Structural Characterization of Rocks Using the X-ray Microtomography Technique

Detalhes bibliográficos
Autor(a) principal: Lima, Lithiely Melo de
Data de Publicação: 2020
Outros Autores: Soares, José Agnelo
Tipo de documento: Artigo
Idioma: eng
Título da fonte: Anuário do Instituto de Geociências (Online)
Texto Completo: https://revistas.ufrj.br/index.php/aigeo/article/view/38579
Resumo: In this article are presented the results obtained for the determination of mineral composition and petrophysical properties of eight sedimentary rock samples through a proposed new method, which is supported by X-ray microtomography image analysis (microCT). The results are compared with their corresponding ones obtained by traditional techniques in order to assess the efficiency of the new method. Three samples of carbonate rocks and five of sandstone were used in this study. Two sandstone samples come from the Rio do Peixe basin (BRP, at northeastern Brazil) while the rest were extracted from USA basins. The best results were obtained in the quantification of the mineral composition of the rocks and, consequently, in the estimation of grain density. Due to its insufficient image resolution, the microtomography was sometimes unable to quantify very small pores, giving low porosity values. The correlation between bulk densities measured by the two methods shows an intermediate efficiency. Although the results presented here indicate that the microCT image analysis is appropriate for quantification of mineral phases, this technique has potential for determination of many other physical properties, such as mechanical, electrical and fluid flow rock properties.
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spelling Structural Characterization of Rocks Using the X-ray Microtomography TechniqueCaracterização Estrutural de Rochas Utilizando a Técnica de Microtomografia de Raios-XRock density; Porosity; MineralogyRock density; Porosity; MineralogyIn this article are presented the results obtained for the determination of mineral composition and petrophysical properties of eight sedimentary rock samples through a proposed new method, which is supported by X-ray microtomography image analysis (microCT). The results are compared with their corresponding ones obtained by traditional techniques in order to assess the efficiency of the new method. Three samples of carbonate rocks and five of sandstone were used in this study. Two sandstone samples come from the Rio do Peixe basin (BRP, at northeastern Brazil) while the rest were extracted from USA basins. The best results were obtained in the quantification of the mineral composition of the rocks and, consequently, in the estimation of grain density. Due to its insufficient image resolution, the microtomography was sometimes unable to quantify very small pores, giving low porosity values. The correlation between bulk densities measured by the two methods shows an intermediate efficiency. Although the results presented here indicate that the microCT image analysis is appropriate for quantification of mineral phases, this technique has potential for determination of many other physical properties, such as mechanical, electrical and fluid flow rock properties.Neste artigo são apresentados os resultados alcançados para a determinação da composição mineral e de propriedades petrofísicas de oito amostras de rochas sedimentares a partir de um novo método proposto, o qual é suportado pela análise de imagens de microtomografia de raios-X (microCT). Os resultados são comparados com seus correspondentes obtidos por técnicas tradicionais a fim de avaliar a eficiência do novo método. Foram utilizadas neste estudo amostras secas, sendo três de rochas carbonáticas e cinco de arenitos. Duas amostras de arenito são oriundas da Bacia do Rio do Peixe (BRP, no Nordeste Brasileiro) enquanto as demais foram extraídas de bacias dos EUA. Os melhores