol:tallow molar ratio and their reciprocal interactions were assessed. The response variables under study were purity and yield of the final biodiesel product. In the selected condition [alcohol:tallow molar ratio(M)=7.5:1, catalyst:tallow mass ratio(C)=1.5%, reaction time(t)=20 min and temperature=50 °C], the conversion yield of tallow biodiesel was 88.4% and the purity was 99.4%. The final biodiesel obtained was analysed and showed to have good quality characteristics.Submitted by Ana Valéria de Jesus Moura (anavaleria_131@hotmail.com) on 2012-02-29T18:12:35Z No. of bitstreams: 1 Application of full factorial design and Doehlert matrix for the optimisation of beef tallow methanolysis via homogeneous catalysis.pdf: 1766386 bytes, checksum: a4a96710cd91895fd2244c4ea66a0c0c (MD5)Made available in DSpace on 2012-02-29T18:12:35Z (GMT). No. of bitstreams: 1 Application of full factorial design and Doehlert matrix for the optimisation of beef tallow methanolysis via homogeneous catalysis.pdf: 1766386 bytes, checksum: a4a96710cd91895fd2244c4ea66a0c0c (MD5) Previous issue date: 2011doi:10.1016/j.fuproc.2010.09.026reponame:Repositório Institucional da UFBAinstname:Universidade Federal da Bahia (UFBA)instacron:UFBABiodieselBeef tallowTransesterificationFull factorial designDoehlert matrixApplication of full factorial design and Doehlert matrix for the optimisation of beef tallow methanolysis via homogeneous catalysisFuel Processing Technologyinfo:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/article10000-01-01enginfo:eu-repo/semantics/openAccessORIGINALApplication of full factorial design and Doehlert matrix for the optimisation of beef tallow methanolysis via homogeneous catalysis.pdfApplication of full factorial design and Doehlert matrix for the optimisation of beef tallow methanolysis via homogeneous catalysis.pdfapplication/pdf1766386https://repositorio.ufba.br/bitstream/ri/5472/1/Application%20of%20full%20factorial%20design%20and%20Doehlert%20matrix%20for%20the%20optimisation%20of%20beef%20tallow%20methanolysis%20via%20homogeneous%20catalysis.pdfa4a96710cd91895fd2244c4ea66a0c0cMD51LICENSElicense.txtlicense.txttext/plain1762https://repositorio.ufba.br/bitstream/ri/5472/2/license.txt1b89a9a0548218172d7c829f87a0eab9MD52TEXTApplication of full factorial design and Doehlert matrix for the optimisation of beef tallow methanolysis via homogeneous catalysis.pdf.txtApplication of full factorial design and Doehlert matrix for the optimisation of beef tallow methanolysis via homogeneous catalysis.pdf.txtExtracted texttext/plain36146https://repositorio.ufba.br/bitstream/ri/5472/3/Application%20of%20full%20factorial%20design%20and%20Doehlert%20matrix%20for%20the%20optimisation%20of%20beef%20tallow%20methanolysis%20via%20homogeneous%20catalysis.pdf.txt0f60ccc8a86558ccfad33ced2a6ed2d4MD53ri/54722022-07-05 14:03:18.984oai:repositorio.ufba.br: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Repositório InstitucionalPUBhttp://192.188.11.11:8080/oai/requestopendoar:19322022-07-05T17:03:18Repositório Institucional da UFBA - Universidade Federal da Bahia (UFBA)false
dc.title.pt_BR.fl_str_mv Application of full factorial design and Doehlert matrix for the optimisation of beef tallow methanolysis via homogeneous catalysis
dc.title.alternative.pt_BR.fl_str_mv Fuel Processing Technology
title Application of full factorial design and Doehlert matrix for the optimisation of beef tallow methanolysis via homogeneous catalysis
spellingShingle Application of full factorial design and Doehlert matrix for the optimisation of beef tallow methanolysis via homogeneous catalysis
Mendonça, Daniel Ribeiro de
Biodiesel
Beef tallow
Transesterification
Full factorial design
Doehlert matrix
title_short Application of full factorial design and Doehlert matrix for the optimisation of beef tallow methanolysis via homogeneous catalysis
title_full Application of full factorial design and Doehlert matrix for the optimisation of beef tallow methanolysis via homogeneous catalysis
title_fullStr Application of full factorial design and Doehlert matrix for the optimisation of beef tallow methanolysis via homogeneous catalysis
title_full_unstemmed Application of full factorial design and Doehlert matrix for the optimisation of beef tallow methanolysis via homogeneous catalysis
title_sort Application of full factorial design and Doehlert matrix for the optimisation of beef tallow methanolysis via homogeneous catalysis
author Mendonça, Daniel Ribeiro de
author_facet Mendonça, Daniel Ribeiro de
Andrade, Heloysa Martins Carvalho
Guimarães, Paulo Roberto Britto
Vianna, Regina Ferreira
Meneghetti, Simoni Margareti Plentz
Pontes, Luiz Antônio Magalhães
Teixeira, Leonardo Sena Gomes
author_role author
author2 Andrade, Heloysa Martins Carvalho
Guimarães, Paulo Roberto Britto
Vianna, Regina Ferreira
Meneghetti, Simoni Margareti Plentz
Pontes, Luiz Antônio Magalhães
Teixeira, Leonardo Sena Gomes
author2_role author
author
author
author
author
author
dc.contributor.author.fl_str_mv Mendonça, Daniel Ribeiro de
Andrade, Heloysa Martins Carvalho
Guimarães, Paulo Roberto Britto
Vianna, Regina Ferreira
Meneghetti, Simoni Margareti Plentz
Pontes, Luiz Antônio Magalhães
Teixeira, Leonardo Sena Gomes
Mendonça, Daniel Ribeiro de
Andrade, Heloysa Martins Carvalho
Guimarães, Paulo Roberto Britto
Vianna, Regina Ferreira
Meneghetti, Simoni Margareti Plentz
Pontes, Luiz Antônio Magalhães
Teixeira, Leonardo Sena Gomes
dc.subject.por.fl_str_mv Biodiesel
Beef tallow
Transesterification
Full factorial design
Doehlert matrix
topic Biodiesel
Beef tallow
Transesterification
Full factorial design
Doehlert matrix
description texto completo: acesso restrito. p.342–348.
publishDate 2011
dc.date.issued.fl_str_mv 2011
dc.date.accessioned.fl_str_mv 2012-02-29T18:12:35Z
dc.type.status.fl_str_mv info:eu-repo/semantics/publishedVersion
dc.type.driver.fl_str_mv info:eu-repo/semantics/article
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dc.identifier.uri.fl_str_mv http://www.repositorio.ufba.br/ri/handle/ri/5472
dc.identifier.issn.none.fl_str_mv 0378-3820
dc.identifier.number.pt_BR.fl_str_mv v. 92.
identifier_str_mv 0378-3820
v. 92.
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dc.source.pt_BR.fl_str_mv doi:10.1016/j.fuproc.2010.09.026
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