Secagem em camada de espuma (Foam-mat drying) da folha do noni (Morinda citrifolia L.)

Detalhes bibliográficos
Autor(a) principal: Lima, Anna Caroline Feitosa
Data de Publicação: 2020
Tipo de documento: Dissertação
Idioma: por
Título da fonte: Biblioteca Digital de Teses e Dissertações da UFPB
Texto Completo: https://repositorio.ufpb.br/jspui/handle/123456789/20633
Resumo: Species Morinda citrifolia L., from Rubiaceae family, popularly known as noni, although widely consumed in Asia for more than 2000 years, is still unknown in Brazil. Phytochemical studies show that noni leaves contain a variety of chemical components, including terpenoids, phytosterols, fatty acids, glycosidic iridoids, glycoside flavonoids, among others. Drying is a way to increase the shelf life of products, since by reducing water activity, the risk of proliferation of microorganisms is reduced. Among the types of drying, there is the drying in foam layer, which among several benefits is the low cost. The aim of this research was to evaluate the drying in the foam layer noni leaf to obtain its powder form. The foaming agent used was Portogel®, previously defined in preliminary tests, and the foam obtained was physically characterized in terms of stability, density and over run. The drying was carried out according to the complete factorial design of 2³ + 3 central points, with independent variables: concentration of foaming agent (3, 4 and 5%), stirring time (3, 4 and 5 minutes) and temperature drying time (50, 60 and 70 ° C) in order to verify their influence on drying time and final dry base moisture. The drying and drying rate curves showed typical behavior, characterized by a long constant period followed by a short period of decreasing rate. The highest drying rates were shown in the experiments at 70 ° C and the lowest rates at 50 ° C. The powder obtained in the eleven experiments showed average humidity values of approximately 5.07% (b.u.) and water activity of 0.288, which favors conservation and commercialization within the standards required by legislation. The other physico-chemical characterizations of the powder (yield, solubility, total soluble solids, total titratable acidity, pH, lipid content, ascorbic acid content and ash) presented values close to those found in literature for other types of powdered leaves as well as for the powdered noni fruit. The influence of addition of the foaming agent was analyzed through the lyophilized powder for the analysis of total soluble solids, pH and total titratable acidity, whose comparison with the values of the eleven experiments did not show significant changes. The best conditions found for large-scale manufacturing are those of experiment 5 (3%, 3min, 70 ° C), since it uses a low concentration of the foaming agent, it presented the second shortest drying time (140 minutes), and the shortest water activity (aw), which minimizes the chances of microbiological contamination and allows greater storage safety.
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spelling Secagem em camada de espuma (Foam-mat drying) da folha do noni (Morinda citrifolia L.)Folha de noniCinética de secagemAtividade de águaAgente espumanteNoni leafDrying kineticsWater activityFoaming agentCNPQ::ENGENHARIAS::ENGENHARIA QUIMICASpecies Morinda citrifolia L., from Rubiaceae family, popularly known as noni, although widely consumed in Asia for more than 2000 years, is still unknown in Brazil. Phytochemical studies show that noni leaves contain a variety of chemical components, including terpenoids, phytosterols, fatty acids, glycosidic iridoids, glycoside flavonoids, among others. Drying is a way to increase the shelf life of products, since by reducing water activity, the risk of proliferation of microorganisms is reduced. Among the types of drying, there is the drying in foam layer, which among several benefits is the low cost. The aim of this research was to evaluate the drying in the foam layer noni leaf to obtain its powder form. The foaming agent used was Portogel®, previously defined in preliminary tests, and the foam obtained was physically characterized in terms of stability, density and over run. The drying was carried out according to the complete factorial design of 2³ + 3 central points, with independent variables: concentration of foaming agent (3, 4 and 5%), stirring time (3, 4 and 5 minutes) and temperature drying time (50, 60 and 70 ° C) in order to verify their influence on drying time and final dry base moisture. The drying and drying rate curves showed typical behavior, characterized by a long constant period followed by a short period of decreasing rate. The highest drying rates were shown in the experiments at 70 ° C and the lowest rates at 50 ° C. The powder obtained in the eleven experiments showed average humidity values of approximately 5.07% (b.u.) and water activity of 0.288, which favors conservation and commercialization within the standards required by legislation. The other physico-chemical characterizations