resultados foram obtidos na quantificação da composição mineral das rochas e, consequentemente, na estimativa da densidade de grãos. Devido à resolução insuficiente das imagens, a microtomografia foi algumas vezes incapaz de quantificar adequadamente poros muito pequenos, fornecendo valores baixos demais para a porosidade. A correlação entre a densidade total medida pelos dois métodos mostra uma eficiência mediana. Embora os resultados apresentados aqui indiquem que a análise de imagens de microCT é apropriada para a quantificação das fases minerais, essa técnica apresenta potencial para a determinação de muitas outras propriedades físicas, tais como propriedades mecânicas, elétricas e de fluxo de fluidos.Universidade Federal do Rio de JaneiroRock densityPorosityMineralogyPetrobrasLima, Lithiely Melo deSoares, José Agnelo2020-09-30info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersionapplication/pdfhttps://revistas.ufrj.br/index.php/aigeo/article/view/3857910.11137/2020_3_313_322Anuário do Instituto de Geociências; Vol 43, No 3 (2020); 313_322Anuário do Instituto de Geociências; Vol 43, No 3 (2020); 313_3221982-39080101-9759reponame:Anuário do Instituto de Geociências (Online)instname:Universidade Federal do Rio de Janeiro (UFRJ)instacron:UFRJenghttps://revistas.ufrj.br/index.php/aigeo/article/view/38579/pdf/*ref*/Archilla, N.L.; Missagia, R.M.; Hollis, C.; Ceia, M.A.R.; McDonald, S.A.; Lima-Neto, I.A.; Eastwood, D.S. & Lee, P. 2016. Permeability and acoustic velocity controlling factors determined from X-ray tomography images of carbonate rocks. AAPG Bulletin, 100(8): 1289-1309. Coelho, J.M. 2016. Rochas digitais como ferramenta para a caracterização de porosidades em carbonatos. Monografia apresentada ao curso de graduação em Geofísica, Universidade Federal Fluminense, 89p. Chalmers, G.R.; Bustin, R.M. & Power, I.M. 2012. Characterization of gas shale pore systems by porosimetry, pycnometry, surface area, and field emission scanning electron microscopy/transmission electron microscopy image analyses: Examples from the Barnett, Woodford, Haynesville, Marcellus, and Doig units. AAPG Bulletin, 96(6): 1099–1119. Dal Col, A.H.; Gali, P.H. & Appoloni, C.R. 2016. Análise microestrutural de arenito da Formação Rio do Rasto pela microtomografia computadorizada por raios X. Revista Semina: Ciências Exatas e Tecnológicas, 37(2): 3-12. Dias, B.L.N.; Oliveira, D.F.; Anjos, J.M. 2017. A utilização e a relevância multidisciplinar da fluorescência de raios X. Revista Brasileira de Ensino de Física, 39: e4308-1–e4308-6. DOI: http://dx.doi.org/10.1590/1806-9126-RBEF-2017-0089. Gruia, I. 2017. Micro-tomography and X-ray analysis of geological samples. Proceedings of the Romanian Academy, Series A, 18(1): 42-49. Kubala-Kukus, A.; Banas, D.; Braziewicz, J.; Dziadowicz, M.; Kopec, E.; Majewska, U.; Mazurek, M.; Pajek, M.; Sobisz, M.; Stabrawa, I.; Wudarczyk-Mocko, J. & Gózdz, S. 2015. X-ray spectrometry and X-ray microtomography techniques for soil and geological samples analysis. Nuclear Instruments and Methods in Physics Research B, (364): 85-92. Lopes, A.P.; Fiori, A.P.; Reis-Neto, J.M.; Marchese, C.; Vasconcellos, E.M.G.; Trzaskos, B.; Onishi, C.T.; Pinto-Coelho, C.V.; Secchi, R. & Silva, G.F. 2012. Análise tridimensional de rochas por meio de microtomografia computadorizada de raios X integrada à Petrografia. Geociências, 31(1): 129-142. Oliveira, N.M. & Soares, J.A. 2018. Microtomographic analysis of controlling parameters on permeability and elastic velocities of black shales. Journal of Geophysical Engineering, 15: 2433-2441. Palombo, L.; Ulsen, C.; Uliana, D.; Costa, F.R.; Yamamoto, M. & Kahn, H. 2015. Caracterização de rochas reservatório por microtomografia de raios X. Revista HOLOS, 5: 65-72. DOI: 10.15628/holos.2015.3103. Reis-Neto, J.M.; Fiori, A.P.; Lopes, A.P.; Marchese, C.; Pinto-Coelho, C.V.; Vasconcellos, E.M.G.; Silva, G.F. & Secchi, R. 2011. A