Analysis of the chemical constituents of Thompson atemoya seed oil

Detalhes bibliográficos
Autor(a) principal: Venceslau, Adneia de Fátima Abreu
Data de Publicação: 2021
Outros Autores: Mendonça, Andressa Campos, Benedick, Lilian Aparecida Zampieri, Thomasi, Sérgio Scherrer, Nunes, Cleiton Antônio, Pinto, Luciana Matos Alves
Tipo de documento: Artigo
Idioma: eng
Título da fonte: Repositório Institucional da UFLA
Texto Completo: http://repositorio.ufla.br/jspui/handle/1/49445
Resumo: The objective of this study was to characterize the chemical composition in extracts of atemoya (var. Thompson) seed oil by spectrometric methods. The following extraction methods were performed: chemical extraction using hexane, mechanical extraction using a press, and partitioned extraction. The composition of each of the extracts was analysed by gas chromatography-mass spectrometry (GC-MS), and more than 100 compounds were identified. The major constituents of the hexane extraction were (Z)-hexadec-9-enal (49.42%) and triolein (23.28%), and the mechanically obtained extract contained elaidic acid (66.11%) and stearic acid (8.81%). In the partitioned extraction, the hydromethanolic fraction contained dihydroxyacetone (19.16%), 3-deoxy-d-mannoic lactone (16.34%), 5-hydroxymethylfurfural (10.77%), and 3-propanediol, 2-(hydroxymethyl)-2-nitro (9.89%); the hexane fraction contained gamma-sitosterol (31.73%), erucic acid (14.64%), stigmasterol (13.30%) and triolein (10.90%); the chloroform fraction contained gamma-sitosterol (22.11%), vaccenic acid (15.49%), triolein (14.65%) and stigmasterol (10.65%); and the ethyl acetate fraction contained (Z)-icos-9-enoic acid (31.28%), beta-sitosterol (16.29%), pentadecanoic acid (11.53%) and eicosanoic acid (8.01%).
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spelling Analysis of the chemical constituents of Thompson atemoya seed oilAnálise dos constituintes químicos do óleo de semente de atemoia ThompsonAnnona atemoyaSeed oil - CharacterizationGas chromatography-mass spectrometry (GC-MS)Óleo de semente - CaracterizaçãoCromatografia gasosa–espectrometria de massa (CG-EM)The objective of this study was to characterize the chemical composition in extracts of atemoya (var. Thompson) seed oil by spectrometric methods. The following extraction methods were performed: chemical extraction using hexane, mechanical extraction using a press, and partitioned extraction. The composition of each of the extracts was analysed by gas chromatography-mass spectrometry (GC-MS), and more than 100 compounds were identified. The major constituents of the hexane extraction were (Z)-hexadec-9-enal (49.42%) and triolein (23.28%), and the mechanically obtained extract contained elaidic acid (66.11%) and stearic acid (8.81%). In the partitioned extraction, the hydromethanolic fraction contained dihydroxyacetone (19.16%), 3-deoxy-d-mannoic lactone (16.34%), 5-hydroxymethylfurfural (10.77%), and 3-propanediol, 2-(hydroxymethyl)-2-nitro (9.89%); the hexane fraction contained gamma-sitosterol (31.73%), erucic acid (14.64%), stigmasterol (13.30%) and triolein (10.90%); the chloroform fraction contained gamma-sitosterol (22.11%), vaccenic acid (15.49%), triolein (14.65%) and stigmasterol (10.65%); and the ethyl acetate fraction contained (Z)-icos-9-enoic acid (31.28%), beta-sitosterol (16.29%), pentadecanoic acid (11.53%) and eicosanoic acid (8.01%).O objetivo deste trabalho foi caracterizar a composição química do óleo de semente de atemoia var. Thompson através de métodos espectrométricos. Foi