Synthesis of NiCuZn ferrite nanoparticles and microwave absorption characterization
Autor(a) principal: | |
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Data de Publicação: | 2008 |
Outros Autores: | , , , , |
Tipo de documento: | Artigo |
Idioma: | eng |
Título da fonte: | Repositório Institucional da UFRN |
Texto Completo: | https://repositorio.ufrn.br/jspui/handle/123456789/29310 |
Resumo: | This study aimed at the low temperature synthesis of NixCu0.5−xZn0.5Fe2O4 ferrite nanoparticles using the citrate precursor method and the reflectivity characterization of Radar absorbing materials. The NiCuZn phase obtained at 350 °C by the Rietveld method showed homogeneous nanoparticle formation. The analysis of particle size and the critical diameter of the domains indicated monodomain formation on nanometric scale. Vibrating sample magnetometry showed that adding copper to NiZn ferrite decreases magnetization saturation and the calcining temperature. Reflectivity measures taken by the wave guide method, obtained absorption radiation of 96.6% for x = 0.3 at 12 GHz. |
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Araújo, José Humberto deLima, U. R.Nasar, Marinalva CerqueiraNasar, Ricardo SilveiraRezende, M. C.Oliveira, José F.2020-06-19T17:00:33Z2020-06-19T17:00:33Z2008-07-25LIMA, U; NASAR, M; NASAR, R; REZENDE, M; ARAUJO, J; OLIVEIRA, J. Synthesis of NiCuZn ferrite nanoparticles and microwave absorption characterization. Materials Science and Engineering. B, Solid State Materials for Advanced Technology, v. 151, p. 238-242, 2008. Disponível em: https://www.sciencedirect.com/science/article/pii/S0921510708002523?via%3Dihub#! Acesso em: 18 jun 2020. https://doi.org/10.1016/j.mseb.2008.06.032.0921-5107https://repositorio.ufrn.br/jspui/handle/123456789/2931010.1016/j.mseb.2008.06.032ElsevierAttribution 3.0 Brazilhttp://creativecommons.org/licenses/by/3.0/br/info:eu-repo/semantics/openAccessMagnetic materialsChemical synthesisX-ray diffractionElectron microscopyMagnetic propertiesSynthesis of NiCuZn ferrite nanoparticles and microwave absorption characterizationinfo:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/articleThis study aimed at the low temperature synthesis of NixCu0.5−xZn0.5Fe2O4 ferrite nanoparticles using the citrate precursor method and the reflectivity characterization of Radar absorbing materials. The NiCuZn phase obtained at 350 °C by the Rietveld method showed homogeneous nanoparticle formation. The analysis of particle size and the critical diameter of the domains indicated monodomain formation on nanometric scale. Vibrating sample magnetometry showed that adding copper to NiZn ferrite decreases magnetization saturation and the calcining temperature. Reflectivity measures taken by the wave guide method, obtained absorption radiation of 96.6% for x = 0.3 at 12 GHz.engreponame:Repositório Institucional da UFRNinstname:Universidade Federal do Rio Grande do Norte (UFRN)instacron:UFRNTEXTSynthesisofNiCuZnferrit_Araujo_2008.pdf.txtSynthesisofNiCuZnferrit_Araujo_2008.pdf.txtExtracted texttext/plain16574https://repositorio.ufrn.br/bitstream/123456789/29310/4/SynthesisofNiCuZnferrit_Araujo_2008.pdf.txtf5518567f47badc72b4d1ad665cda329MD54THUMBNAILSynthesisofNiCuZnferrit_Araujo_2008.pdf.jpgSynthesisofNiCuZnferrit_Araujo_2008.pdf.jpgGenerated Thumbnailimage/jpeg1690https://repositorio.ufrn.br/bitstream/123456789/29310/5/SynthesisofNiCuZnferrit_Araujo_2008.pdf.jpg332a60e88574dd5940f74b099d231c5bMD55ORIGINALSynthesisofNiCuZnferrit_Araujo_2008.pdfSynthesisofNiCuZnferrit_Araujo_2008.pdfapplication/pdf828144https://repositorio.ufrn.br/bitstream/123456789/29310/1/SynthesisofNiCuZnferrit_Araujo_2008.pdfd0a0dba0e2b54a1bf55495246d49e9c2MD51CC-LICENSElicense_rdflicense_rdfapplication/rdf+xml; charset=utf-8914https://repositorio.ufrn.br/bitstream/123456789/29310/2/license_rdf4d2950bda3d176f570a9f8b328dfbbefMD52LICENSElicense.txtlicense.txttext/plain; charset=utf-81484https://repositorio.ufrn.br/bitstream/123456789/29310/3/license.txte9597aa2854d128fd968be5edc8a28d9MD53123456789/293102020-06-21 04:45:31.449oai:https://repositorio.ufrn.br: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Repositório de PublicaçõesPUBhttp://repositorio.ufrn.br/oai/opendoar:2020-06-21T07:45:31Repositório Institucional da UFRN - Universidade Federal do Rio Grande do Norte (UFRN)false |
dc.title.pt_BR.fl_str_mv |
Synthesis of NiCuZn ferrite nanoparticles and microwave absorption characterization |
title |
Synthesis of NiCuZn ferrite nanoparticles and microwave absorption characterization |
spellingShingle |