microtomografia computadorizada de raios X integrada à petrografia no estudo tridimensional de porosidade em rochas. Revista Brasileira de Geociências, 41(3): 498-508. Schmitt, M.; Fernandes, C.P.; Wolf, F.G.; Cunha, J.A.B.; Rahner, C.P. & Santos, V.S.S. 2015. Characterization of Brazilian tight gas sandstones relating permeability and Angstrom-to micron-scale pore structures. Journal of Natural Gas Science and Engineering, 27: 785-807. Sena, M.R.S. & Soares, J.A. 2017. Effect of mineral composition of carbonate rocks on their petrophysical properties. Revista Brasileira de Geofísica, 35(1): 45-55. Soares, J.A.; Andrade, P.R.L. & Batista, J.T. 2018. Contributions of digital image analysis to sedimentary rock characterization. Revista Brasileira de Geofísica, 36(4): 1-15.Copyright (c) 2020 Anuário do Instituto de Geociênciashttp://creativecommons.org/licenses/by/4.0info:eu-repo/semantics/openAccess2020-10-06T16:22:34Zoai:www.revistas.ufrj.br:article/38579Revistahttps://revistas.ufrj.br/index.php/aigeo/indexPUBhttps://revistas.ufrj.br/index.php/aigeo/oaianuario@igeo.ufrj.br||1982-39080101-9759opendoar:2020-10-06T16:22:34Anuário do Instituto de Geociências (Online) - Universidade Federal do Rio de Janeiro (UFRJ)false
dc.title.none.fl_str_mv Structural Characterization of Rocks Using the X-ray Microtomography Technique
Caracterização Estrutural de Rochas Utilizando a Técnica de Microtomografia de Raios-X
title Structural Characterization of Rocks Using the X-ray Microtomography Technique
spellingShingle Structural Characterization of Rocks Using the X-ray Microtomography Technique
Lima, Lithiely Melo de
Rock density; Porosity; Mineralogy
Rock density; Porosity; Mineralogy
title_short Structural Characterization of Rocks Using the X-ray Microtomography Technique
title_full Structural Characterization of Rocks Using the X-ray Microtomography Technique
title_fullStr Structural Characterization of Rocks Using the X-ray Microtomography Technique
title_full_unstemmed Structural Characterization of Rocks Using the X-ray Microtomography Technique
title_sort Structural Characterization of Rocks Using the X-ray Microtomography Technique
author Lima, Lithiely Melo de
author_facet Lima, Lithiely Melo de
Soares, José Agnelo
author_role author
author2 Soares, José Agnelo
author2_role author
dc.contributor.none.fl_str_mv Rock density
Porosity
Mineralogy
Petrobras
dc.contributor.author.fl_str_mv Lima, Lithiely Melo de
Soares, José Agnelo
dc.subject.por.fl_str_mv Rock density; Porosity; Mineralogy
Rock density; Porosity; Mineralogy
topic Rock density; Porosity; Mineralogy
Rock density; Porosity; Mineralogy
description In this article are presented the results obtained for the determination of mineral composition and petrophysical properties of eight sedimentary rock samples through a proposed new method, which is supported by X-ray microtomography image analysis (microCT). The results are compared with their corresponding ones obtained by traditional techniques in order to assess the efficiency of the new method. Three samples of carbonate rocks and five of sandstone were used in this study. Two sandstone samples come from the Rio do Peixe basin (BRP, at northeastern Brazil) while the rest were extracted from USA basins. The best results were obtained in the quantification of the mineral composition of the rocks and, consequently, in the estimation of grain density. Due to its insufficient image resolution, the microtomography was sometimes unable to quantify very small pores, giving low porosity values. The correlation between bulk densities measured by the two methods shows an intermediate efficiency. Although the results presented here indicate that the microCT image analysis is appropriate for quantification of mineral phases, this technique has potential for determination of many other physical properties, such as mechanical, electrical and fluid flow rock properties.
