Estudo do compósito aço/ceramico AISI-316L/Sr1,8Y0,2CrReO6 produzido através da metalurgia do pó

Detalhes bibliográficos
Autor(a) principal: Salvador, Jose Firmino
Data de Publicação: 2019
Tipo de documento: Tese
Idioma: por
Título da fonte: Repositório Institucional da Universidade Federal do Espírito Santo (riUfes)
Texto Completo: http://repositorio.ufes.br/handle/10/13637
Resumo: This work studies the sintering of a steel/ceramic composite with stainless steel AISI 316L and Sr1.8Y0.2CrReO6 double perovskite (316L/SYCRO) by powder metallurgy. The goal was to produce a material that could be used in additive manufacture with structurally impact, corrosion and magnetic properties. AISI 316L stainless steel is a corrosion resistant material, but not magnetic. Sr1.8Y0.2CrReO6 (SYCRO) ceramic shows magnetic propriety until ~360 ºC (~640 K). 90% of 316L powder was mixed with 10% of SYCRO powder. The mixture was homogenized in a ball milling at low temperature (~77 K). The obtained powder was compacted in cylindrical forms, sealed in a evacuated quartzo tube and submitted to termal treatment for sintering. As a comparative standard, samples of 316L powder were sintered as the similar way of 316L/SYCRO samples. The sintered samples were evaluated by Scanning Electron Microscopy (SEM), X-ray Powder Diffraction (XRD), X-ray Computed Microtomography, Magnetic Susceptibility and Mechanical Compression test. The 316L/SYCRO composite showed a similar magnetism of SYCRO ceramic and a diferente mechanical behavior of sintered 316L sample. Taken into account this work it was demonstrated that it is possible to produce steel/ceramic composites with controllable contents.
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spelling Orlando, Marcos Tadeu D Azeredohttps://orcid.org/0000000283876504http://lattes.cnpq.br/3562894103432242Salvador, Jose Firminohttps://orcid.org/http://lattes.cnpq.br/0061402424211214Franco Junior, Adonias Ribeiro https://orcid.org/http://lattes.cnpq.br/6677652514776940Passamai Junior, Jose Luis https://orcid.org/0000-0001-6866-1460http://lattes.cnpq.br/5445869592199028Passos, Carlos Augusto Cardosohttps://orcid.org/2528679879816545http://lattes.cnpq.br/2528679879816545Vieira, Estefano AparecidoCavichini, Arthur Sant Ana2024-05-29T22:11:53Z2024-05-29T22:11:53Z2019-06-05This work studies the sintering of a steel/ceramic composite with stainless steel AISI 316L and Sr1.8Y0.2CrReO6 double perovskite (316L/SYCRO) by powder metallurgy. The goal was to produce a material that could be used in additive manufacture with structurally impact, corrosion and magnetic properties. AISI 316L stainless steel is a corrosion resistant material, but not magnetic. Sr1.8Y0.2CrReO6 (SYCRO) ceramic shows magnetic propriety until ~360 ºC (~640 K). 90% of 316L powder was mixed with 10% of SYCRO powder. The mixture was homogenized in a ball milling at low temperature (~77 K). The obtained powder was compacted in cylindrical forms, sealed in a evacuated quartzo tube and submitted to termal treatment for sintering. As a comparative standard, samples of 316L powder were sintered as the similar way of 316L/SYCRO samples. The sintered samples were evaluated by Scanning Electron Microscopy (SEM), X-ray Powder Diffraction (XRD), X-ray Computed Microtomography, Magnetic Susceptibility and Mechanical Compression test. The 316L/SYCRO composite showed a similar magnetism of SYCRO ceramic and a diferente mechanical behavior of sintered 316L sample. Taken into account this work it was demonstrated that it is possible to produce steel/ceramic composites with controllable contents.O trabalho descrito aqui investiga a sinterização do compósito aço/cerâmico AISI 316L/Sr1,8Y0,2CrReO6 (316L/SYCRO) produzido através da metalurgia do pó. O objetivo foi produzir um material possível de ser utilizado em manufatura aditiva com características estruturalmente resistente