of the powder (yield, solubility, total soluble solids, total titratable acidity, pH, lipid content, ascorbic acid content and ash) presented values close to those found in literature for other types of powdered leaves as well as for the powdered noni fruit. The influence of addition of the foaming agent was analyzed through the lyophilized powder for the analysis of total soluble solids, pH and total titratable acidity, whose comparison with the values of the eleven experiments did not show significant changes. The best conditions found for large-scale manufacturing are those of experiment 5 (3%, 3min, 70 ° C), since it uses a low concentration of the foaming agent, it presented the second shortest drying time (140 minutes), and the shortest water activity (aw), which minimizes the chances of microbiological contamination and allows greater storage safety.Coordenação de Aperfeiçoamento de Pessoal de Nível Superior - CAPESA espécie Morinda citrifolia L., da família Rubiaceae, popularmente conhecida por noni, embora bastante consumida na Ásia há mais de 2000 anos, é ainda pouco conhecida no Brasil. Estudos fitoquímicos mostram que as folhas do noni contêm uma variedade de componentes químicos, incluindo terpenóides, fitoesteróis, ácidos graxos, iridóides glicosídicos, flavonóides glicosídeos, entre outros. A secagem é uma maneira de aumentar o tempo de vida útil de produtos, uma vez que ao se reduzir a atividade de água, diminui-se o risco de proliferação de microrganismos. E dentre os tipos de secagem, há a secagem em camada de espuma, que entre os diversos benefícios está o baixo custo. O objetivo desta pesquisa foi avaliar a secagem em camada de espuma da folha do noni para obtenção da sua forma em pó. O agente espumante utilizado foi o Portogel®, definido previamente em testes preliminares, e a espuma obtida foi caracterizada fisicamente quanto a estabilidade, densidade e over run. A secagem foi realizada de acordo com o planejamento experimental fatorial completo de 2³ + 3 pontos centrais, sendo as variáveis independentes: concentração de agente espumante (3, 4 e 5%), tempo de agitação (3, 4 e 5 minutos) e temperatura de secagem (50, 60 e 70 °C) com o intuito de verificar suas influências no tempo de secagem e umidade final de base seca. As curvas de secagem e de taxa de secagem apresentaram comportamento típico, caracterizado por um longo período constante seguido de um curto período de taxa decrescente. As maiores taxas de secagem foram apresentadas nos experimentos à temperatura de 70 °C e as menores taxas para temperatura de 50°C. O pó obtido nos onze experimentos mostraram valores médios de umidade de aproximadamente 5,07% (b.u.) e atividade de água de 0,288, o que favorece a conservação e comercialização dentro dos padrões exigidos pela legislação. As demais caracterizações físico-químicas do pó (rendimento, solubilidade, sólidos solúveis totais, acidez titulável total, pH, teor de lipídeos, teor de ácido ascórbico e cinzas) apresentaram valores próximos aos encontrados na literatura para outros tipos de folhas em pó bem como para o fruto do noni em pó. A influência da adição do agente espumante foi analisada através o pó liofilizado para as análises de sólidos solúveis totais, pH e acidez titulável total, cujo comparativo com os valores dos onze experimentos não apresentou alterações significativas. As melhores condições encontradas para a fabricação em larga escala são as do experimento 5 (3%, 3min, 70° C), pois utiliza uma baixa concentração do agente espumante, apresentou o segundo menor tempo de secagem (140 minutos), e a menor atividade de água (aw), que minimiza as chances de contaminação microbiológica e permite uma maior segurança de estocagem.Universidade Federal da ParaíbaBrasilEngenharia QuímicaPrograma de Pós-Graduação em Engenharia QuímicaUFPBCavalcante, Josilene de Assishttp://lattes.cnpq.br/5620795941510888Cornélio, Melânia Lopeshttp://lattes.cnpq.br/9470334173934601Lima, Anna Caroline Feitosa2021-08-09T16:31:10Z2020-11-262021-08-09T16:31:10Z2020-11-13info:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/masterThesishttps://repositorio.ufpb.br/jspui/handle/123456789/20633porhttp://creativecommons.org/licenses/by-nd/3.0/br/info:eu-repo/semantics/openAccessreponame:Biblioteca Digital de Teses e Dissertações da UFPBinstname:Universidade Federal da Paraíba (UFPB)instacron:UFPB2022-08-10T11:03:45Zoai:repositorio.ufpb.br:123456789/20633Biblioteca Digital de Teses e Dissertaçõeshttps://repositorio.ufpb.br/PUBhttp://tede.biblioteca.ufpb.br:8080/oai/requestdiretoria@ufpb.br|| diretoria@ufpb.bropendoar:2022-08-10T11:03:45Biblioteca Digital de Teses e Dissertações da UFPB - Universidade Federal da Paraíba (UFPB)false
dc.title.none.fl_str_mv Secagem em camada de espuma (Foam-mat drying) da folha do noni (Morinda citrifolia L.)
title Secagem em camada de espuma (Foam-mat drying) da folha do noni (Morinda citrifolia L.)
spellingShingle Secagem em camada de espuma (Foam-mat drying) da folha do noni (Morinda citrifolia L.)
