Extract mesquite as alternative source for production bacterial cellulose
Autor(a) principal: | |
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Data de Publicação: | 2014 |
Tipo de documento: | Dissertação |
Idioma: | por |
Título da fonte: | Biblioteca Digital de Teses e Dissertações da UFC |
Texto Completo: | http://www.teses.ufc.br/tde_busca/arquivo.php?codArquivo=12079 |
Resumo: | Bacterial cellulose (BC) is a naturally nanoscale biomaterial with high purity and excellent chemical and mechanical properties. There are several sugar-rich renewable sources and wastes that can be used as alternative media for bacterial cellulose production.The aim of this study was to evaluate the suitability of an extract of mesquite pods as an alternative carbohydrate source for the production of BC through fermentation by Gluconacetobacter hansenii. The amount of sugars, soluble solids, and pH of the extract was characterized. The influence of the initial sugar concentration, pH, and the source of supplementary nitrogen on the fermentation were evaluated. The best production of bacterial cellulose was achieved in the medium with a sugar concentration of 30 g /L, pH 4.0, and supplemented with 10 g /L of yeast extract. The films from the optimized medium were oven dried and characterized by x-ray diffraction (XRD), Fourier Transform Infrared spectroscopy (FTIR), thermal gravimetric analysis (TGA), differential scanning calorimetry (DSC) and electron microscopy (SEM). The results were similar to typical bacterial cellulose films produced in the reference medium HS. Thus, it was possible to demonstrate the suitability of mesquite pod aqueous extract to produce BC. |
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info:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/masterThesisExtract mesquite as alternative source for production bacterial cellulose Extrato de algaroba como fonte alternativa para produÃÃo de celulose bacteriana2014-02-25Morsyleide de Freitas Rosa82089205768http://lattes.cnpq.br/7670383899259509Maria Valderez Ponte Rocha64669335391http://lattes.cnpq.br/0639546287060338Men de Sà Moreira de Souza Filho16931700359http://lattes.cnpq.br/476890137557919997587168320ElÃgenes Sampaio do NascimentoUniversidade Federal do CearÃPrograma de PÃs-GraduaÃÃo em Engenharia QuÃmicaUFCBRbacterial cellulose, mesquite, fermentationENGENHARIA QUIMICABacterial cellulose (BC) is a naturally nanoscale biomaterial with high purity and excellent chemical and mechanical properties. There are several sugar-rich renewable sources and wastes that can be used as alternative media for bacterial cellulose production.The aim of this study was to evaluate the suitability of an extract of mesquite pods as an alternative carbohydrate source for the production of BC through fermentation by Gluconacetobacter hansenii. The amount of sugars, soluble solids, and pH of the extract was characterized. The influence of the initial sugar concentration, pH, and the source of supplementary nitrogen on the fermentation were evaluated. The best production of bacterial cellulose was achieved in the medium with a sugar concentration of 30 g /L, pH 4.0, and supplemented with 10 g /L of yeast extract. The films from the optimized medium were oven dried and characterized by x-ray diffraction (XRD), Fourier Transform Infrared spectroscopy (FTIR), thermal gravimetric analysis (TGA), differential scanning calorimetry (DSC) and electron microscopy (SEM). The results were similar to typical bacterial cellulose films produced in the reference medium HS. Thus, it was possible to demonstrate the suitability of mesquite pod aqueous extract to produce BC.A celulose bacteriana (CB) à um biomaterial naturalmente nanomÃtrico, com elevado grau de pureza e excelentes propriedades quÃmicas e mecÃnicas. Existem na natureza fontes renovÃveis e resÃduos ricos em aÃÃcares que despertam um crescente interesse como meios alternativos em substituiÃÃo aos tradicionalmente empregados na produÃÃo de celulose. O objetivo deste estudo foi avaliar o extrato de vagens de algaroba (Prosopis juliflora) como fonte alternativa para produÃÃo de CB atravÃs de fermentaÃÃo por Gluconacetobacter hansenii. O extrato foi caracterizado quanto à quantidade de aÃÃcares, pH e sÃlidos solÃveis. AtravÃs da fermentaÃÃo do extrato foram realizados testes de influÃncia da concentraÃÃo inicial de aÃÃcares, influÃncia do pH e efeito da variaÃÃo da