Laüe back-reflection method for crystallographic orientation of a martensitic Cu-Zn-Al single crystal of the monoclinic system

Detalhes bibliográficos
Autor(a) principal: Zambrano, Uíslei Carlos
Data de Publicação: 2008
Outros Autores: Blanco, Matildes, Barelli, Nilso, Benedetti, Assis Vicente, Fernández, Javier
Tipo de documento: Artigo
Idioma: eng
Título da fonte: Repositório Institucional da UFMS
Texto Completo: https://repositorio.ufms.br/handle/123456789/470
http://dx.doi.org/10.1590/S0100-40422008000100027
Resumo: A martensitic single crystal Cu-23.95Zn-3.62(wt.%)Al alloy was obtained melting pure Cu, Zn and Al using Bridgman's method. The martensitic phase (monoclinic) can present up to 24 variants, and orienting the surface according to a certain plane is a very hard task. The single crystal was submitted to 8 tons of tension (stress) along the longitudinal direction to reduce the number of variants and facilitate the surface orientation according to the desired plane. This single crystal was oriented using the Laüe back-reflection method to give surfaces with the following oriented crystallographic planes: (010), (120) and (130). It was observed that the tension stress was applied along the [010] direction.
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spelling 2011-09-08T12:42:00Z2021-09-30T19:56:53Z2008ZAMBRANO, Uíslei Carlos et al . Laüe back-reflection method for crystallographic orientation of a martensitic Cu-Zn-Al single crystal of the monoclinic system. Quím. Nova, São Paulo, v. 31, n. 1, 2008 . Disponível em <http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0100-40422008000100027&lng=pt&nrm=iso>. acessos em 30 ago. 2011. http://dx.doi.org/10.1590/S0100-40422008000100027.https://repositorio.ufms.br/handle/123456789/470http://dx.doi.org/10.1590/S0100-40422008000100027A martensitic single crystal Cu-23.95Zn-3.62(wt.%)Al alloy was obtained melting pure Cu, Zn and Al using Bridgman's method. The martensitic phase (monoclinic) can present up to 24 variants, and orienting the surface according to a certain plane is a very hard task. The single crystal was submitted to 8 tons of tension (stress) along the longitudinal direction to reduce the number of variants and facilitate the surface orientation according to the desired plane. This single crystal was oriented using the Laüe back-reflection method to give surfaces with the following oriented crystallographic planes: (010), (120) and (130). It was observed that the tension stress was applied along the [010] direction.engQuímica NovaEletroquímicaCobreCristalografiaLaüe back-reflection method for crystallographic orientation of a martensitic Cu-Zn-Al single crystal of the monoclinic systeminfo:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/articleZambrano, Uíslei CarlosBlanco, MatildesBarelli, NilsoBenedetti, Assis VicenteFernández, Javierinfo:eu-repo/semantics/openAccessreponame:Repositório Institucional da UFMSinstname:Universidade Federal de Mato Grosso do Sul (UFMS)instacron:UFMSTHUMBNAILLaue back-reflection.pdf.jpgLaue back-reflection.pdf.jpgGenerated Thumbnailimage/jpeg1672https://repositorio.ufms.br/bitstream/123456789/470/4/Laue%20back-reflection.pdf.jpgaa79e92f451e04180935701932d84d5fMD54ORIGINALLaue back-reflection.pdfLaue back-reflection.pdfapplication/pdf3703824https://repositorio.ufms.br/bitstream/123456789/470/1/Laue%20back-reflection.pdf51ce774b8e88cf99c2c38c3df022c4aeMD51LICENSElicense.txtlicense.txttext/plain; charset=utf-81748https://repositorio.ufms.br/bitstream/123456789/470/2/license.txt8a4605be74aa9ea9d79846c1fba20a33MD52TEXTLaue back-reflection.pdf.txtLaue back-reflection.pdf.txtExtracted texttext/plain32268https://repositorio.ufms.br/bitstream/123456789/470/3/Laue%20back-reflection.pdf.txt9b396f3e13fc24c16a405fc495cbd7c3MD53123456789/4702021-09-30 15:56:53.268oai:repositorio.ufms.br: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Repositório InstitucionalPUBhttps://repositorio.ufms.br/oai/requestri.prograd@ufms.bropendoar:21242021-09-30T19:56:53Repositório Institucional da UFMS - Universidade Federal de Mato Grosso do Sul (UFMS)false
