Synthesis and characterization of Co2+ and Mn2+ Codoped ZnO nanoparticles obtained by the sonochemical method: photocatalytic and antimicrobial properties
Autor(a) principal: | |
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Data de Publicação: | 2019 |
Outros Autores: | , , |
Tipo de documento: | Artigo |
Idioma: | eng |
Título da fonte: | Repositório Institucional da UFRN |
Texto Completo: | https://repositorio.ufrn.br/handle/123456789/43747 |
Resumo: | Nanoparticles of Co2+ and Mn2+ codoped ZnO have been obtained by the sonochemical method. The nanoparticles were characterized by x-ray diffraction, scanning electron microscopy, ultraviolet–visible spectroscopy, N2 adsorption by the Brunauer–Emmett–Teller method and electrical measurements by current–voltage curves. The photocatalytic property was analyzed against the methylene blue (MB) dye and the antimicrobial properties were estimated against the Staphylococcus aureus (Gram-positive) and Escherichia coli (Gram-negative) bacteria by the disc diffusion method. The results indicate that ZnO powders were obtained without the formation of secondary phases, with initial nanoplate morphology, which is lost with doping. The codoped sample had a five-fold higher electrical response, reduced the MB dye concentration by 10% and increased the inhibition halo by 3 cm and 4 cm against S. aureus and E. coli, respectively, compared to bare ZnO |
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Andrade Neto, Nivaldo Freire deOliveira, Y. G.Delmonte, Maurício Roberto BomioMotta, Fabiana Villela da2021-10-08T17:32:09Z2021-10-08T17:32:09Z2019-06-18ANDRADE NETO, N. F.; OLIVEIRA, Y. G.; BOMIO, M. R. D.; MOTTA, F. V.. Synthesis and Characterization of Co2+ and Mn2+ Codoped ZnO Nanoparticles Obtained by the Sonochemical Method: photocatalytic and antimicrobial properties. Journal of Electronic Materials, [S.L.], v. 48, n. 9, p. 5900-5905, 18 jun. 2019. Disponível em: https://link.springer.com/article/10.1007%2Fs11664-019-07367-4. Acesso em: 22 abr. 2021. http://dx.doi.org/10.1007/s11664-019-07367-4.1543-186X0361-5235https://repositorio.ufrn.br/handle/123456789/4374710.1007/s11664-019-07367-4SpringerAttribution 3.0 Brazilhttp://creativecommons.org/licenses/by/3.0/br/info:eu-repo/semantics/openAccessSonochemical methodCo2+ and Mn2+ codoped ZnOPhotocatalytic propertiesAntimicrobial activitySynthesis and characterization of Co2+ and Mn2+ Codoped ZnO nanoparticles obtained by the sonochemical method: photocatalytic and antimicrobial propertiesinfo:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/articleNanoparticles of Co2+ and Mn2+ codoped ZnO have been obtained by the sonochemical method. The nanoparticles were characterized by x-ray diffraction, scanning electron microscopy, ultraviolet–visible spectroscopy, N2 adsorption by the Brunauer–Emmett–Teller method and electrical measurements by current–voltage curves. The photocatalytic property was analyzed against the methylene blue (MB) dye and the antimicrobial properties were estimated against the Staphylococcus aureus (Gram-positive) and Escherichia coli (Gram-negative) bacteria by the disc diffusion method. The results indicate that ZnO powders were obtained without the formation of secondary phases, with initial nanoplate morphology, which is lost with doping. The codoped sample had a five-fold higher electrical response, reduced the MB dye concentration by 10% and increased the inhibition halo by 3 cm and 4 cm against S. aureus and E. coli, respectively, compared to bare ZnOengreponame:Repositório Institucional da UFRNinstname:Universidade Federal do Rio Grande do Norte (UFRN)instacron:UFRNORIGINALSynthesisCharacterizationCo_BOMIO_2019.pdfSynthesisCharacterizationCo_BOMIO_2019.pdfapplication/pdf1028118https://repositorio.ufrn.br/bitstream/123456789/43747/1/SynthesisCharacterizationCo_BOMIO_2019.pdf7041042ddbcc3d320cc5aa297a4449baMD51CC-LICENSElicense_rdflicense_rdfapplication/rdf+xml; charset=utf-8914https://repositorio.ufrn.br/bitstream/123456789/43747/2/license_rdf4d2950bda3d176f570a9f8b328dfbbefMD52LICENSElicense.txtlicense.txttext/plain; charset=utf-81484https://repositorio.ufrn.br/bitstream/123456789/43747/3/license.txte9597aa2854d128fd968be5edc8a28d9MD53123456789/437472021-10-08 14:32:11.834oai:https://repositorio.ufrn.br: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Repositório de PublicaçõesPUBhttp://repositorio.ufrn.br/oai/opendoar:2021-10-08T17:32:11Repositório Institucional da UFRN - Universidade Federal do Rio Grande do Norte (UFRN)false |
dc.title.pt_BR.fl_str_mv |
Synthesis and characterization of Co2+ and Mn2+ Codoped ZnO nanoparticles obtained by the sonochemical method: photocatalytic and antimicrobial properties |
title |
Synthesis and characterization of Co2+ and Mn2+ Codoped ZnO nanoparticles obtained by the sonochemical method: photocatalytic and antimicrobial properties |
spellingShingle |
