Análises bromatológicas e fitoquímicas de frutos de Licania tomentosa (Benth) FRITSCH

Detalhes bibliográficos
Autor(a) principal: Teixeira, Luciane de Lira
Data de Publicação: 2012
Tipo de documento: Dissertação
Idioma: por
Título da fonte: Repositório Institucional da UFRN
Texto Completo: https://repositorio.ufrn.br/jspui/handle/123456789/17695
Resumo: This study conducted chemical analyzes of the fruits of Licania tomentosa Benth belonging to the Chrysobalanaceae family, order and superorder Rosiflorae Rosales. Samples were collected in February 2011 in the city of Natal - RN. The fruits were separated into peel, pulp and seed, and the samples were analyzed on moisture and ash by thermogravimetric methods, reducing and total sugars, lipids by Soxhlet extraction, minerals by ICP / OES and other analyzes by physical measurements of the fruit. The fruits for the analysis of determination of flavonoids and phenolic compounds were dried at 40 ° C and ground. For the analyzes to determine the content of phenolics and flavonols was used spectroscopy in the visible region, and also performed the characterization of ethanol extracts by high performance liquid chromatography and test for antioxidant activity hydroethanolic extracts. The results obtained are about 83.9% of the fruits have a length between 4.0 to 6.0 cm with respect to the diameter of the fruit about 97.4% of the fruits have a diameter between 2.0 - 4, 0 cm, mean weight of 36.14 g (7.86), the bark showed 60.5 (1.5)% relative humidity, the flesh 72.3 (0.9) and 44.4 seeds (0.4 )%, the bark showed 0.22 (0.00)% ash, the pulp 1.41 (0.01)% and the seed 1.18 (0.01)%, the bark showed 3.73 (0, 09) mg lipids / 100 g sample of the pulp 0.40 (0.04) and the seed 0.05 (0.00). With respect to reducing sugars and total gave the results, 16.23 (0.23) g/100g and 20.70 (0.24) g/100g. The fruit is presented with a good source of nutrients especially carbohydrates and lipids. The analysis for determining the antioxidant activity tests were performed reducing power and antioxidant capacity, the antioxidant capacity of hydroethanolic extracts of peel and pulp showed similar results, with higher concentrations however hydroethanolic bark extract. Regarding the content of phenolics and flavonoids hidroetanílico bark extract showed higher concentration values. The characterization of the extracts by high performance liquid chromatography identified the following compounds by retention time indicated by the race of the standards: galic acid, kaempferol and kaempferol derivatives. Considering the results of the fruit Licania tomentosa Benth may be an alternative food by analysis of their nutritional content and has substances with antioxidant action
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spelling Teixeira, Luciane de Lirahttp://lattes.cnpq.br/0076797197805817http://lattes.cnpq.br/2959800336802498Assis, Cristiane Fernandes dehttp://lattes.cnpq.br/0034694007210837Silva, Djalma Ribeiro dahttp://lattes.cnpq.br/2791074318745945Moita, Graziella Ciaramellahttp://lattes.cnpq.br/6123729636062436Moura, Maria de Fátima Vitória de2014-12-17T15:42:04Z2013-07-242014-12-17T15:42:04Z2012-03-22TEIXEIRA, Luciane de Lira. Análises bromatológicas e fitoquímicas de frutos de Licania tomentosa (Benth) FRITSCH. 2012. 108 f. Dissertação (Mestrado em Físico-Química; Química) - Universidade Federal do Rio Grande do Norte, Natal, 2012.https://repositorio.ufrn.br/jspui/handle/123456789/17695This study conducted chemical analyzes of the fruits of Licania tomentosa Benth belonging to the Chrysobalanaceae family, order and superorder Rosiflorae Rosales. Samples were collected in February 2011 in the city of Natal - RN. The fruits were separated into peel, pulp and seed, and the samples were analyzed on moisture and ash by thermogravimetric methods, reducing and total sugars, lipids by Soxhlet