Incorporação de nanopartículas de ferrita de cobalto (CoFe2O4) em resina epoxídica para a obtenção de nanocompósitos
Autor(a) principal: | |
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Data de Publicação: | 2016 |
Tipo de documento: | Dissertação |
Idioma: | por |
Título da fonte: | Repositório Institucional da UFG |
dARK ID: | ark:/38995/001300000dwnp |
Texto Completo: | http://repositorio.bc.ufg.br/tede/handle/tede/6858 |
Resumo: | Nanocomposites based on magnetic nanoparticles dispersed in a polymer matrix has emerged as a new class of materials that might be applied in various technology segments, such as telecommunication, aerospace and recently biomedical industry. However, obtaining nanocomposites with uniform distribution of nanoparticles in the polymeric matrix has been a challenge due to the chemical incompatibility between these materials. In this context, the objective of this study was to evaluate the homogeneity of the dispersion of cobalt ferrite (CoFe2O4) nanoparticles in an epoxy resin matrix by varying the method of incorporating them into the polymeric matrix (by adding a powder or a colloidal dispersion of nanoparticles). The prepared materials were evaluated by chemical (FTIR, AA, UV-Vis), structural (XRD), thermal (TG, DSC), morphological (DLS, SEM, TEM) and magnetic (VSM) characterization techniques. A strong correlation between the method of incorporation of the cobalt ferrite nanoparticles, the uniformity of their dispersion into the polymeric matrix and the thermal and magnetic properties of the nanocomposites was verified. |
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Sartoratto, Patrícia Pommé Confessorihttp://lattes.cnpq.br/9777959525393785Franco Júnior, Adolfohttp://lattes.cnpq.br/0187547195548392Sartoratto, Patrícia Pommé ConfessoriFranco Júnior, AdolfoCaiado, Kely LopesNunes, Liliane Magalhãeshttp://lattes.cnpq.br/5652994361900692Alves Júnior, Eli Silveira2017-02-20T11:59:07Z2016-10-18ALVES JR., E. S. Incorporação de nanopartículas de ferrita de cobalto (CoFe2O4) em resina epoxídica para a obtenção de nanocompósitos. 2016. 177 f. Dissertação (Mestrado em Química) - Universidade Federal de Goiás, Goiânia, 2016.http://repositorio.bc.ufg.br/tede/handle/tede/6858ark:/38995/001300000dwnpNanocomposites based on magnetic nanoparticles dispersed in a polymer matrix has emerged as a new class of materials that might be applied in various technology segments, such as telecommunication, aerospace and recently biomedical industry. However, obtaining nanocomposites with uniform distribution of nanoparticles in the polymeric matrix has been a challenge due to the chemical incompatibility between these materials. In this context, the objective of this study was to evaluate the homogeneity of the dispersion of cobalt ferrite (CoFe2O4) nanoparticles in an epoxy resin matrix by varying the method of incorporating them into the polymeric matrix (by adding a powder or a colloidal dispersion of nanoparticles). The prepared materials were evaluated by chemical (FTIR, AA, UV-Vis), structural (XRD), thermal (TG, DSC), morphological (DLS, SEM, TEM) and magnetic (VSM) characterization techniques. A strong correlation between the method of incorporation of the cobalt ferrite nanoparticles, the uniformity of their dispersion into the polymeric matrix and the thermal and magnetic properties of the nanocomposites was verified.Nanocompósitos de nanopartículas magnéticas dispersas numa matriz polimérica tem se destacado como uma nova classe de materiais que podem ser aplicados em diversos segmentos tecnológicos, como nas indústrias de telecomunicações, indústria aeroespacial e, recentemente, na indústria biomédica. Contudo, a confecção de nanocompósitos com distribuição uniforme das nanopartículas na matriz polimérica tem sido um desafio, em virtude da incompatibilidade química entre estes materiais. Nesse contexto, o objetivo deste trabalho foi avaliar a homogeneidade da dispersão de nanopartículas de ferrita de cobalto (CoFe2O4) em uma matriz epoxídica, variando-se o método de incorporação das nanopartícula na matriz polimérica (adicionando-se