suplementaÃÃo com fonte de nitrogÃnio sobre a produÃÃo de CB. A melhor produÃÃo foi proveniente da fermentaÃÃo do extrato de algaroba diluÃdo a uma concentraÃÃo de aÃÃcares de 30 g/L com pH 4,0 suplementado com 10 g/L de extrato de levedura. As pelÃculas obtidas do extrato com condiÃÃes melhoradas foram secas em estufa e caracterizadas por difraÃÃo de raios x (DRX), espectroscopia de absorÃÃo no infravermelho (FTIR), anÃlise termogravimÃtrica (TGA), calorimetria exploratÃria diferencial (DSC) e microscopia eletrÃnica de varredura (MEV), e apresentaram resultados tÃpicos de celulose bacteriana quando comparados à CB produzida no meio de referÃncia HS. Assim, foi possÃvel mostrar a viabilidade de produÃÃo de CB com extrato aquoso de vagens de algaroba.Conselho Nacional de Desenvolvimento CientÃfico e TecnolÃgicohttp://www.teses.ufc.br/tde_busca/arquivo.php?codArquivo=12079application/pdfinfo:eu-repo/semantics/openAccessporreponame:Biblioteca Digital de Teses e Dissertações da UFCinstname:Universidade Federal do Cearáinstacron:UFC2019-01-21T11:25:17Zmail@mail.com - |
dc.title.en.fl_str_mv |
Extract mesquite as alternative source for production bacterial cellulose |
dc.title.alternative.pt.fl_str_mv |
Extrato de algaroba como fonte alternativa para produÃÃo de celulose bacteriana |
title |
Extract mesquite as alternative source for production bacterial cellulose |
spellingShingle |
Extract mesquite as alternative source for production bacterial cellulose ElÃgenes Sampaio do Nascimento bacterial cellulose, mesquite, fermentation ENGENHARIA QUIMICA |
title_short |
Extract mesquite as alternative source for production bacterial cellulose |
title_full |
Extract mesquite as alternative source for production bacterial cellulose |
title_fullStr |
Extract mesquite as alternative source for production bacterial cellulose |
title_full_unstemmed |
Extract mesquite as alternative source for production bacterial cellulose |
title_sort |
Extract mesquite as alternative source for production bacterial cellulose |
author |
ElÃgenes Sampaio do Nascimento |
author_facet |
ElÃgenes Sampaio do Nascimento |
author_role |
author |
dc.contributor.advisor1.fl_str_mv |
Morsyleide de Freitas Rosa |
dc.contributor.advisor1ID.fl_str_mv |
82089205768 |
dc.contributor.advisor1Lattes.fl_str_mv |
http://lattes.cnpq.br/7670383899259509 |
dc.contributor.referee1.fl_str_mv |
Maria Valderez Ponte Rocha |
dc.contributor.referee1ID.fl_str_mv |
64669335391 |
dc.contributor.referee1Lattes.fl_str_mv |
http://lattes.cnpq.br/0639546287060338 |
dc.contributor.referee2.fl_str_mv |
Men de SÃ Moreira de Souza Filho |
dc.contributor.referee2ID.fl_str_mv |
16931700359 |
dc.contributor.referee2Lattes.fl_str_mv |
http://lattes.cnpq.br/4768901375579199 |
dc.contributor.authorID.fl_str_mv |
97587168320 |
dc.contributor.author.fl_str_mv |
ElÃgenes Sampaio do Nascimento |
contributor_str_mv |
Morsyleide de Freitas Rosa Maria Valderez Ponte Rocha Men de SÃ Moreira de Souza Filho |
dc.subject.eng.fl_str_mv |
bacterial cellulose, mesquite, fermentation |
topic |
bacterial cellulose, mesquite, fermentation ENGENHARIA QUIMICA |
dc.subject.cnpq.fl_str_mv |
ENGENHARIA QUIMICA |
dc.description.sponsorship.fl_txt_mv |
Conselho Nacional de Desenvolvimento CientÃfico e TecnolÃgico |
dc.description.abstract.por.fl_txt_mv |
Bacterial cellulose (BC) is a naturally nanoscale biomaterial with high purity and excellent chemical and mechanical properties. There are several sugar-rich renewable sources and wastes that can be used as alternative media for bacterial cellulose production.The aim of this study was to evaluate the suitability of an extract of mesquite pods as an alternative carbohydrate source for the production of BC through fermentation by Gluconacetobacter hansenii. The amount of sugars, soluble solids, and pH of the extract was characterized. The influence of the initial sugar concentration, pH, and the source of supplementary nitrogen on the fermentation were evaluated. The best production of bacterial cellulose was achieved in the medium with a sugar concentration of 30 g /L, pH 4.0, and supplemented with 10 g /L of yeast extract. The films from the optimized medium were oven dried and characterized by x-ray diffraction (XRD), Fourier Transform Infrared spectroscopy (FTIR), thermal gravimetric analysis (TGA), differential scanning calorimetry (DSC) and electron microscopy (SEM). The results were similar to typical bacterial