Synthesis of NiCuZn ferrite nanoparticles and microwave absorption characterization Araújo, José Humberto de Magnetic materials Chemical synthesis X-ray diffraction Electron microscopy Magnetic properties |
title_short |
Synthesis of NiCuZn ferrite nanoparticles and microwave absorption characterization |
title_full |
Synthesis of NiCuZn ferrite nanoparticles and microwave absorption characterization |
title_fullStr |
Synthesis of NiCuZn ferrite nanoparticles and microwave absorption characterization |
title_full_unstemmed |
Synthesis of NiCuZn ferrite nanoparticles and microwave absorption characterization |
title_sort |
Synthesis of NiCuZn ferrite nanoparticles and microwave absorption characterization |
author |
Araújo, José Humberto de |
author_facet |
Araújo, José Humberto de Lima, U. R. Nasar, Marinalva Cerqueira Nasar, Ricardo Silveira Rezende, M. C. Oliveira, José F. |
author_role |
author |
author2 |
Lima, U. R. Nasar, Marinalva Cerqueira Nasar, Ricardo Silveira Rezende, M. C. Oliveira, José F. |
author2_role |
author author author author author |
dc.contributor.author.fl_str_mv |
Araújo, José Humberto de Lima, U. R. Nasar, Marinalva Cerqueira Nasar, Ricardo Silveira Rezende, M. C. Oliveira, José F. |
dc.subject.por.fl_str_mv |
Magnetic materials Chemical synthesis X-ray diffraction Electron microscopy Magnetic properties |
topic |
Magnetic materials Chemical synthesis X-ray diffraction Electron microscopy Magnetic properties |
description |
This study aimed at the low temperature synthesis of NixCu0.5−xZn0.5Fe2O4 ferrite nanoparticles using the citrate precursor method and the reflectivity characterization of Radar absorbing materials. The NiCuZn phase obtained at 350 °C by the Rietveld method showed homogeneous nanoparticle formation. The analysis of particle size and the critical diameter of the domains indicated monodomain formation on nanometric scale. Vibrating sample magnetometry showed that adding copper to NiZn ferrite decreases magnetization saturation and the calcining temperature. Reflectivity measures taken by the wave guide method, obtained absorption radiation of 96.6% for x = 0.3 at 12 GHz. |
publishDate |
2008 |
dc.date.issued.fl_str_mv |
2008-07-25 |
dc.date.accessioned.fl_str_mv |
2020-06-19T17:00:33Z |
dc.date.available.fl_str_mv |
2020-06-19T17:00:33Z |
dc.type.status.fl_str_mv |
info:eu-repo/semantics/publishedVersion |
dc.type.driver.fl_str_mv |
info:eu-repo/semantics/article |
format |
article |
status_str |
publishedVersion |
dc.identifier.citation.fl_str_mv |
LIMA, U; NASAR, M; NASAR, R; REZENDE, M; ARAUJO, J; OLIVEIRA, J. Synthesis of NiCuZn ferrite nanoparticles and microwave absorption characterization. Materials Science and Engineering. B, Solid State Materials for Advanced Technology, v. 151, p. 238-242, 2008. Disponível em: https://www.sciencedirect.com/science/article/pii/S0921510708002523?via%3Dihub#! Acesso em: 18 jun 2020. https://doi.org/10.1016/j.mseb.2008.06.032. |
dc.identifier.uri.fl_str_mv |
https://repositorio.ufrn.br/jspui/handle/123456789/29310 |
dc.identifier.issn.none.fl_str_mv |
0921-5107 |
dc.identifier.doi.none.fl_str_mv |
10.1016/j.mseb.2008.06.032 |
identifier_str_mv |
LIMA, U; NASAR, M; NASAR, R; REZENDE, M; ARAUJO, J; OLIVEIRA, J. Synthesis of NiCuZn ferrite nanoparticles and microwave absorption characterization. Materials Science and Engineering. B, Solid State Materials for Advanced Technology, v. 151, p. 238-242, 2008. Disponível em: https://www.sciencedirect.com/science/article/pii/S0921510708002523?via%3Dihub#! Acesso em: 18 jun 2020. https://doi.org/10.1016/j.mseb.2008.06.032. 0921-5107 10.1016/j.mseb.2008.06.032 |
url |
https://repositorio.ufrn.br/jspui/handle/123456789/29310 |
dc.language.iso.fl_str_mv |
eng |
language |
eng |
dc.rights.driver.fl_str_mv |
Attribution 3.0 Brazil http://creativecommons.org/licenses/by/3.0/br/ info:eu-repo/semantics/openAccess |
rights_invalid_str_mv |
Attribution 3.0 Brazil http://creativecommons.org/licenses/by/3.0/br/ |
eu_rights_str_mv |
openAccess |
dc.publisher.none.fl_str_mv |
Elsevier |
publisher.none.fl_str_mv |
Elsevier |
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reponame:Repositório Institucional da UFRN instname:Universidade Federal do Rio Grande do Norte (UFRN) instacron:UFRN |
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Universidade Federal do Rio Grande do Norte (UFRN) |
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UFRN |
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Repositório Institucional da UFRN |
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