Lima, Anna Caroline Feitosa
Folha de noni
Cinética de secagem
Atividade de água
Agente espumante
Noni leaf
Drying kinetics
Water activity
Foaming agent
CNPQ::ENGENHARIAS::ENGENHARIA QUIMICA
title_short Secagem em camada de espuma (Foam-mat drying) da folha do noni (Morinda citrifolia L.)
title_full Secagem em camada de espuma (Foam-mat drying) da folha do noni (Morinda citrifolia L.)
title_fullStr Secagem em camada de espuma (Foam-mat drying) da folha do noni (Morinda citrifolia L.)
title_full_unstemmed Secagem em camada de espuma (Foam-mat drying) da folha do noni (Morinda citrifolia L.)
title_sort Secagem em camada de espuma (Foam-mat drying) da folha do noni (Morinda citrifolia L.)
author Lima, Anna Caroline Feitosa
author_facet Lima, Anna Caroline Feitosa
author_role author
dc.contributor.none.fl_str_mv Cavalcante, Josilene de Assis
http://lattes.cnpq.br/5620795941510888
Cornélio, Melânia Lopes
http://lattes.cnpq.br/9470334173934601
dc.contributor.author.fl_str_mv Lima, Anna Caroline Feitosa
dc.subject.por.fl_str_mv Folha de noni
Cinética de secagem
Atividade de água
Agente espumante
Noni leaf
Drying kinetics
Water activity
Foaming agent
CNPQ::ENGENHARIAS::ENGENHARIA QUIMICA
topic Folha de noni
Cinética de secagem
Atividade de água
Agente espumante
Noni leaf
Drying kinetics
Water activity
Foaming agent
CNPQ::ENGENHARIAS::ENGENHARIA QUIMICA
description Species Morinda citrifolia L., from Rubiaceae family, popularly known as noni, although widely consumed in Asia for more than 2000 years, is still unknown in Brazil. Phytochemical studies show that noni leaves contain a variety of chemical components, including terpenoids, phytosterols, fatty acids, glycosidic iridoids, glycoside flavonoids, among others. Drying is a way to increase the shelf life of products, since by reducing water activity, the risk of proliferation of microorganisms is reduced. Among the types of drying, there is the drying in foam layer, which among several benefits is the low cost. The aim of this research was to evaluate the drying in the foam layer noni leaf to obtain its powder form. The foaming agent used was Portogel®, previously defined in preliminary tests, and the foam obtained was physically characterized in terms of stability, density and over run. The drying was carried out according to the complete factorial design of 2³ + 3 central points, with independent variables: concentration of foaming agent (3, 4 and 5%), stirring time (3, 4 and 5 minutes) and temperature drying time (50, 60 and 70 ° C) in order to verify their influence on drying time and final dry base moisture. The drying and drying rate curves showed typical behavior, characterized by a long constant period followed by a short period of decreasing rate. The highest drying rates were shown in the experiments at 70 ° C and the lowest rates at 50 ° C. The powder obtained in the eleven experiments showed average humidity values of approximately 5.07% (b.u.) and water activity of 0.288, which favors conservation and commercialization within the standards required by legislation. The other physico-chemical characterizations of the powder (yield, solubility, total soluble solids, total titratable acidity, pH, lipid content, ascorbic acid content and ash) presented values close to those found in literature for other types of powdered leaves as well as for the powdered noni fruit. The influence of addition of the foaming agent was analyzed through the lyophilized powder for the analysis of total soluble solids, pH and total titratable acidity, whose comparison with the values of the eleven experiments did not show significant changes. The best conditions found for large-scale manufacturing are those of experiment 5 (3%, 3min, 70 ° C), since it uses a low concentration of the foaming agent, it presented the second shortest drying time (140 minutes), and the shortest water activity (aw), which minimizes the chances of microbiological contamination and allows greater storage safety.
publishDate 2020
dc.date.none.fl_str_mv 2020-11-26
2020-11-13
2021-08-09T16:31:10Z
2021-08-09T16:31:10Z
dc.type.status.fl_str_mv info:eu-repo/semantics/publishedVersion
dc.type.driver.fl_str_mv info:eu-repo/semantics/masterThesis
format masterThesis
status_str publishedVersion
dc.identifier.uri.fl_str_mv https://repositorio.ufpb.br/jspui/handle/123456789/20633
url https://repositorio.ufpb.br/jspui/handle/123456789/20633
dc.language.iso.fl_str_mv por
language por
dc.rights.driver.fl_str_mv http://creativecommons.org/licenses/by-nd/3.0/br/
info:eu-repo/semantics/openAccess
rights_invalid_str_mv http://creativecommons.org/licenses/by-nd/3.0/br/
eu_rights_str_mv openAccess
dc.publisher.none.fl_str_mv Universidade Federal da Paraíba
Brasil
Engenharia Química
Programa de Pós-Graduação em Engenharia Química
UFPB
publisher.none.fl_str_mv Universidade Federal da Paraíba
Brasil
Engenharia Química
Programa de Pós-Graduação em Engenharia Química
UFPB
dc.source.none.fl_str_mv reponame:Biblioteca Digital de Teses e Dissertações da UFPB
instname:Universidade Federal da Paraíba (UFPB)
instacron:UFPB
instname_str Universidade Federal da Paraíba (UFPB)
instacron_str UFPB
institution UFPB
reponame_str Biblioteca Digital de Teses e Dissertações da UFPB
collection Biblioteca Digital de Teses e Dissertações da UFPB
repository.name.fl_str_mv Biblioteca Digital de Teses e Dissertações da UFPB - Universidade Federal da Paraíba (UFPB)
repository.mail.fl_str_mv diretoria@ufpb.br|| diretoria@ufpb.br
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