cellulose films produced in the reference medium HS. Thus, it was possible to demonstrate the suitability of mesquite pod aqueous extract to produce BC. A celulose bacteriana (CB) à um biomaterial naturalmente nanomÃtrico, com elevado grau de pureza e excelentes propriedades quÃmicas e mecÃnicas. Existem na natureza fontes renovÃveis e resÃduos ricos em aÃÃcares que despertam um crescente interesse como meios alternativos em substituiÃÃo aos tradicionalmente empregados na produÃÃo de celulose. O objetivo deste estudo foi avaliar o extrato de vagens de algaroba (Prosopis juliflora) como fonte alternativa para produÃÃo de CB atravÃs de fermentaÃÃo por Gluconacetobacter hansenii. O extrato foi caracterizado quanto à quantidade de aÃÃcares, pH e sÃlidos solÃveis. AtravÃs da fermentaÃÃo do extrato foram realizados testes de influÃncia da concentraÃÃo inicial de aÃÃcares, influÃncia do pH e efeito da variaÃÃo da suplementaÃÃo com fonte de nitrogÃnio sobre a produÃÃo de CB. A melhor produÃÃo foi proveniente da fermentaÃÃo do extrato de algaroba diluÃdo a uma concentraÃÃo de aÃÃcares de 30 g/L com pH 4,0 suplementado com 10 g/L de extrato de levedura. As pelÃculas obtidas do extrato com condiÃÃes melhoradas foram secas em estufa e caracterizadas por difraÃÃo de raios x (DRX), espectroscopia de absorÃÃo no infravermelho (FTIR), anÃlise termogravimÃtrica (TGA), calorimetria exploratÃria diferencial (DSC) e microscopia eletrÃnica de varredura (MEV), e apresentaram resultados tÃpicos de celulose bacteriana quando comparados à CB produzida no meio de referÃncia HS. Assim, foi possÃvel mostrar a viabilidade de produÃÃo de CB com extrato aquoso de vagens de algaroba. |
description |
Bacterial cellulose (BC) is a naturally nanoscale biomaterial with high purity and excellent chemical and mechanical properties. There are several sugar-rich renewable sources and wastes that can be used as alternative media for bacterial cellulose production.The aim of this study was to evaluate the suitability of an extract of mesquite pods as an alternative carbohydrate source for the production of BC through fermentation by Gluconacetobacter hansenii. The amount of sugars, soluble solids, and pH of the extract was characterized. The influence of the initial sugar concentration, pH, and the source of supplementary nitrogen on the fermentation were evaluated. The best production of bacterial cellulose was achieved in the medium with a sugar concentration of 30 g /L, pH 4.0, and supplemented with 10 g /L of yeast extract. The films from the optimized medium were oven dried and characterized by x-ray diffraction (XRD), Fourier Transform Infrared spectroscopy (FTIR), thermal gravimetric analysis (TGA), differential scanning calorimetry (DSC) and electron microscopy (SEM). The results were similar to typical bacterial cellulose films produced in the reference medium HS. Thus, it was possible to demonstrate the suitability of mesquite pod aqueous extract to produce BC. |
publishDate |
2014 |
dc.date.issued.fl_str_mv |
2014-02-25 |
dc.type.status.fl_str_mv |
info:eu-repo/semantics/publishedVersion |
dc.type.driver.fl_str_mv |
info:eu-repo/semantics/masterThesis |
status_str |
publishedVersion |
format |
masterThesis |
dc.identifier.uri.fl_str_mv |
http://www.teses.ufc.br/tde_busca/arquivo.php?codArquivo=12079 |
url |
http://www.teses.ufc.br/tde_busca/arquivo.php?codArquivo=12079 |
dc.language.iso.fl_str_mv |
por |
language |
por |
dc.rights.driver.fl_str_mv |
info:eu-repo/semantics/openAccess |
eu_rights_str_mv |
openAccess |
dc.format.none.fl_str_mv |
application/pdf |
dc.publisher.none.fl_str_mv |
Universidade Federal do Cearà |
dc.publisher.program.fl_str_mv |
Programa de PÃs-GraduaÃÃo em Engenharia QuÃmica |
dc.publisher.initials.fl_str_mv |
UFC |
dc.publisher.country.fl_str_mv |
BR |
publisher.none.fl_str_mv |
Universidade Federal do Cearà |
dc.source.none.fl_str_mv |
reponame:Biblioteca Digital de Teses e Dissertações da UFC instname:Universidade Federal do Ceará instacron:UFC |
reponame_str |
Biblioteca Digital de Teses e Dissertações da UFC |
collection |
Biblioteca Digital de Teses e Dissertações da UFC |
instname_str |
Universidade Federal do Ceará |
instacron_str |
UFC |
institution |
UFC |
repository.name.fl_str_mv |
-
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repository.mail.fl_str_mv |
mail@mail.com |
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1643295189996929024 |