a impactos, a corrosão e com propriedades magnéticas. O aço AISI 316L é um material resistente à corrosão, porém não magnético. A cerâmica Sr1,8Y0,2CrReO6 (SYCRO), apresenta propriedade magnética até temperatura de Tc~360ºC (~640 K). O aço 316L na forma de pó (90%) foi misturado com 10% em massa de pó de SYCRO. A mistura foi homogeneizada em um moinho de bolas em baixa temperatura (~77 K). O pó da mistura final obtida foi compactado na forma de cilindros, selado à vácuo em uma ampola de quartzo e submetido a tratamento térmico para sinterização. Como referência comparativa, amostras do aço 316L foram sinterizadas de forma similar sem a cerâmica SYCRO. As amostras obtidas foram avaliadas através de microscopia eletrônica de varredura (MEV), difração e raios X (DRX), microtomografia computadorizada de raios X ( CT), susceptibilidade magnética e ensaio de compressão mecânica. O compósito 316L/SYCRO apresentou magnetismo similar à cerâmica SYCRO e comportamento mecânico diferente da amostra sinterizada de 316L. Com este trabalho ficou demonstrado ser possível produzir compósitos aço/cerâmicos magnéticos com teores controláveis.Texthttp://repositorio.ufes.br/handle/10/13637porUniversidade Federal do Espírito SantoDoutorado em Engenharia MecânicaPrograma de Pós-Graduação em Engenharia MecânicaUFESBRCentro Tecnológicosubject.br-rjbnEngenharia MecânicaCompósitoAISI 316LPerovskita duplaMagnetismoCompositeDouble PerovskiteMagnetismEstudo do compósito aço/ceramico AISI-316L/Sr1,8Y0,2CrReO6 produzido através da metalurgia do pótitle.alternativeinfo:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/doctoralThesisinfo:eu-repo/semantics/openAccessreponame:Repositório Institucional da Universidade Federal do Espírito Santo (riUfes)instname:Universidade Federal do Espírito Santo (UFES)instacron:UFESORIGINALJose Firmino Salvador.pdfapplication/pdf4135358http://repositorio.ufes.br/bitstreams/e885f650-9ae8-482b-82dd-fb2e95fa346c/download4abec8cf75d28a50abcb9054db75edf0MD5110/136372024-09-25 21:01:45.313oai:repositorio.ufes.br:10/13637http://repositorio.ufes.brRepositório InstitucionalPUBhttp://repositorio.ufes.br/oai/requestopendoar:21082024-10-15T17:53:58.753906Repositório Institucional da Universidade Federal do Espírito Santo (riUfes) - Universidade Federal do Espírito Santo (UFES)false
dc.title.none.fl_str_mv Estudo do compósito aço/ceramico AISI-316L/Sr1,8Y0,2CrReO6 produzido através da metalurgia do pó
dc.title.alternative.none.fl_str_mv title.alternative
title Estudo do compósito aço/ceramico AISI-316L/Sr1,8Y0,2CrReO6 produzido através da metalurgia do pó
spellingShingle Estudo do compósito aço/ceramico AISI-316L/Sr1,8Y0,2CrReO6 produzido através da metalurgia do pó
Salvador, Jose Firmino
Engenharia Mecânica
Compósito
AISI 316L
Perovskita dupla
Magnetismo
Composite
Double Perovskite
Magnetism
subject.br-rjbn
title_short Estudo do compósito aço/ceramico AISI-316L/Sr1,8Y0,2CrReO6 produzido através da metalurgia do pó
title_full Estudo do compósito aço/ceramico AISI-316L/Sr1,8Y0,2CrReO6 produzido através da metalurgia do pó
title_fullStr Estudo do compósito aço/ceramico AISI-316L/Sr1,8Y0,2CrReO6 produzido através da metalurgia do pó
title_full_unstemmed Estudo do compósito aço/ceramico AISI-316L/Sr1,8Y0,2CrReO6 produzido através da metalurgia do pó
title_sort Estudo do compósito aço/ceramico AISI-316L/Sr1,8Y0,2CrReO6 produzido através da metalurgia do pó
author Salvador, Jose Firmino
author_facet Salvador, Jose Firmino
author_role author
dc.contributor.authorID.none.fl_str_mv https://orcid.org/
dc.contributor.authorLattes.none.fl_str_mv http://lattes.cnpq.br/0061402424211214
dc.contributor.advisor1.fl_str_mv Orlando, Marcos Tadeu D Azeredo
dc.contributor.advisor1ID.fl_str_mv https://orcid.org/0000000283876504
dc.contributor.advisor1Lattes.fl_str_mv http://lattes.cnpq.br/3562894103432242
dc.contributor.author.fl_str_mv Salvador, Jose Firmino
