Compósitos poliméricos a base de fibras de licuri: efeitos da hibridização e do envelhecimento ambiental acelerado

Detalhes bibliográficos
Autor(a) principal: Leão, Mirtânia Antunes
Data de Publicação: 2013
Tipo de documento: Tese
Idioma: por
Título da fonte: Repositório Institucional da UFRN
Texto Completo: https://repositorio.ufrn.br/jspui/handle/123456789/12822
Resumo: The gradual replacement of conventional materials by the ones called composite materials is becoming a concern about the response of these composites against adverse environmental conditions, such as ultraviolet radiation, high temperature and moist. Also the search for new composite using natural fibers or a blend of it with synthetic fibers as reinforcement has been studied. In this sense, this research begins with a thorough study of microstructural characterization of licuri fiber, as a proposal of alternative reinforcement to polymeric composites. Thus, a study about the development of two composite laminates was done. The first one, involving only the fiber of licuri and the second comprising a hybrid composite based of fiber glass E and the fiber of licuri, in order to know the performance of the fiber when of fiber across the hybridization process. The laminates were made in the form of plates using the tereftálica ortho-polyester resin as matrix. The composite laminate made only by licuri fiber had two reinforcing fabric layers of unidirectional licuri and the hybrid composite had two reinforcing layers of unidirectional licuri fabric and three layers of fiber short glass-E mat. Finally, both laminates was exposed to aging acceleration in order to study the influence of environmental degradation involving the mechanical properties and fracture characteristics thereof. Regarding the mechanical properties of composites, these were determined through uniaxial tensile tests, uniaxial compression and three bending points for both laminates in original state, and uniaxial tensile tests and three bending points after accelerated aging. As regards the study of structural degradation due to aging of the laminates, it was carried out based on microscopic analysis and microstructure, as well as measuring weight loss. The characteristics of the fracture was performed by macroscopic and microscopic (optical and SEM) analysis. In general, the laminated composites based on fiber licuri showed some advantages in their responses to environmental aging. These advantages are observed in the behavior related to stiffness as well as the microstructural degradation and photo-oxidation processes. However, the structural integrity of this laminate was more affected in case the action of uniaxial tensile loads, where it was noted a lower rate of withholding his last resistance property
id UFRN_43c17be98dd93606d2cd094caab860f9
oai_identifier_str oai:https://repositorio.ufrn.br:123456789/12822
network_acronym_str UFRN
network_name_str Repositório Institucional da UFRN
repository_id_str
spelling Leão, Mirtânia Antuneshttp://lattes.cnpq.br/9156822767910160http://lattes.cnpq.br/1196595599227394Ribeiro, Kilder César de Araújohttp://lattes.cnpq.br/2642512473401139Felipe, Raimundo Nonato Barbosahttp://lattes.cnpq.br/7520491414631153Felipe, Renata Carla Tavares Santoshttp://lattes.cnpq.br/6720439923599015Nascimento, Rubens Maribondo dohttp://lattes.cnpq.br/8671649752936793Aquino, Eve Maria Freire de2014-12-17T14:07:15Z2013-09-032014-12-17T14:07:15Z2013-05-03LEÃO, Mirtânia Antunes. Compósitos poliméricos a base de fibras de licuri: efeitos da hibridização e do envelhecimento ambiental acelerado. 2013. 190 f. Tese (Doutorado em Processamento de Materiais a partir do Pó; Polímeros e Compósitos; Processamento de Materiais a part) - Universidade Federal do Rio Grande do Norte, Natal, 2013.https://repositorio.ufrn.br/jspui/handle/123456789/12822The gradual replacement of conventional materials by the ones called composite materials is becoming a concern about the response of these composites against adverse environmental conditions, such as ultraviolet radiation, high temperature and moist. Also the search for new composite using natural fibers or a blend of it with synthetic fibers as reinforcement has been studied. In this sense, this research begins with a