realizada extração química utilizando hexano, extração mecânica utilizando prensa e uma extração particionada. A composição de cada uma das extrações foi analisada por CG/EM e mais de 100 compostos foram identificados. Os constituintes majoritários de cada extração foram hexano: (Z)-hexadec- 9-enal (49,42%) e trioleína (23,28%); prensa: ácido elaídico (66,11%) e ácido esteárico (8,81%). Na extração particionada, tem-se as frações hidrometanólica: diidroxiacetona (19,16%), lactona 3-desoxi-d-mannóica (16,34%), 5-hidroximetilfurfural (10,77%), 3-propanodiol, 2-(hidroximetil)-2-nitro (9,89%); hexânica: gama-sitosterol (31,73%), ácido erúcico (14,64%), estigmasterol (13,30%) e trioleína (10,90%); clorofórmica: gama-sitosterol (22,11%), ácido vacênico (15,49%), trioleína (14,65%) e estigmasterol (10,65%); acetato de etila: ácido (Z)- icos-9-enóico (31,28%), beta-sitosterol (16,29%), ácido pentadecanóico (11,53%) e ácido icosanóico (8,01%).Sociedade Brasileira de Fruticultura2022-02-25T20:28:45Z2022-02-25T20:28:45Z2021-10info:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/articleapplication/pdfVENCESLAU, A. de F. A. et al. Analysis of the chemical constituents of Thompson atemoya seed oil. Revista Brasileira de Fruticultura, Jaboticabal, v. 43, n. 6, e-015, 2021. DOI: http://dx.doi.org /10.1590/0100-29452021015.http://repositorio.ufla.br/jspui/handle/1/49445Revista Brasileira de Fruticulturareponame:Repositório Institucional da UFLAinstname:Universidade Federal de Lavras (UFLA)instacron:UFLAhttp://creativecommons.org/licenses/by/4.0/info:eu-repo/semantics/openAccessVenceslau, Adneia de Fátima AbreuMendonça, Andressa CamposBenedick, Lilian Aparecida ZampieriThomasi, Sérgio ScherrerNunes, Cleiton AntônioPinto, Luciana Matos Alveseng2022-02-25T20:29:17Zoai:localhost:1/49445Repositório InstitucionalPUBhttp://repositorio.ufla.br/oai/requestnivaldo@ufla.br || repositorio.biblioteca@ufla.bropendoar:2022-02-25T20:29:17Repositório Institucional da UFLA - Universidade Federal de Lavras (UFLA)false
dc.title.none.fl_str_mv Analysis of the chemical constituents of Thompson atemoya seed oil
Análise dos constituintes químicos do óleo de semente de atemoia Thompson
title Analysis of the chemical constituents of Thompson atemoya seed oil
spellingShingle Analysis of the chemical constituents of Thompson atemoya seed oil
Venceslau, Adneia de Fátima Abreu
Annona atemoya
Seed oil - Characterization
Gas chromatography-mass spectrometry (GC-MS)
Óleo de semente - Caracterização
Cromatografia gasosa–espectrometria de massa (CG-EM)
title_short Analysis of the chemical constituents of Thompson atemoya seed oil
title_full Analysis of the chemical constituents of Thompson atemoya seed oil
title_fullStr Analysis of the chemical constituents of Thompson atemoya seed oil
title_full_unstemmed Analysis of the chemical constituents of Thompson atemoya seed oil
title_sort Analysis of the chemical constituents of Thompson atemoya seed oil
author Venceslau, Adneia de Fátima Abreu
author_facet Venceslau, Adneia de Fátima Abreu
Mendonça, Andressa Campos
Benedick, Lilian Aparecida Zampieri
Thomasi, Sérgio Scherrer
Nunes, Cleiton Antônio
Pinto, Luciana Matos Alves
author_role author
author2 Mendonça, Andressa Campos
Benedick, Lilian Aparecida Zampieri
Thomasi, Sérgio Scherrer
Nunes, Cleiton Antônio
Pinto, Luciana Matos Alves
author2_role author
author
author
author
author
dc.contributor.author.fl_str_mv Venceslau, Adneia de Fátima Abreu
Mendonça, Andressa Campos
Benedick, Lilian Aparecida Zampieri
Thomasi, Sérgio Scherrer