dc.title.pt_BR.fl_str_mv Laüe back-reflection method for crystallographic orientation of a martensitic Cu-Zn-Al single crystal of the monoclinic system
title Laüe back-reflection method for crystallographic orientation of a martensitic Cu-Zn-Al single crystal of the monoclinic system
spellingShingle Laüe back-reflection method for crystallographic orientation of a martensitic Cu-Zn-Al single crystal of the monoclinic system
Zambrano, Uíslei Carlos
Eletroquímica
Cobre
Cristalografia
title_short Laüe back-reflection method for crystallographic orientation of a martensitic Cu-Zn-Al single crystal of the monoclinic system
title_full Laüe back-reflection method for crystallographic orientation of a martensitic Cu-Zn-Al single crystal of the monoclinic system
title_fullStr Laüe back-reflection method for crystallographic orientation of a martensitic Cu-Zn-Al single crystal of the monoclinic system
title_full_unstemmed Laüe back-reflection method for crystallographic orientation of a martensitic Cu-Zn-Al single crystal of the monoclinic system
title_sort Laüe back-reflection method for crystallographic orientation of a martensitic Cu-Zn-Al single crystal of the monoclinic system
author Zambrano, Uíslei Carlos
author_facet Zambrano, Uíslei Carlos
Blanco, Matildes
Barelli, Nilso
Benedetti, Assis Vicente
Fernández, Javier
author_role author
author2 Blanco, Matildes
Barelli, Nilso
Benedetti, Assis Vicente
Fernández, Javier
author2_role author
author
author
author
dc.contributor.author.fl_str_mv Zambrano, Uíslei Carlos
Blanco, Matildes
Barelli, Nilso
Benedetti, Assis Vicente
Fernández, Javier
dc.subject.por.fl_str_mv Eletroquímica
Cobre
Cristalografia
topic Eletroquímica
Cobre
Cristalografia
description A martensitic single crystal Cu-23.95Zn-3.62(wt.%)Al alloy was obtained melting pure Cu, Zn and Al using Bridgman's method. The martensitic phase (monoclinic) can present up to 24 variants, and orienting the surface according to a certain plane is a very hard task. The single crystal was submitted to 8 tons of tension (stress) along the longitudinal direction to reduce the number of variants and facilitate the surface orientation according to the desired plane. This single crystal was oriented using the Laüe back-reflection method to give surfaces with the following oriented crystallographic planes: (010), (120) and (130). It was observed that the tension stress was applied along the [010] direction.
publishDate 2008
dc.date.issued.fl_str_mv 2008
dc.date.accessioned.fl_str_mv 2011-09-08T12:42:00Z
dc.date.available.fl_str_mv 2021-09-30T19:56:53Z
dc.type.status.fl_str_mv info:eu-repo/semantics/publishedVersion
dc.type.driver.fl_str_mv info:eu-repo/semantics/article
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status_str publishedVersion
dc.identifier.citation.fl_str_mv ZAMBRANO, Uíslei Carlos et al . Laüe back-reflection method for crystallographic orientation of a martensitic Cu-Zn-Al single crystal of the monoclinic system. Quím. Nova, São Paulo, v. 31, n. 1, 2008 . Disponível em <http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0100-40422008000100027&lng=pt&nrm=iso>. acessos em 30 ago. 2011. http://dx.doi.org/10.1590/S0100-40422008000100027.
dc.identifier.uri.fl_str_mv https://repositorio.ufms.br/handle/123456789/470
dc.identifier.doi.none.fl_str_mv http://dx.doi.org/10.1590/S0100-40422008000100027
identifier_str_mv ZAMBRANO, Uíslei Carlos et al . Laüe back-reflection method for crystallographic orientation of a martensitic Cu-Zn-Al single crystal of the monoclinic system. Quím. Nova, São Paulo, v. 31, n. 1, 2008 . Disponível em <http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0100-40422008000100027&lng=pt&nrm=iso>. acessos em 30 ago. 2011. http://dx.doi.org/10.1590/S0100-40422008000100027.
url https://repositorio.ufms.br/handle/123456789/470
http://dx.doi.org/10.1590/S0100-40422008000100027
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dc.publisher.none.fl_str_mv Química Nova
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