thorough study of microstructural characterization of licuri fiber, as a proposal of alternative reinforcement to polymeric composites. Thus, a study about the development of two composite laminates was done. The first one, involving only the fiber of licuri and the second comprising a hybrid composite based of fiber glass E and the fiber of licuri, in order to know the performance of the fiber when of fiber across the hybridization process. The laminates were made in the form of plates using the tereftálica ortho-polyester resin as matrix. The composite laminate made only by licuri fiber had two reinforcing fabric layers of unidirectional licuri and the hybrid composite had two reinforcing layers of unidirectional licuri fabric and three layers of fiber short glass-E mat. Finally, both laminates was exposed to aging acceleration in order to study the influence of environmental degradation involving the mechanical properties and fracture characteristics thereof. Regarding the mechanical properties of composites, these were determined through uniaxial tensile tests, uniaxial compression and three bending points for both laminates in original state, and uniaxial tensile tests and three bending points after accelerated aging. As regards the study of structural degradation due to aging of the laminates, it was carried out based on microscopic analysis and microstructure, as well as measuring weight loss. The characteristics of the fracture was performed by macroscopic and microscopic (optical and SEM) analysis. In general, the laminated composites based on fiber licuri showed some advantages in their responses to environmental aging. These advantages are observed in the behavior related to stiffness as well as the microstructural degradation and photo-oxidation processes. However, the structural integrity of this laminate was more affected in case the action of uniaxial tensile loads, where it was noted a lower rate of withholding his last resistance propertyA substituição gradativa dos materiais ditos convencionais por materiais compósitos vem se tornando uma preocupação quanto à resposta destes frente a condições ambientais adversas, tais como, a presença de radiação ultravioleta, alta temperatura e umidade. Também a busca de novos compósitos que utilizem fibras naturais ou uma mistura de fibras naturais com fibras sintéticas como reforço tem sido objeto de estudo. Neste sentido, o presente trabalho de pesquisa inicia com um completo estudo de caracterização microestrutural da fibra de licuri, essa como proposta alternativa de reforço aos compósitos poliméricos. Em seguida, foi realizado um estudo do desenvolvimento de dois laminados compósitos, um somente a base de fibra de licuri e um laminado híbrido a base de fibra de licuri e fibra de vidro-E, de modo a conhecer o comportamento da fibra de licuri frente ao processo de hibridização. Os laminados foram confeccionados em forma de placas utilizando a resina poliéster orto-tereftálica como matriz. O laminado compósito só de fibras de licuri teve como reforço duas lâminas de tecido unidirecional e o laminado híbrido teve como reforço duas lâminas desse mesmo tecido unidirecional e três lâminas de manta de fibras curtas de vidro-E. Por fim, os dois laminados compósitos foram submetidos ao processo de envelhecimento ambiental acelerado para o estudo da influência da degradação ambiental nas propriedades mecânicas e características da fratura dos mesmos. Quanto às propriedades mecânicas dos laminados compósitos, estas foram determinadas através dos ensaios de tração uniaxial, compressão uniaxial e flexão em três pontos no estado original, e de tração uniaxial e flexão em três pontos após envelhecimento acelerado. Quanto ao estudo da degradação estrutural dos laminados devido ao envelhecimento, o mesmo foi realizado com base nas análises microscópicas da microestrutura e, bem como, da medição de perda de massa. As características da fratura foram realizadas através de análises macroscópicas e microscópicas (ótica e MEV). De forma geral os laminados compósitos a base de fibras de licuri, apresentaram algumas vantagens em suas respostas frente ao envelhecimento ambiental. Essas vantagens são evidenciadas no comportamento relacionado à rigidez, bem como, aos processos