extraction, minerals by ICP / OES and other analyzes by physical measurements of the fruit. The fruits for the analysis of determination of flavonoids and phenolic compounds were dried at 40 ° C and ground. For the analyzes to determine the content of phenolics and flavonols was used spectroscopy in the visible region, and also performed the characterization of ethanol extracts by high performance liquid chromatography and test for antioxidant activity hydroethanolic extracts. The results obtained are about 83.9% of the fruits have a length between 4.0 to 6.0 cm with respect to the diameter of the fruit about 97.4% of the fruits have a diameter between 2.0 - 4, 0 cm, mean weight of 36.14 g (7.86), the bark showed 60.5 (1.5)% relative humidity, the flesh 72.3 (0.9) and 44.4 seeds (0.4 )%, the bark showed 0.22 (0.00)% ash, the pulp 1.41 (0.01)% and the seed 1.18 (0.01)%, the bark showed 3.73 (0, 09) mg lipids / 100 g sample of the pulp 0.40 (0.04) and the seed 0.05 (0.00). With respect to reducing sugars and total gave the results, 16.23 (0.23) g/100g and 20.70 (0.24) g/100g. The fruit is presented with a good source of nutrients especially carbohydrates and lipids. The analysis for determining the antioxidant activity tests were performed reducing power and antioxidant capacity, the antioxidant capacity of hydroethanolic extracts of peel and pulp showed similar results, with higher concentrations however hydroethanolic bark extract. Regarding the content of phenolics and flavonoids hidroetanílico bark extract showed higher concentration values. The characterization of the extracts by high performance liquid chromatography identified the following compounds by retention time indicated by the race of the standards: galic acid, kaempferol and kaempferol derivatives. Considering the results of the fruit Licania tomentosa Benth may be an alternative food by analysis of their nutritional content and has substances with antioxidant actionO presente trabalho realizou das análises bromatológicas com os frutos da Licania tomentosa Benth que pertence à família Chrysobalanaceae, ordem Rosales e superordem Rosiflorae. As amostras foram coletadas no mês de fevereiro de 2011 no município de Natal RN. Os frutos foram fracionados em casca, polpa e semente, e com as amostras foram realizadas as determinações de umidade e cinzas por métodos termogravimétricos, açúcares redutores e totais, lipídeos por extração com Soxhlet, minerais por ICP/OES e demais análises por medições físicas dos frutos. Os frutos destinados as análises de determinação do teor de flavonóides e fenólicos totais foram secos a 40ºC e triturados. Para as análises de determinação do teor de fenólicos e flavonóis totais se utilizou a espectroscopia na região do visível, sendo também realizada a caracterização dos extratos etanólicos por cromatografia líquida de alta eficiência e teste de atividade antioxidante para os extratos hidroetanólicos. Como resultados obteve-se cerca de 83,9% dos frutos apresentaram comprimento entre 4,0 6,0 cm, com relação à determinação do diâmetro dos frutos cerca de 97,4 % dos frutos apresentaram diâmetro entre 2,0 4,0 cm, peso médio de 36,14 (7,86) g, a casca apresentou 60,5 (1,5)% de umidade, a polpa 72,3 (0,9) e a semente 44,4 (0,4)%, a casca apresentou 0,22 (0,00) % de cinzas, a polpa 1,41(0,01)% e a semente 1,18(0,01)%, a casca apresentou 3,73 (0,09)mg de lipídeos/ 100 g de amostra, a polpa 0,40(0,04) e a semente 0,05(0,00). Com relação aos teores de açúcares redutores e totais obteve-se os respectivos resultados, 16,23 (0,23) g/100g e 20,70(0,24) g/100g. O fruto se apresenta com uma boa fonte de nutrientes principalmente carboidratos e lipídeos. As análises de determinação da atividade antioxidante realizadas foram os testes de poder redutor e capacidade antioxidante, a capacidade antioxidante dos extratos hidroetanólicos da casca e