um pó ou uma dispersão coloidal de nanopartículas). As propriedades dos materiais preparados foram avaliadas pelas técnicas de caracterização química (FTIR, AA, UV-Vis), estrutural (XRD), térmica (TG, DSC), morfológica (DLS, SEM, TEM) e magnética (VSM). Verificou-se forte correlação entre o método de incorporação das nanopartículas de ferrita de cobalto, a uniformidade da dispersão destas na matriz polimérica e as propriedades térmicas e magnéticas apresentadas pelos nanocompósitos.Submitted by Luciana Ferreira (lucgeral@gmail.com) on 2017-02-20T11:58:42Z No. of bitstreams: 2 Dissertação - Eli Silveira Alves Júnior - 2016.pdf: 12417931 bytes, checksum: 6db7ee264bfc1aa30451796af3624091 (MD5) license_rdf: 0 bytes, checksum: d41d8cd98f00b204e9800998ecf8427e (MD5)Approved for entry into archive by Luciana Ferreira (lucgeral@gmail.com) on 2017-02-20T11:59:06Z (GMT) No. of bitstreams: 2 Dissertação - Eli Silveira Alves Júnior - 2016.pdf: 12417931 bytes, checksum: 6db7ee264bfc1aa30451796af3624091 (MD5) license_rdf: 0 bytes, checksum: d41d8cd98f00b204e9800998ecf8427e (MD5)Made available in DSpace on 2017-02-20T11:59:07Z (GMT). No. of bitstreams: 2 Dissertação - Eli Silveira Alves Júnior - 2016.pdf: 12417931 bytes, checksum: 6db7ee264bfc1aa30451796af3624091 (MD5) license_rdf: 0 bytes, checksum: d41d8cd98f00b204e9800998ecf8427e (MD5) Previous issue date: 2016-10-18Fundação de Amparo à Pesquisa do Estado de Goiás - FAPEGapplication/pdfporUniversidade Federal de GoiásPrograma de Pós-graduação em Química (IQ)UFGBrasilInstituto de Química - IQ (RG)http://creativecommons.org/licenses/by-nc-nd/4.0/info:eu-repo/semantics/openAccessNanocompósitosFerrita de cobaltoResina epoxídicaNanocompositesCobalt ferriteEpoxy resinQUIMICA ORGANICA::POLIMEROS E COLOIDESIncorporação de nanopartículas de ferrita de cobalto (CoFe2O4) em resina epoxídica para a obtenção de nanocompósitosIncorporation of cobalt ferrite (CoFe2O4) nanoparticles in epoxy resin for the obtainment of nanocompositesinfo:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/masterThesis66369392132541515860060060060078260667437411972788670851189960801127-961409807440757778reponame:Repositório Institucional da UFGinstname:Universidade Federal de Goiás (UFG)instacron:UFGLICENSElicense.txtlicense.txttext/plain; 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dc.title.por.fl_str_mv |
Incorporação de nanopartículas de ferrita de cobalto (CoFe2O4) em resina epoxídica para a obtenção de nanocompósitos |
dc.title.alternative.eng.fl_str_mv |
Incorporation of cobalt ferrite (CoFe2O4) nanoparticles in epoxy resin for the obtainment of nanocomposites |
title |
Incorporação de nanopartículas de ferrita de cobalto (CoFe2O4) em resina epoxídica para a obtenção de nanocompósitos |
spellingShingle |
Incorporação de nanopartículas de ferrita de cobalto (CoFe2O4) em resina epoxídica para a obtenção de nanocompósitos Alves Júnior, Eli Silveira Nanocompósitos Ferrita de cobalto Resina epoxídica Nanocomposites Cobalt ferrite Epoxy resin QUIMICA ORGANICA::POLIMEROS E COLOIDES |
title_short |
Incorporação de nanopartículas de ferrita de cobalto (CoFe2O4) em resina epoxídica para a obtenção de nanocompósitos |
title_full |
Incorporação de nanopartículas de ferrita de cobalto (CoFe2O4) em resina epoxídica para a obtenção de nanocompósitos |
title_fullStr |
Incorporação de nanopartículas de ferrita de cobalto (CoFe2O4) em resina epoxídica para a obtenção de nanocompósitos |
title_full_unstemmed |
Incorporação de nanopartículas de ferrita de cobalto (CoFe2O4) em resina epoxídica para a obtenção de nanocompósitos |
title_sort |
Incorporação de nanopartículas de ferrita de cobalto (CoFe2O4) em resina epoxídica para a obtenção de nanocompósitos |
author |
Alves Júnior, Eli Silveira |
author_facet |
Alves Júnior, Eli Silveira |
author_role |
author |
dc.contributor.advisor1.fl_str_mv |
Sartoratto, Patrícia Pommé Confessori |
dc.contributor.advisor1Lattes.fl_str_mv |
http://lattes.cnpq.br/9777959525393785 |
dc.contributor.advisor-co1.fl_str_mv |
Franco Júnior, Adolfo |
dc.contributor.advisor-co1Lattes.fl_str_mv |
http://lattes.cnpq.br/0187547195548392 |