fotoxidação e degradação microestrutural. Entretanto, a integridade estrutural desse laminado foi mais afetada para o caso ação de cargas uniaxiais de tração onde foi verificada uma menor taxa de retenção de sua propriedade de resistência últimaCoordenação de Aperfeiçoamento de Pessoal de Nível Superiorapplication/pdfporUniversidade Federal do Rio Grande do NortePrograma de Pós-Graduação em Ciência e Engenharia de MateriaisUFRNBRProcessamento de Materiais a partir do Pó; Polímeros e Compósitos; Processamento de Materiais a partCompósitos poliméricos. Fibras de Licuri. Hibridização e envelhecimento ambiental aceleradoPolymeric composites. Licuri fibers and accelerated environmental ageingCNPQ::OUTROSCompósitos poliméricos a base de fibras de licuri: efeitos da hibridização e do envelhecimento ambiental aceleradoinfo:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/doctoralThesisinfo:eu-repo/semantics/openAccessreponame:Repositório Institucional da UFRNinstname:Universidade Federal do Rio Grande do Norte (UFRN)instacron:UFRNORIGINALCompósitosPoliméricosBase_Leao_2013.pdfCompósitosPoliméricosBase_Leao_2013.pdfapplication/pdf14661352https://repositorio.ufrn.br/bitstream/123456789/12822/1/Comp%c3%b3sitosPolim%c3%a9ricosBase_Leao_2013.pdf527da7422d4330badc921b0d8b269abaMD51TEXTMirtaniaAL_TESE.pdf.txtMirtaniaAL_TESE.pdf.txtExtracted texttext/plain294256https://repositorio.ufrn.br/bitstream/123456789/12822/6/MirtaniaAL_TESE.pdf.txtbbfeb904a670614ddcee9e919956f405MD56CompósitosPoliméricosBase_Leao_2013.pdf.txtCompósitosPoliméricosBase_Leao_2013.pdf.txtExtracted texttext/plain294256https://repositorio.ufrn.br/bitstream/123456789/12822/8/Comp%c3%b3sitosPolim%c3%a9ricosBase_Leao_2013.pdf.txtbbfeb904a670614ddcee9e919956f405MD58THUMBNAILMirtaniaAL_TESE.pdf.jpgMirtaniaAL_TESE.pdf.jpgIM Thumbnailimage/jpeg3825https://repositorio.ufrn.br/bitstream/123456789/12822/7/MirtaniaAL_TESE.pdf.jpgb92592114f3a727afc915777cee54ad3MD57CompósitosPoliméricosBase_Leao_2013.pdf.jpgCompósitosPoliméricosBase_Leao_2013.pdf.jpgIM Thumbnailimage/jpeg3825https://repositorio.ufrn.br/bitstream/123456789/12822/9/Comp%c3%b3sitosPolim%c3%a9ricosBase_Leao_2013.pdf.jpgb92592114f3a727afc915777cee54ad3MD59123456789/128222019-01-29 18:36:22.587oai:https://repositorio.ufrn.br:123456789/12822Repositório de PublicaçõesPUBhttp://repositorio.ufrn.br/oai/opendoar:2019-01-29T21:36:22Repositório Institucional da UFRN - Universidade Federal do Rio Grande do Norte (UFRN)false
dc.title.por.fl_str_mv Compósitos poliméricos a base de fibras de licuri: efeitos da hibridização e do envelhecimento ambiental acelerado
title Compósitos poliméricos a base de fibras de licuri: efeitos da hibridização e do envelhecimento ambiental acelerado
spellingShingle Compósitos poliméricos a base de fibras de licuri: efeitos da hibridização e do envelhecimento ambiental acelerado
Leão, Mirtânia Antunes
Compósitos poliméricos. Fibras de Licuri. Hibridização e envelhecimento ambiental acelerado
Polymeric composites. Licuri fibers and accelerated environmental ageing
CNPQ::OUTROS
title_short Compósitos poliméricos a base de fibras de licuri: efeitos da hibridização e do envelhecimento ambiental acelerado
title_full Compósitos poliméricos a base de fibras de licuri: efeitos da hibridização e do envelhecimento ambiental acelerado
title_fullStr Compósitos poliméricos a base de fibras de licuri: efeitos da hibridização e do envelhecimento ambiental acelerado
title_full_unstemmed Compósitos poliméricos a base de fibras de licuri: efeitos da hibridização e do envelhecimento ambiental acelerado
title_sort Compósitos poliméricos a base de fibras de licuri: efeitos da hibridização e do envelhecimento ambiental acelerado
author Leão, Mirtânia Antunes
author_facet Leão, Mirtânia Antunes
author_role author
dc.contributor.authorID.por.fl_str_mv
dc.contributor.authorLattes.por.fl_str_mv http://lattes.cnpq.br/9156822767910160
dc.contributor.advisorID.por.fl_str_mv
dc.contributor.advisorLattes.por.fl_str_mv http://lattes.cnpq.br/1196595599227394
dc.contributor.referees1.pt_BR.fl_str_mv Ribeiro, Kilder César de Araújo
dc.contributor.referees1ID.por.fl_str_mv
dc.contributor.referees1Lattes.por.fl_str_mv http://lattes.cnpq.br/2642512473401139
dc.contributor.referees2.pt_BR.fl_str_mv Felipe, Raimundo Nonato Barbosa