da polpa apresentaram resultados semelhantes, sendo entretanto superior as concentrações do extrato hidroetanólico da casca. Com relação ao teor de fenólicos e flavonóides totais o extrato hidroetanílico da casca apresentou valores de concentração superiores. Na caracterização dos extratos por cromatografia líquida de alta eficiência foram identificados os seguintes compostos por meio do tempo de retenção indicado pela corrida dos padrões: ácido gálico, campferol e derivados. Diante dos resultados o fruto da Licania tomentosa Benth pode ser uma alternativa de alimento mediante a análise de seu conteúdo nutricional e por possuir substâncias com ação antioxidanteCoordenação de Aperfeiçoamento de Pessoal de Nível Superiorapplication/pdfporUniversidade Federal do Rio Grande do NortePrograma de Pós-Graduação em QuímicaUFRNBRFísico-Química; QuímicaLicania. Oiti. AntioxidanteLicania. Oiti. AntioxidantCNPQ::CIENCIAS EXATAS E DA TERRA::QUIMICAAnálises bromatológicas e fitoquímicas de frutos de Licania tomentosa (Benth) FRITSCHinfo:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/masterThesisinfo:eu-repo/semantics/openAccessreponame:Repositório Institucional da UFRNinstname:Universidade Federal do Rio Grande do Norte (UFRN)instacron:UFRNORIGINALLucianeLT_DISSERT.pdfapplication/pdf3099685https://repositorio.ufrn.br/bitstream/123456789/17695/1/LucianeLT_DISSERT.pdfcf9ca201e507efce1126bfa70e5a1f3bMD51TEXTLucianeLT_DISSERT.pdf.txtLucianeLT_DISSERT.pdf.txtExtracted texttext/plain143136https://repositorio.ufrn.br/bitstream/123456789/17695/6/LucianeLT_DISSERT.pdf.txtba77a23697b5c7c75825563c78ab0dd4MD56THUMBNAILLucianeLT_DISSERT.pdf.jpgLucianeLT_DISSERT.pdf.jpgIM Thumbnailimage/jpeg5216https://repositorio.ufrn.br/bitstream/123456789/17695/7/LucianeLT_DISSERT.pdf.jpg234cf2ccfe935436e7fad8a1faf39006MD57123456789/176952017-11-04 14:04:56.695oai:https://repositorio.ufrn.br:123456789/17695Repositório de PublicaçõesPUBhttp://repositorio.ufrn.br/oai/opendoar:2017-11-04T17:04:56Repositório Institucional da UFRN - Universidade Federal do Rio Grande do Norte (UFRN)false
dc.title.por.fl_str_mv Análises bromatológicas e fitoquímicas de frutos de Licania tomentosa (Benth) FRITSCH
title Análises bromatológicas e fitoquímicas de frutos de Licania tomentosa (Benth) FRITSCH
spellingShingle Análises bromatológicas e fitoquímicas de frutos de Licania tomentosa (Benth) FRITSCH
Teixeira, Luciane de Lira
Licania. Oiti. Antioxidante
Licania. Oiti. Antioxidant
CNPQ::CIENCIAS EXATAS E DA TERRA::QUIMICA
title_short Análises bromatológicas e fitoquímicas de frutos de Licania tomentosa (Benth) FRITSCH
title_full Análises bromatológicas e fitoquímicas de frutos de Licania tomentosa (Benth) FRITSCH
title_fullStr Análises bromatológicas e fitoquímicas de frutos de Licania tomentosa (Benth) FRITSCH
title_full_unstemmed Análises bromatológicas e fitoquímicas de frutos de Licania tomentosa (Benth) FRITSCH
title_sort Análises bromatológicas e fitoquímicas de frutos de Licania tomentosa (Benth) FRITSCH
author Teixeira, Luciane de Lira
author_facet Teixeira, Luciane de Lira
author_role author
dc.contributor.authorID.por.fl_str_mv
dc.contributor.authorLattes.por.fl_str_mv http://lattes.cnpq.br/0076797197805817
dc.contributor.advisorID.por.fl_str_mv
dc.contributor.advisorLattes.por.fl_str_mv http://lattes.cnpq.br/2959800336802498
dc.contributor.referees1.pt_BR.fl_str_mv Assis, Cristiane Fernandes de
dc.contributor.referees1ID.por.fl_str_mv
dc.contributor.referees1Lattes.por.fl_str_mv http://lattes.cnpq.br/0034694007210837
dc.contributor.referees2.pt_BR.fl_str_mv Silva, Djalma Ribeiro da
dc.contributor.referees2ID.por.fl_str_mv
dc.contributor.referees2Lattes.por.fl_str_mv http://lattes.cnpq.br/2791074318745945
dc.contributor.referees3.pt_BR.fl_str_mv Moita, Graziella Ciaramella
dc.contributor.referees3ID.por.fl_str_mv
dc.contributor.referees3Lattes.por.fl_str_mv http://lattes.cnpq.br/6123729636062436