publishDate 2020
dc.date.none.fl_str_mv 2020-09-30
dc.type.none.fl_str_mv

dc.type.driver.fl_str_mv info:eu-repo/semantics/article
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dc.identifier.uri.fl_str_mv https://revistas.ufrj.br/index.php/aigeo/article/view/38579
10.11137/2020_3_313_322
url https://revistas.ufrj.br/index.php/aigeo/article/view/38579
identifier_str_mv 10.11137/2020_3_313_322
dc.language.iso.fl_str_mv eng
language eng
dc.relation.none.fl_str_mv https://revistas.ufrj.br/index.php/aigeo/article/view/38579/pdf
/*ref*/Archilla, N.L.; Missagia, R.M.; Hollis, C.; Ceia, M.A.R.; McDonald, S.A.; Lima-Neto, I.A.; Eastwood, D.S. & Lee, P. 2016. Permeability and acoustic velocity controlling factors determined from X-ray tomography images of carbonate rocks. AAPG Bulletin, 100(8): 1289-1309. Coelho, J.M. 2016. Rochas digitais como ferramenta para a caracterização de porosidades em carbonatos. Monografia apresentada ao curso de graduação em Geofísica, Universidade Federal Fluminense, 89p. Chalmers, G.R.; Bustin, R.M. & Power, I.M. 2012. Characterization of gas shale pore systems by porosimetry, pycnometry, surface area, and field emission scanning electron microscopy/transmission electron microscopy image analyses: Examples from the Barnett, Woodford, Haynesville, Marcellus, and Doig units. AAPG Bulletin, 96(6): 1099–1119. Dal Col, A.H.; Gali, P.H. & Appoloni, C.R. 2016. Análise microestrutural de arenito da Formação Rio do Rasto pela microtomografia computadorizada por raios X. Revista Semina: Ciências Exatas e Tecnológicas, 37(2): 3-12. Dias, B.L.N.; Oliveira, D.F.; Anjos, J.M. 2017. A utilização e a relevância multidisciplinar da fluorescência de raios X. Revista Brasileira de Ensino de Física, 39: e4308-1–e4308-6. DOI: http://dx.doi.org/10.1590/1806-9126-RBEF-2017-0089. Gruia, I. 2017. Micro-tomography and X-ray analysis of geological samples. Proceedings of the Romanian Academy, Series A, 18(1): 42-49. Kubala-Kukus, A.; Banas, D.; Braziewicz, J.; Dziadowicz, M.; Kopec, E.; Majewska, U.; Mazurek, M.; Pajek, M.; Sobisz, M.; Stabrawa, I.; Wudarczyk-Mocko, J. & Gózdz, S. 2015. X-ray spectrometry and X-ray microtomography techniques for soil and geological samples analysis. Nuclear Instruments and Methods in Physics Research B, (364): 85-92. Lopes, A.P.; Fiori, A.P.; Reis-Neto, J.M.; Marchese, C.; Vasconcellos, E.M.G.; Trzaskos, B.; Onishi, C.T.; Pinto-Coelho, C.V.; Secchi, R. & Silva, G.F. 2012. Análise tridimensional de rochas por meio de microtomografia computadorizada de raios X integrada à Petrografia. Geociências, 31(1): 129-142. Oliveira, N.M. & Soares, J.A. 2018. Microtomographic analysis of controlling parameters on permeability and elastic velocities of black shales. Journal of Geophysical Engineering, 15: 2433-2441. Palombo, L.; Ulsen, C.; Uliana, D.; Costa, F.R.; Yamamoto, M. & Kahn, H. 2015. Caracterização de rochas reservatório por microtomografia de raios X. Revista HOLOS, 5: 65-72. DOI: 10.15628/holos.2015.3103. Reis-Neto, J.M.; Fiori, A.P.; Lopes, A.P.; Marchese, C.; Pinto-Coelho, C.V.; Vasconcellos, E.M.G.; Silva, G.F. & Secchi, R. 2011. A microtomografia computadorizada de raios X integrada à petrografia no estudo tridimensional de porosidade em rochas. Revista Brasileira de Geociências, 41(3): 498-508. Schmitt, M.; Fernandes, C.P.; Wolf, F.G.; Cunha, J.A.B.; Rahner, C.P. & Santos, V.S.S. 2015. Characterization of Brazilian tight gas sandstones relating permeability and Angstrom-to micron-scale pore structures. Journal of Natural Gas Science and Engineering, 27: 785-807. Sena, M.R.S. & Soares, J.A. 2017. Effect of mineral composition of carbonate rocks on their petrophysical properties. Revista Brasileira de Geofísica, 35(1): 45-55. Soares, J.A.; Andrade, P.R.L. & Batista, J.T. 2018. Contributions of digital image analysis to sedimentary rock characterization. Revista Brasileira de Geofísica, 36(4): 1-15.
dc.rights.driver.fl_str_mv Copyright (c) 2020 Anuário do Instituto de Geociências
http://creativecommons.org/licenses/by/4.0
info:eu-repo/semantics/openAccess
rights_invalid_str_mv Copyright (c) 2020 Anuário do Instituto de Geociências
http://creativecommons.org/licenses/by/4.0
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dc.publisher.none.fl_str_mv Universidade Federal do Rio de Janeiro
publisher.none.fl_str_mv Universidade Federal do Rio de Janeiro
dc.source.none.fl_str_mv Anuário do Instituto de Geociências; Vol 43, No 3 (2020); 313_322
Anuário do Instituto de Geociências; Vol 43, No 3 (2020); 313_322
1982-3908
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