dc.contributor.referees2ID.por.fl_str_mv
dc.contributor.referees2Lattes.por.fl_str_mv http://lattes.cnpq.br/7520491414631153
dc.contributor.referees3.pt_BR.fl_str_mv Felipe, Renata Carla Tavares Santos
dc.contributor.referees3ID.por.fl_str_mv
dc.contributor.referees3Lattes.por.fl_str_mv http://lattes.cnpq.br/6720439923599015
dc.contributor.referees4.pt_BR.fl_str_mv Nascimento, Rubens Maribondo do
dc.contributor.referees4ID.por.fl_str_mv
dc.contributor.referees4Lattes.por.fl_str_mv http://lattes.cnpq.br/8671649752936793
dc.contributor.author.fl_str_mv Leão, Mirtânia Antunes
dc.contributor.advisor1.fl_str_mv Aquino, Eve Maria Freire de
contributor_str_mv Aquino, Eve Maria Freire de
dc.subject.por.fl_str_mv Compósitos poliméricos. Fibras de Licuri. Hibridização e envelhecimento ambiental acelerado
topic Compósitos poliméricos. Fibras de Licuri. Hibridização e envelhecimento ambiental acelerado
Polymeric composites. Licuri fibers and accelerated environmental ageing
CNPQ::OUTROS
dc.subject.eng.fl_str_mv Polymeric composites. Licuri fibers and accelerated environmental ageing
dc.subject.cnpq.fl_str_mv CNPQ::OUTROS
description The gradual replacement of conventional materials by the ones called composite materials is becoming a concern about the response of these composites against adverse environmental conditions, such as ultraviolet radiation, high temperature and moist. Also the search for new composite using natural fibers or a blend of it with synthetic fibers as reinforcement has been studied. In this sense, this research begins with a thorough study of microstructural characterization of licuri fiber, as a proposal of alternative reinforcement to polymeric composites. Thus, a study about the development of two composite laminates was done. The first one, involving only the fiber of licuri and the second comprising a hybrid composite based of fiber glass E and the fiber of licuri, in order to know the performance of the fiber when of fiber across the hybridization process. The laminates were made in the form of plates using the tereftálica ortho-polyester resin as matrix. The composite laminate made only by licuri fiber had two reinforcing fabric layers of unidirectional licuri and the hybrid composite had two reinforcing layers of unidirectional licuri fabric and three layers of fiber short glass-E mat. Finally, both laminates was exposed to aging acceleration in order to study the influence of environmental degradation involving the mechanical properties and fracture characteristics thereof. Regarding the mechanical properties of composites, these were determined through uniaxial tensile tests, uniaxial compression and three bending points for both laminates in original state, and uniaxial tensile tests and three bending points after accelerated aging. As regards the study of structural degradation due to aging of the laminates, it was carried out based on microscopic analysis and microstructure, as well as measuring weight loss. The characteristics of the fracture was performed by macroscopic and microscopic (optical and SEM) analysis. In general, the laminated composites based on fiber licuri showed some advantages in their responses to environmental aging. These advantages are observed in the behavior related to stiffness as well as the microstructural degradation and photo-oxidation processes. However, the structural integrity of this laminate was more affected in case the action of uniaxial tensile loads, where it was noted a lower rate of withholding his last resistance property
publishDate 2013
dc.date.available.fl_str_mv 2013-09-03
2014-12-17T14:07:15Z
dc.date.issued.fl_str_mv 2013-05-03
dc.date.accessioned.fl_str_mv 2014-12-17T14:07:15Z
dc.type.status.fl_str_mv info:eu-repo/semantics/publishedVersion
dc.type.driver.fl_str_mv info:eu-repo/semantics/doctoralThesis
format doctoralThesis
status_str publishedVersion
dc.identifier.citation.fl_str_mv LEÃO, Mirtânia Antunes. Compósitos poliméricos a base de fibras de licuri: efeitos da hibridização e do envelhecimento ambiental acelerado. 2013. 190 f. Tese (Doutorado em Processamento de Materiais a partir do Pó; Polímeros e Compósitos; Processamento de Materiais a part) - Universidade Federal do Rio Grande do Norte, Natal, 2013.