Synthesis and characterization of Co2+ and Mn2+ Codoped ZnO nanoparticles obtained by the sonochemical method: photocatalytic and antimicrobial properties Andrade Neto, Nivaldo Freire de Sonochemical method Co2+ and Mn2+ codoped ZnO Photocatalytic properties Antimicrobial activity |
title_short |
Synthesis and characterization of Co2+ and Mn2+ Codoped ZnO nanoparticles obtained by the sonochemical method: photocatalytic and antimicrobial properties |
title_full |
Synthesis and characterization of Co2+ and Mn2+ Codoped ZnO nanoparticles obtained by the sonochemical method: photocatalytic and antimicrobial properties |
title_fullStr |
Synthesis and characterization of Co2+ and Mn2+ Codoped ZnO nanoparticles obtained by the sonochemical method: photocatalytic and antimicrobial properties |
title_full_unstemmed |
Synthesis and characterization of Co2+ and Mn2+ Codoped ZnO nanoparticles obtained by the sonochemical method: photocatalytic and antimicrobial properties |
title_sort |
Synthesis and characterization of Co2+ and Mn2+ Codoped ZnO nanoparticles obtained by the sonochemical method: photocatalytic and antimicrobial properties |
author |
Andrade Neto, Nivaldo Freire de |
author_facet |
Andrade Neto, Nivaldo Freire de Oliveira, Y. G. Delmonte, Maurício Roberto Bomio Motta, Fabiana Villela da |
author_role |
author |
author2 |
Oliveira, Y. G. Delmonte, Maurício Roberto Bomio Motta, Fabiana Villela da |
author2_role |
author author author |
dc.contributor.author.fl_str_mv |
Andrade Neto, Nivaldo Freire de Oliveira, Y. G. Delmonte, Maurício Roberto Bomio Motta, Fabiana Villela da |
dc.subject.por.fl_str_mv |
Sonochemical method Co2+ and Mn2+ codoped ZnO Photocatalytic properties Antimicrobial activity |
topic |
Sonochemical method Co2+ and Mn2+ codoped ZnO Photocatalytic properties Antimicrobial activity |
description |
Nanoparticles of Co2+ and Mn2+ codoped ZnO have been obtained by the sonochemical method. The nanoparticles were characterized by x-ray diffraction, scanning electron microscopy, ultraviolet–visible spectroscopy, N2 adsorption by the Brunauer–Emmett–Teller method and electrical measurements by current–voltage curves. The photocatalytic property was analyzed against the methylene blue (MB) dye and the antimicrobial properties were estimated against the Staphylococcus aureus (Gram-positive) and Escherichia coli (Gram-negative) bacteria by the disc diffusion method. The results indicate that ZnO powders were obtained without the formation of secondary phases, with initial nanoplate morphology, which is lost with doping. The codoped sample had a five-fold higher electrical response, reduced the MB dye concentration by 10% and increased the inhibition halo by 3 cm and 4 cm against S. aureus and E. coli, respectively, compared to bare ZnO |
publishDate |
2019 |
dc.date.issued.fl_str_mv |
2019-06-18 |
dc.date.accessioned.fl_str_mv |
2021-10-08T17:32:09Z |
dc.date.available.fl_str_mv |
2021-10-08T17:32:09Z |
dc.type.status.fl_str_mv |
info:eu-repo/semantics/publishedVersion |
dc.type.driver.fl_str_mv |
info:eu-repo/semantics/article |
format |
article |
status_str |
publishedVersion |
dc.identifier.citation.fl_str_mv |
ANDRADE NETO, N. F.; OLIVEIRA, Y. G.; BOMIO, M. R. D.; MOTTA, F. V.. Synthesis and Characterization of Co2+ and Mn2+ Codoped ZnO Nanoparticles Obtained by the Sonochemical Method: photocatalytic and antimicrobial properties. Journal of Electronic Materials, [S.L.], v. 48, n. 9, p. 5900-5905, 18 jun. 2019. Disponível em: https://link.springer.com/article/10.1007%2Fs11664-019-07367-4. Acesso em: 22 abr. 2021. http://dx.doi.org/10.1007/s11664-019-07367-4. |
dc.identifier.uri.fl_str_mv |
https://repositorio.ufrn.br/handle/123456789/43747 |
dc.identifier.issn.none.fl_str_mv |
1543-186X 0361-5235 |
dc.identifier.doi.none.fl_str_mv |
10.1007/s11664-019-07367-4 |
identifier_str_mv |
ANDRADE NETO, N. F.; OLIVEIRA, Y. G.; BOMIO, M. R. D.; MOTTA, F. V.. Synthesis and Characterization of Co2+ and Mn2+ Codoped ZnO Nanoparticles Obtained by the Sonochemical Method: photocatalytic and antimicrobial properties. Journal of Electronic Materials, [S.L.], v. 48, n. 9, p. 5900-5905, 18 jun. 2019. Disponível em: https://link.springer.com/article/10.1007%2Fs11664-019-07367-4. Acesso em: 22 abr. 2021. http://dx.doi.org/10.1007/s11664-019-07367-4. 1543-186X 0361-5235 10.1007/s11664-019-07367-4 |
url |
https://repositorio.ufrn.br/handle/123456789/43747 |
dc.language.iso.fl_str_mv |
eng |
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eng |
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Attribution 3.0 Brazil http://creativecommons.org/licenses/by/3.0/br/ info:eu-repo/semantics/openAccess |
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Attribution 3.0 Brazil http://creativecommons.org/licenses/by/3.0/br/ |
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openAccess |
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Springer |
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Springer |
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