dc.contributor.author.fl_str_mv Teixeira, Luciane de Lira
dc.contributor.advisor1.fl_str_mv Moura, Maria de Fátima Vitória de
contributor_str_mv Moura, Maria de Fátima Vitória de
dc.subject.por.fl_str_mv Licania. Oiti. Antioxidante
topic Licania. Oiti. Antioxidante
Licania. Oiti. Antioxidant
CNPQ::CIENCIAS EXATAS E DA TERRA::QUIMICA
dc.subject.eng.fl_str_mv Licania. Oiti. Antioxidant
dc.subject.cnpq.fl_str_mv CNPQ::CIENCIAS EXATAS E DA TERRA::QUIMICA
description This study conducted chemical analyzes of the fruits of Licania tomentosa Benth belonging to the Chrysobalanaceae family, order and superorder Rosiflorae Rosales. Samples were collected in February 2011 in the city of Natal - RN. The fruits were separated into peel, pulp and seed, and the samples were analyzed on moisture and ash by thermogravimetric methods, reducing and total sugars, lipids by Soxhlet extraction, minerals by ICP / OES and other analyzes by physical measurements of the fruit. The fruits for the analysis of determination of flavonoids and phenolic compounds were dried at 40 ° C and ground. For the analyzes to determine the content of phenolics and flavonols was used spectroscopy in the visible region, and also performed the characterization of ethanol extracts by high performance liquid chromatography and test for antioxidant activity hydroethanolic extracts. The results obtained are about 83.9% of the fruits have a length between 4.0 to 6.0 cm with respect to the diameter of the fruit about 97.4% of the fruits have a diameter between 2.0 - 4, 0 cm, mean weight of 36.14 g (7.86), the bark showed 60.5 (1.5)% relative humidity, the flesh 72.3 (0.9) and 44.4 seeds (0.4 )%, the bark showed 0.22 (0.00)% ash, the pulp 1.41 (0.01)% and the seed 1.18 (0.01)%, the bark showed 3.73 (0, 09) mg lipids / 100 g sample of the pulp 0.40 (0.04) and the seed 0.05 (0.00). With respect to reducing sugars and total gave the results, 16.23 (0.23) g/100g and 20.70 (0.24) g/100g. The fruit is presented with a good source of nutrients especially carbohydrates and lipids. The analysis for determining the antioxidant activity tests were performed reducing power and antioxidant capacity, the antioxidant capacity of hydroethanolic extracts of peel and pulp showed similar results, with higher concentrations however hydroethanolic bark extract. Regarding the content of phenolics and flavonoids hidroetanílico bark extract showed higher concentration values. The characterization of the extracts by high performance liquid chromatography identified the following compounds by retention time indicated by the race of the standards: galic acid, kaempferol and kaempferol derivatives. Considering the results of the fruit Licania tomentosa Benth may be an alternative food by analysis of their nutritional content and has substances with antioxidant action
publishDate 2012
dc.date.issued.fl_str_mv 2012-03-22
dc.date.available.fl_str_mv 2013-07-24
2014-12-17T15:42:04Z
dc.date.accessioned.fl_str_mv 2014-12-17T15:42:04Z
dc.type.status.fl_str_mv info:eu-repo/semantics/publishedVersion
dc.type.driver.fl_str_mv info:eu-repo/semantics/masterThesis
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dc.identifier.citation.fl_str_mv TEIXEIRA, Luciane de Lira. Análises bromatológicas e fitoquímicas de frutos de Licania tomentosa (Benth) FRITSCH. 2012. 108 f. Dissertação (Mestrado em Físico-Química; Química) - Universidade Federal do Rio Grande do Norte, Natal, 2012.
dc.identifier.uri.fl_str_mv https://repositorio.ufrn.br/jspui/handle/123456789/17695
identifier_str_mv TEIXEIRA, Luciane de Lira. Análises bromatológicas e fitoquímicas de frutos de Licania tomentosa (Benth) FRITSCH. 2012. 108 f. Dissertação (Mestrado em Físico-Química; Química) - Universidade Federal do Rio Grande do Norte, Natal, 2012.
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