dc.contributor.referee1.fl_str_mv Franco Junior, Adonias Ribeiro
dc.contributor.referee1ID.fl_str_mv https://orcid.org/
dc.contributor.referee1Lattes.fl_str_mv http://lattes.cnpq.br/6677652514776940
dc.contributor.referee2.fl_str_mv Passamai Junior, Jose Luis
dc.contributor.referee2ID.fl_str_mv https://orcid.org/0000-0001-6866-1460
dc.contributor.referee2Lattes.fl_str_mv http://lattes.cnpq.br/5445869592199028
dc.contributor.referee3.fl_str_mv Passos, Carlos Augusto Cardoso
dc.contributor.referee3ID.fl_str_mv https://orcid.org/2528679879816545
dc.contributor.referee3Lattes.fl_str_mv http://lattes.cnpq.br/2528679879816545
dc.contributor.referee4.fl_str_mv Vieira, Estefano Aparecido
dc.contributor.referee5.fl_str_mv Cavichini, Arthur Sant Ana
contributor_str_mv Orlando, Marcos Tadeu D Azeredo
Franco Junior, Adonias Ribeiro
Passamai Junior, Jose Luis
Passos, Carlos Augusto Cardoso
Vieira, Estefano Aparecido
Cavichini, Arthur Sant Ana
dc.subject.cnpq.fl_str_mv Engenharia Mecânica
topic Engenharia Mecânica
Compósito
AISI 316L
Perovskita dupla
Magnetismo
Composite
Double Perovskite
Magnetism
subject.br-rjbn
dc.subject.por.fl_str_mv Compósito
AISI 316L
Perovskita dupla
Magnetismo
Composite
Double Perovskite
Magnetism
dc.subject.br-rjbn.none.fl_str_mv subject.br-rjbn
description This work studies the sintering of a steel/ceramic composite with stainless steel AISI 316L and Sr1.8Y0.2CrReO6 double perovskite (316L/SYCRO) by powder metallurgy. The goal was to produce a material that could be used in additive manufacture with structurally impact, corrosion and magnetic properties. AISI 316L stainless steel is a corrosion resistant material, but not magnetic. Sr1.8Y0.2CrReO6 (SYCRO) ceramic shows magnetic propriety until ~360 ºC (~640 K). 90% of 316L powder was mixed with 10% of SYCRO powder. The mixture was homogenized in a ball milling at low temperature (~77 K). The obtained powder was compacted in cylindrical forms, sealed in a evacuated quartzo tube and submitted to termal treatment for sintering. As a comparative standard, samples of 316L powder were sintered as the similar way of 316L/SYCRO samples. The sintered samples were evaluated by Scanning Electron Microscopy (SEM), X-ray Powder Diffraction (XRD), X-ray Computed Microtomography, Magnetic Susceptibility and Mechanical Compression test. The 316L/SYCRO composite showed a similar magnetism of SYCRO ceramic and a diferente mechanical behavior of sintered 316L sample. Taken into account this work it was demonstrated that it is possible to produce steel/ceramic composites with controllable contents.
publishDate 2019
dc.date.issued.fl_str_mv 2019-06-05
dc.date.accessioned.fl_str_mv 2024-05-29T22:11:53Z
dc.date.available.fl_str_mv 2024-05-29T22:11:53Z
dc.type.status.fl_str_mv info:eu-repo/semantics/publishedVersion
dc.type.driver.fl_str_mv info:eu-repo/semantics/doctoralThesis
format doctoralThesis
status_str publishedVersion
dc.identifier.uri.fl_str_mv http://repositorio.ufes.br/handle/10/13637
url http://repositorio.ufes.br/handle/10/13637
dc.language.iso.fl_str_mv por
language por
dc.rights.driver.fl_str_mv info:eu-repo/semantics/openAccess
eu_rights_str_mv openAccess
dc.format.none.fl_str_mv Text
dc.publisher.none.fl_str_mv Universidade Federal do Espírito Santo
Doutorado em Engenharia Mecânica
dc.publisher.program.fl_str_mv Programa de Pós-Graduação em Engenharia Mecânica
dc.publisher.initials.fl_str_mv UFES
dc.publisher.country.fl_str_mv BR
dc.publisher.department.fl_str_mv Centro Tecnológico
publisher.none.fl_str_mv Universidade Federal do Espírito Santo
Doutorado em Engenharia Mecânica
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institution UFES
reponame_str Repositório Institucional da Universidade Federal do Espírito Santo (riUfes)
collection Repositório Institucional da Universidade Federal do Espírito Santo (riUfes)
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