Incorporação de nanopartículas de ferrita de cobalto (CoFe2O4) em resina epoxídica para a obtenção de nanocompósitos

Detalhes bibliográficos
Autor(a) principal: Alves Júnior, Eli Silveira
Data de Publicação: 2016
Tipo de documento: Dissertação
Idioma: por
Título da fonte: Repositório Institucional da UFG
dARK ID: ark:/38995/001300000dwnp
Texto Completo: http://repositorio.bc.ufg.br/tede/handle/tede/6858
Resumo: Nanocomposites based on magnetic nanoparticles dispersed in a polymer matrix has emerged as a new class of materials that might be applied in various technology segments, such as telecommunication, aerospace and recently biomedical industry. However, obtaining nanocomposites with uniform distribution of nanoparticles in the polymeric matrix has been a challenge due to the chemical incompatibility between these materials. In this context, the objective of this study was to evaluate the homogeneity of the dispersion of cobalt ferrite (CoFe2O4) nanoparticles in an epoxy resin matrix by varying the method of incorporating them into the polymeric matrix (by adding a powder or a colloidal dispersion of nanoparticles). The prepared materials were evaluated by chemical (FTIR, AA, UV-Vis), structural (XRD), thermal (TG, DSC), morphological (DLS, SEM, TEM) and magnetic (VSM) characterization techniques. A strong correlation between the method of incorporation of the cobalt ferrite nanoparticles, the uniformity of their dispersion into the polymeric matrix and the thermal and magnetic properties of the nanocomposites was verified.
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spelling Sartoratto, Patrícia Pommé Confessorihttp://lattes.cnpq.br/9777959525393785Franco Júnior, Adolfohttp://lattes.cnpq.br/0187547195548392Sartoratto, Patrícia Pommé ConfessoriFranco Júnior, AdolfoCaiado, Kely LopesNunes, Liliane Magalhãeshttp://lattes.cnpq.br/5652994361900692Alves Júnior, Eli Silveira2017-02-20T11:59:07Z2016-10-18ALVES JR., E. S. Incorporação de nanopartículas de ferrita de cobalto (CoFe2O4) em resina epoxídica para a obtenção de nanocompósitos. 2016. 177 f. Dissertação (Mestrado em Química) - Universidade Federal de Goiás, Goiânia, 2016.http://repositorio.bc.ufg.br/tede/handle/tede/6858ark:/38995/001300000dwnpNanocomposites based on magnetic nanoparticles dispersed in a polymer matrix has emerged as a new class of materials that might be applied in various technology segments, such as telecommunication, aerospace and recently biomedical industry. However, obtaining nanocomposites with uniform distribution of nanoparticles in the polymeric matrix has been a challenge due to the chemical incompatibility between these materials. In this context, the objective of this study was to evaluate the homogeneity of the dispersion of cobalt ferrite (CoFe2O4) nanoparticles in an epoxy resin matrix by varying the method of incorporating them into the polymeric matrix (by adding a powder or a colloidal dispersion of nanoparticles). The prepared materials were evaluated by chemical (FTIR, AA, UV-Vis), structural (XRD), thermal (TG, DSC), morphological (DLS, SEM, TEM) and magnetic (VSM) characterization techniques. A strong correlation between the method of incorporation of the cobalt ferrite nanoparticles, the uniformity of their dispersion into the polymeric matrix and the thermal and magnetic properties of the nanocomposites was verified.Nanocompósitos de nanopartículas magnéticas dispersas numa matriz polimérica tem se destacado como uma nova classe de materiais que podem ser aplicados em diversos segmentos tecnológicos, como nas indústrias de telecomunicações, indústria aeroespacial e, recentemente, na indústria biomédica. Contudo, a confecção de nanocompósitos com distribuição uniforme das nanopartículas na matriz polimérica tem sido um desafio, em virtude da incompatibilidade química entre estes materiais. Nesse contexto, o objetivo deste trabalho foi avaliar a homogeneidade da dispersão de nanopartículas de ferrita de cobalto (CoFe2O4) em uma matriz epoxídica, variando-se o método de incorporação das nanopartícula na matriz polimérica (adicionando-se um pó ou uma dispersão coloidal de nanopartículas). As propriedades dos materiais preparados foram avaliadas pelas técnicas de caracterização química (FTIR, AA, UV-Vis), estrutural (XRD), térmica (TG, DSC), morfológica (DLS, SEM, TEM) e magnética (VSM). Verificou-se forte correlação entre o método de incorporação das nanopartículas de ferrita de cobalto, a uniformidade da dispersão destas na matriz polimérica e as propriedades térmicas e magnéticas apresentadas pelos nanocompósitos.Submitted by Luciana Ferreira (lucgeral@gmail.com) on 2017-02-20T11:58:42Z No. of bitstreams: 2 Dissertação - Eli Silveira Alves Júnior - 2016.pdf: 12417931 bytes, checksum: 6db7ee264bfc1aa30451796af3624091 (MD5) license_rdf: 0 bytes, checksum: d41d8cd98f00b204e9800998ecf8427e (MD5)Approved for entry into archive by Luciana Ferreira (lucgeral@gmail.com) on 2017-02-20T11:59:06Z (GMT) No. of bitstreams: 2 Dissertação - Eli Silveira Alves Júnior - 2016.pdf: 12417931 bytes, checksum: 6db7ee264bfc1aa30451796af3624091 (MD5) license_rdf: 0 bytes, checksum: d41d8cd98f00b204e9800998ecf8427e (MD5)Made available in DSpace on 2017-02-20T11:59:07Z (GMT). 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dc.title.por.fl_str_mv Incorporação de nanopartículas de ferrita de cobalto (CoFe2O4) em resina epoxídica para a obtenção de nanocompósitos
