Separation of phenol from bio-oil produced from pyrolysis of agricultural wastes
Autor(a) principal: | |
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Data de Publicação: | 2017 |
Outros Autores: | , , |
Tipo de documento: | Artigo |
Idioma: | eng |
Título da fonte: | Repositório Institucional da UFRGS |
Texto Completo: | http://hdl.handle.net/10183/159743 |
Resumo: | The aim of this study was to separate phenol from Bio-Oil obtained from the pyrolysis of agricultural wastes (BAW). The BAW was obtained in one step catalytic pyrolysis in which temperature of the reactor was kept at 30°C and then increased up to 900°C. After pyrolysis, the BAW was distillated and analyzed by Gas chromatography and Mass spectrometry (GC-MS) technique and comprehensive two-dimensional gas chromatography with time-of-flight mass spectrometry detection (GC × GC/TOFMS) Where BAW showed the presence of more than 120 other important compounds and phenol. After detection, phenol was separated by solvent extraction method, where Ethyl ether (C4H10O), Caustic soda (NaOH) and Hydrochloric acid (HCl) were used to separate phenol from BAW and then Nuclear magnetic resonance spectroscopy (NMR) was done to confirm the recovery of phenol. |
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Shah, ZebanCataluña Veses, RenatoCeschi, Marco AntonioSilva, Rosângela da2017-06-20T02:32:28Z20172329-6798http://hdl.handle.net/10183/159743001023918The aim of this study was to separate phenol from Bio-Oil obtained from the pyrolysis of agricultural wastes (BAW). The BAW was obtained in one step catalytic pyrolysis in which temperature of the reactor was kept at 30°C and then increased up to 900°C. After pyrolysis, the BAW was distillated and analyzed by Gas chromatography and Mass spectrometry (GC-MS) technique and comprehensive two-dimensional gas chromatography with time-of-flight mass spectrometry detection (GC × GC/TOFMS) Where BAW showed the presence of more than 120 other important compounds and phenol. After detection, phenol was separated by solvent extraction method, where Ethyl ether (C4H10O), Caustic soda (NaOH) and Hydrochloric acid (HCl) were used to separate phenol from BAW and then Nuclear magnetic resonance spectroscopy (NMR) was done to confirm the recovery of phenol.application/pdfengModern Chemistry and Applications. Los Angeles. Vol. 5, no. 1 (Mar. 2017), 1000199Bio-óleoCromatografia gasosa : Espectrometria de massaFenóis : Extração em fase sólida : Cromatografia gasosaPiróliseBiomassaChromatographic analysisGC/MSBiomass pyrolysisBio-oil productionSeparation of phenol from bio-oil produced from pyrolysis of agricultural wastesEstrangeiroinfo:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/openAccessreponame:Repositório Institucional da UFRGSinstname:Universidade Federal do Rio Grande do Sul (UFRGS)instacron:UFRGSORIGINAL001023918.pdf001023918.pdfTexto completo (inglês)application/pdf2202926http://www.lume.ufrgs.br/bitstream/10183/159743/1/001023918.pdf2bf3d7e24f3a90a307af0e6ffa57da05MD51TEXT001023918.pdf.txt001023918.pdf.txtExtracted Texttext/plain28479http://www.lume.ufrgs.br/bitstream/10183/159743/2/001023918.pdf.txt09fd267829f5f6de854318de65905e17MD52THUMBNAIL001023918.pdf.jpg001023918.pdf.jpgGenerated Thumbnailimage/jpeg2137http://www.lume.ufrgs.br/bitstream/10183/159743/3/001023918.pdf.jpga471826afe5a6408bb39230bc522d7adMD5310183/1597432021-09-18 04:48:19.54353oai:www.lume.ufrgs.br:10183/159743Repositório de PublicaçõesPUBhttps://lume.ufrgs.br/oai/requestopendoar:2021-09-18T07:48:19Repositório Institucional da UFRGS - Universidade Federal do Rio Grande do Sul (UFRGS)false |
dc.title.pt_BR.fl_str_mv |
Separation of phenol from bio-oil produced from pyrolysis of agricultural wastes |