dc.contributor.referee1.fl_str_mv |
Sartoratto, Patrícia Pommé Confessori |
dc.contributor.referee2.fl_str_mv |
Franco Júnior, Adolfo |
dc.contributor.referee3.fl_str_mv |
Caiado, Kely Lopes |
dc.contributor.referee4.fl_str_mv |
Nunes, Liliane Magalhães |
dc.contributor.authorLattes.fl_str_mv |
http://lattes.cnpq.br/5652994361900692 |
dc.contributor.author.fl_str_mv |
Alves Júnior, Eli Silveira |
contributor_str_mv |
Sartoratto, Patrícia Pommé Confessori Franco Júnior, Adolfo Sartoratto, Patrícia Pommé Confessori Franco Júnior, Adolfo Caiado, Kely Lopes Nunes, Liliane Magalhães |
dc.subject.por.fl_str_mv |
Nanocompósitos Ferrita de cobalto Resina epoxídica |
topic |
Nanocompósitos Ferrita de cobalto Resina epoxídica Nanocomposites Cobalt ferrite Epoxy resin QUIMICA ORGANICA::POLIMEROS E COLOIDES |
dc.subject.eng.fl_str_mv |
Nanocomposites Cobalt ferrite Epoxy resin |
dc.subject.cnpq.fl_str_mv |
QUIMICA ORGANICA::POLIMEROS E COLOIDES |
description |
Nanocomposites based on magnetic nanoparticles dispersed in a polymer matrix has emerged as a new class of materials that might be applied in various technology segments, such as telecommunication, aerospace and recently biomedical industry. However, obtaining nanocomposites with uniform distribution of nanoparticles in the polymeric matrix has been a challenge due to the chemical incompatibility between these materials. In this context, the objective of this study was to evaluate the homogeneity of the dispersion of cobalt ferrite (CoFe2O4) nanoparticles in an epoxy resin matrix by varying the method of incorporating them into the polymeric matrix (by adding a powder or a colloidal dispersion of nanoparticles). The prepared materials were evaluated by chemical (FTIR, AA, UV-Vis), structural (XRD), thermal (TG, DSC), morphological (DLS, SEM, TEM) and magnetic (VSM) characterization techniques. A strong correlation between the method of incorporation of the cobalt ferrite nanoparticles, the uniformity of their dispersion into the polymeric matrix and the thermal and magnetic properties of the nanocomposites was verified. |
publishDate |
2016 |
dc.date.issued.fl_str_mv |
2016-10-18 |
dc.date.accessioned.fl_str_mv |
2017-02-20T11:59:07Z |
dc.type.status.fl_str_mv |
info:eu-repo/semantics/publishedVersion |
dc.type.driver.fl_str_mv |
info:eu-repo/semantics/masterThesis |
format |
masterThesis |
status_str |
publishedVersion |
dc.identifier.citation.fl_str_mv |
ALVES JR., E. S. Incorporação de nanopartículas de ferrita de cobalto (CoFe2O4) em resina epoxídica para a obtenção de nanocompósitos. 2016. 177 f. Dissertação (Mestrado em Química) - Universidade Federal de Goiás, Goiânia, 2016. |
dc.identifier.uri.fl_str_mv |
http://repositorio.bc.ufg.br/tede/handle/tede/6858 |
dc.identifier.dark.fl_str_mv |
ark:/38995/001300000dwnp |
identifier_str_mv |
ALVES JR., E. S. Incorporação de nanopartículas de ferrita de cobalto (CoFe2O4) em resina epoxídica para a obtenção de nanocompósitos. 2016. 177 f. Dissertação (Mestrado em Química) - Universidade Federal de Goiás, Goiânia, 2016. ark:/38995/001300000dwnp |
url |
http://repositorio.bc.ufg.br/tede/handle/tede/6858 |
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por |
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por |
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8670851189960801127 |
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http://creativecommons.org/licenses/by-nc-nd/4.0/ info:eu-repo/semantics/openAccess |
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http://creativecommons.org/licenses/by-nc-nd/4.0/ |
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openAccess |
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Universidade Federal de Goiás |
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Programa de Pós-graduação em Química (IQ) |
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UFG |
dc.publisher.country.fl_str_mv |
Brasil |
dc.publisher.department.fl_str_mv |
Instituto de Química - IQ (RG) |
publisher.none.fl_str_mv |
Universidade Federal de Goiás |
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