dc.identifier.uri.fl_str_mv https://repositorio.ufrn.br/jspui/handle/123456789/12822
identifier_str_mv LEÃO, Mirtânia Antunes. Compósitos poliméricos a base de fibras de licuri: efeitos da hibridização e do envelhecimento ambiental acelerado. 2013. 190 f. Tese (Doutorado em Processamento de Materiais a partir do Pó; Polímeros e Compósitos; Processamento de Materiais a part) - Universidade Federal do Rio Grande do Norte, Natal, 2013.
url https://repositorio.ufrn.br/jspui/handle/123456789/12822
dc.language.iso.fl_str_mv por
language por
dc.rights.driver.fl_str_mv info:eu-repo/semantics/openAccess
eu_rights_str_mv openAccess
dc.format.none.fl_str_mv application/pdf
dc.publisher.none.fl_str_mv Universidade Federal do Rio Grande do Norte
dc.publisher.program.fl_str_mv Programa de Pós-Graduação em Ciência e Engenharia de Materiais
dc.publisher.initials.fl_str_mv UFRN
dc.publisher.country.fl_str_mv BR
dc.publisher.department.fl_str_mv Processamento de Materiais a partir do Pó; Polímeros e Compósitos; Processamento de Materiais a part
publisher.none.fl_str_mv Universidade Federal do Rio Grande do Norte
dc.source.none.fl_str_mv reponame:Repositório Institucional da UFRN
instname:Universidade Federal do Rio Grande do Norte (UFRN)
instacron:UFRN
instname_str Universidade Federal do Rio Grande do Norte (UFRN)
instacron_str UFRN
institution UFRN
reponame_str Repositório Institucional da UFRN
collection Repositório Institucional da UFRN
bitstream.url.fl_str_mv https://repositorio.ufrn.br/bitstream/123456789/12822/1/Comp%c3%b3sitosPolim%c3%a9ricosBase_Leao_2013.pdf
https://repositorio.ufrn.br/bitstream/123456789/12822/6/MirtaniaAL_TESE.pdf.txt
https://repositorio.ufrn.br/bitstream/123456789/12822/8/Comp%c3%b3sitosPolim%c3%a9ricosBase_Leao_2013.pdf.txt
https://repositorio.ufrn.br/bitstream/123456789/12822/7/MirtaniaAL_TESE.pdf.jpg
https://repositorio.ufrn.br/bitstream/123456789/12822/9/Comp%c3%b3sitosPolim%c3%a9ricosBase_Leao_2013.pdf.jpg
bitstream.checksum.fl_str_mv 527da7422d4330badc921b0d8b269aba
bbfeb904a670614ddcee9e919956f405
bbfeb904a670614ddcee9e919956f405
b92592114f3a727afc915777cee54ad3
b92592114f3a727afc915777cee54ad3
bitstream.checksumAlgorithm.fl_str_mv MD5
MD5
MD5
MD5
MD5
repository.name.fl_str_mv Repositório Institucional da UFRN - Universidade Federal do Rio Grande do Norte (UFRN)
repository.mail.fl_str_mv
_version_ 1802117497376210944