title |
Separation of phenol from bio-oil produced from pyrolysis of agricultural wastes |
spellingShingle |
Separation of phenol from bio-oil produced from pyrolysis of agricultural wastes Shah, Zeban Bio-óleo Cromatografia gasosa : Espectrometria de massa Fenóis : Extração em fase sólida : Cromatografia gasosa Pirólise Biomassa Chromatographic analysis GC/MS Biomass pyrolysis Bio-oil production |
title_short |
Separation of phenol from bio-oil produced from pyrolysis of agricultural wastes |
title_full |
Separation of phenol from bio-oil produced from pyrolysis of agricultural wastes |
title_fullStr |
Separation of phenol from bio-oil produced from pyrolysis of agricultural wastes |
title_full_unstemmed |
Separation of phenol from bio-oil produced from pyrolysis of agricultural wastes |
title_sort |
Separation of phenol from bio-oil produced from pyrolysis of agricultural wastes |
author |
Shah, Zeban |
author_facet |
Shah, Zeban Cataluña Veses, Renato Ceschi, Marco Antonio Silva, Rosângela da |
author_role |
author |
author2 |
Cataluña Veses, Renato Ceschi, Marco Antonio Silva, Rosângela da |
author2_role |
author author author |
dc.contributor.author.fl_str_mv |
Shah, Zeban Cataluña Veses, Renato Ceschi, Marco Antonio Silva, Rosângela da |
dc.subject.por.fl_str_mv |
Bio-óleo Cromatografia gasosa : Espectrometria de massa Fenóis : Extração em fase sólida : Cromatografia gasosa Pirólise Biomassa |
topic |
Bio-óleo Cromatografia gasosa : Espectrometria de massa Fenóis : Extração em fase sólida : Cromatografia gasosa Pirólise Biomassa Chromatographic analysis GC/MS Biomass pyrolysis Bio-oil production |
dc.subject.eng.fl_str_mv |
Chromatographic analysis GC/MS Biomass pyrolysis Bio-oil production |
description |
The aim of this study was to separate phenol from Bio-Oil obtained from the pyrolysis of agricultural wastes (BAW). The BAW was obtained in one step catalytic pyrolysis in which temperature of the reactor was kept at 30°C and then increased up to 900°C. After pyrolysis, the BAW was distillated and analyzed by Gas chromatography and Mass spectrometry (GC-MS) technique and comprehensive two-dimensional gas chromatography with time-of-flight mass spectrometry detection (GC × GC/TOFMS) Where BAW showed the presence of more than 120 other important compounds and phenol. After detection, phenol was separated by solvent extraction method, where Ethyl ether (C4H10O), Caustic soda (NaOH) and Hydrochloric acid (HCl) were used to separate phenol from BAW and then Nuclear magnetic resonance spectroscopy (NMR) was done to confirm the recovery of phenol. |
publishDate |
2017 |
dc.date.accessioned.fl_str_mv |
2017-06-20T02:32:28Z |
dc.date.issued.fl_str_mv |
2017 |
dc.type.driver.fl_str_mv |
Estrangeiro info:eu-repo/semantics/article |
dc.type.status.fl_str_mv |
info:eu-repo/semantics/publishedVersion |
format |
article |
status_str |
publishedVersion |
dc.identifier.uri.fl_str_mv |
http://hdl.handle.net/10183/159743 |
dc.identifier.issn.pt_BR.fl_str_mv |
2329-6798 |
dc.identifier.nrb.pt_BR.fl_str_mv |
001023918 |
identifier_str_mv |
2329-6798 001023918 |
url |
http://hdl.handle.net/10183/159743 |
dc.language.iso.fl_str_mv |
eng |
language |
eng |
dc.relation.ispartof.pt_BR.fl_str_mv |
Modern Chemistry and Applications. Los Angeles. Vol. 5, no. 1 (Mar. 2017), 1000199 |
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info:eu-repo/semantics/openAccess |
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openAccess |
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application/pdf |
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Repositório Institucional da UFRGS |
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