dc.title.alternative.eng.fl_str_mv Incorporation of cobalt ferrite (CoFe2O4) nanoparticles in epoxy resin for the obtainment of nanocomposites
title Incorporação de nanopartículas de ferrita de cobalto (CoFe2O4) em resina epoxídica para a obtenção de nanocompósitos
spellingShingle Incorporação de nanopartículas de ferrita de cobalto (CoFe2O4) em resina epoxídica para a obtenção de nanocompósitos
Alves Júnior, Eli Silveira
Nanocompósitos
Ferrita de cobalto
Resina epoxídica
Nanocomposites
Cobalt ferrite
Epoxy resin
QUIMICA ORGANICA::POLIMEROS E COLOIDES
title_short Incorporação de nanopartículas de ferrita de cobalto (CoFe2O4) em resina epoxídica para a obtenção de nanocompósitos
title_full Incorporação de nanopartículas de ferrita de cobalto (CoFe2O4) em resina epoxídica para a obtenção de nanocompósitos
title_fullStr Incorporação de nanopartículas de ferrita de cobalto (CoFe2O4) em resina epoxídica para a obtenção de nanocompósitos
title_full_unstemmed Incorporação de nanopartículas de ferrita de cobalto (CoFe2O4) em resina epoxídica para a obtenção de nanocompósitos
title_sort Incorporação de nanopartículas de ferrita de cobalto (CoFe2O4) em resina epoxídica para a obtenção de nanocompósitos
author Alves Júnior, Eli Silveira
author_facet Alves Júnior, Eli Silveira
author_role author
dc.contributor.advisor1.fl_str_mv Sartoratto, Patrícia Pommé Confessori
dc.contributor.advisor1Lattes.fl_str_mv http://lattes.cnpq.br/9777959525393785
dc.contributor.advisor-co1.fl_str_mv Franco Júnior, Adolfo
dc.contributor.advisor-co1Lattes.fl_str_mv http://lattes.cnpq.br/0187547195548392
dc.contributor.referee1.fl_str_mv Sartoratto, Patrícia Pommé Confessori
dc.contributor.referee2.fl_str_mv Franco Júnior, Adolfo
dc.contributor.referee3.fl_str_mv Caiado, Kely Lopes
dc.contributor.referee4.fl_str_mv Nunes, Liliane Magalhães
dc.contributor.authorLattes.fl_str_mv http://lattes.cnpq.br/5652994361900692
dc.contributor.author.fl_str_mv Alves Júnior, Eli Silveira
contributor_str_mv Sartoratto, Patrícia Pommé Confessori
Franco Júnior, Adolfo
Sartoratto, Patrícia Pommé Confessori
Franco Júnior, Adolfo
Caiado, Kely Lopes
Nunes, Liliane Magalhães
dc.subject.por.fl_str_mv Nanocompósitos
Ferrita de cobalto
Resina epoxídica
topic Nanocompósitos
Ferrita de cobalto
Resina epoxídica
Nanocomposites
Cobalt ferrite
Epoxy resin
QUIMICA ORGANICA::POLIMEROS E COLOIDES
dc.subject.eng.fl_str_mv Nanocomposites
Cobalt ferrite
Epoxy resin
dc.subject.cnpq.fl_str_mv QUIMICA ORGANICA::POLIMEROS E COLOIDES
description Nanocomposites based on magnetic nanoparticles dispersed in a polymer matrix has emerged as a new class of materials that might be applied in various technology segments, such as telecommunication, aerospace and recently biomedical industry. However, obtaining nanocomposites with uniform distribution of nanoparticles in the polymeric matrix has been a challenge due to the chemical incompatibility between these materials. In this context, the objective of this study was to evaluate the homogeneity of the dispersion of cobalt ferrite (CoFe2O4) nanoparticles in an epoxy resin matrix by varying the method of incorporating them into the polymeric matrix (by adding a powder or a colloidal dispersion of nanoparticles). The prepared materials were evaluated by chemical (FTIR, AA, UV-Vis), structural (XRD), thermal (TG, DSC), morphological (DLS, SEM, TEM) and magnetic (VSM) characterization techniques. A strong correlation between the method of incorporation of the cobalt ferrite nanoparticles, the uniformity of their dispersion into the polymeric matrix and the thermal and magnetic properties of the nanocomposites was verified.
publishDate 2016
dc.date.issued.fl_str_mv 2016-10-18
dc.date.accessioned.fl_str_mv 2017-02-20T11:59:07Z
dc.type.status.fl_str_mv info:eu-repo/semantics/publishedVersion
dc.type.driver.fl_str_mv info:eu-repo/semantics/masterThesis
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dc.identifier.citation.fl_str_mv ALVES JR., E. S. Incorporação de nanopartículas de ferrita de cobalto (CoFe2O4) em resina epoxídica para a obtenção de nanocompósitos. 2016. 177 f. Dissertação (Mestrado em Química) - Universidade Federal de Goiás, Goiânia, 2016.
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dc.identifier.dark.fl_str_mv ark:/38995/001300000dwnp
identifier_str_mv ALVES JR., E. S. Incorporação de nanopartículas de ferrita de cobalto (CoFe2O4) em resina epoxídica para a obtenção de nanocompósitos. 2016. 177 f. Dissertação (Mestrado em Química) - Universidade Federal de Goiás, Goiânia, 2016.
ark:/38995/001300000dwnp
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dc.publisher.program.fl_str_mv Programa de Pós-graduação em Química (IQ)
dc.publisher.initials.fl_str_mv UFG
dc.publisher.country.fl_str_mv Brasil
dc.publisher.department.fl_str_mv Instituto de Química - IQ (RG)
publisher.none.fl_str_mv Universidade Federal de Goiás
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