Nunes, Cleiton Antônio
Pinto, Luciana Matos Alves
dc.subject.por.fl_str_mv Annona atemoya
Seed oil - Characterization
Gas chromatography-mass spectrometry (GC-MS)
Óleo de semente - Caracterização
Cromatografia gasosa–espectrometria de massa (CG-EM)
topic Annona atemoya
Seed oil - Characterization
Gas chromatography-mass spectrometry (GC-MS)
Óleo de semente - Caracterização
Cromatografia gasosa–espectrometria de massa (CG-EM)
description The objective of this study was to characterize the chemical composition in extracts of atemoya (var. Thompson) seed oil by spectrometric methods. The following extraction methods were performed: chemical extraction using hexane, mechanical extraction using a press, and partitioned extraction. The composition of each of the extracts was analysed by gas chromatography-mass spectrometry (GC-MS), and more than 100 compounds were identified. The major constituents of the hexane extraction were (Z)-hexadec-9-enal (49.42%) and triolein (23.28%), and the mechanically obtained extract contained elaidic acid (66.11%) and stearic acid (8.81%). In the partitioned extraction, the hydromethanolic fraction contained dihydroxyacetone (19.16%), 3-deoxy-d-mannoic lactone (16.34%), 5-hydroxymethylfurfural (10.77%), and 3-propanediol, 2-(hydroxymethyl)-2-nitro (9.89%); the hexane fraction contained gamma-sitosterol (31.73%), erucic acid (14.64%), stigmasterol (13.30%) and triolein (10.90%); the chloroform fraction contained gamma-sitosterol (22.11%), vaccenic acid (15.49%), triolein (14.65%) and stigmasterol (10.65%); and the ethyl acetate fraction contained (Z)-icos-9-enoic acid (31.28%), beta-sitosterol (16.29%), pentadecanoic acid (11.53%) and eicosanoic acid (8.01%).
publishDate 2021
dc.date.none.fl_str_mv 2021-10
2022-02-25T20:28:45Z
2022-02-25T20:28:45Z
dc.type.status.fl_str_mv info:eu-repo/semantics/publishedVersion
dc.type.driver.fl_str_mv info:eu-repo/semantics/article
format article
status_str publishedVersion
dc.identifier.uri.fl_str_mv VENCESLAU, A. de F. A. et al. Analysis of the chemical constituents of Thompson atemoya seed oil. Revista Brasileira de Fruticultura, Jaboticabal, v. 43, n. 6, e-015, 2021. DOI: http://dx.doi.org /10.1590/0100-29452021015.
http://repositorio.ufla.br/jspui/handle/1/49445
identifier_str_mv VENCESLAU, A. de F. A. et al. Analysis of the chemical constituents of Thompson atemoya seed oil. Revista Brasileira de Fruticultura, Jaboticabal, v. 43, n. 6, e-015, 2021. DOI: http://dx.doi.org /10.1590/0100-29452021015.
url http://repositorio.ufla.br/jspui/handle/1/49445
dc.language.iso.fl_str_mv eng
language eng
dc.rights.driver.fl_str_mv http://creativecommons.org/licenses/by/4.0/
info:eu-repo/semantics/openAccess
rights_invalid_str_mv http://creativecommons.org/licenses/by/4.0/
eu_rights_str_mv openAccess
dc.format.none.fl_str_mv application/pdf
dc.publisher.none.fl_str_mv Sociedade Brasileira de Fruticultura
publisher.none.fl_str_mv Sociedade Brasileira de Fruticultura
dc.source.none.fl_str_mv Revista Brasileira de Fruticultura
reponame:Repositório Institucional da UFLA
instname:Universidade Federal de Lavras (UFLA)
instacron:UFLA
instname_str Universidade Federal de Lavras (UFLA)
instacron_str UFLA
institution UFLA
reponame_str Repositório Institucional da UFLA
collection Repositório Institucional da UFLA
repository.name.fl_str_mv Repositório Institucional da UFLA - Universidade Federal de Lavras (UFLA)
repository.mail.fl_str_mv nivaldo@ufla.br || repositorio.biblioteca@ufla.br
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