Avaliação das propriedades mecânicas e microestrutura de concreto de ultra alto desempenho com adições minerais e resíduos industriais

Detalhes bibliográficos
Autor(a) principal: Sokolovicz, Bóris Casanova
Data de Publicação: 2020
Tipo de documento: Tese
Idioma: por
Título da fonte: Manancial - Repositório Digital da UFSM
dARK ID: ark:/26339/001300001165s
Texto Completo: http://repositorio.ufsm.br/handle/1/19866
Resumo: With the increase in the world population, civil construction is the largest consumer of resources, with great environmental impact. One of the ways to reduce this impact is to increase the mechanical strength of the concrete, reducing the resistant sections of the structural parts, dematerializing them from the emanation of greenhouse gases. The use of industrial and pozzolan waste in concrete, in addition to the packaging of particles, are concrete actions that reduce environmental impacts, increasing sustainability. Thus, the general objective of this research was to analyze the microstructure and physical-mechanical properties of ultra high performance concrete (UHPC) with hydrated lime, foundry sand, pozzolanic and inert mineral additions, through the packaging effects of the particles. The specific objectives were: to evaluate the workability of UHPC with rice husk ash (RHA), fly ash (FA), lime CH I, limestone filler (LF), quartz powder and foundry sand, in relation to the reference concrete, with structural white cement, silica fume (SF), quartz powder and sand industrial; study the packaging of particles by the modified Andreassen method; analyze the performance of variables related to the mechanical strength of concrete in wet and thermal cures: axial compression, modulus of elasticity and instrumented breaks; and analyze the microstructure of UHPC mixtures by: X-Ray Diffraction (XRD), Thermogravimetric Analysis (TG/DTG), Fourier Transform Infrared (FTIR) and Scanning Electron Microscopy (SEM/EDS). The greatest resistance for all ages was the REF mixture. The efficiency of thermal curing was verified, mainly in early ages, with emphasis on the mixture with 15% partial replacement of cement with rice husk ash (RHA15). For mixtures with mineral additions, the similar behavior was noticeable. This performance confirms that the physical effect was representative, because, even with changes in levels and types of mineral additions, the average clinker intensity did not vary significantly. The elasticity modules showed the same trend of resistance behavior. In instrumented breaks, the stresses were proportional to the specific deformations in almost the entire test. In mixtures with mineral additions (RHA15, FA15, RHA10-FA5 and RHA10-LF5), the deformations were greater, attesting to the less fragile behavior. In XRD, the presence of non-hydrated compounds (alite and belite) was observed due to the low a / mc ratio. In mixtures with the addition of lime there was an increase in the peaks of portlandite and calcite, showing that a portion of the lime did not react with the pozzolana. In TG-DTG, mixtures with mineral additions had higher levels of combined water, calcium hydroxide (CH) and carbonates than REF, attesting that the lime partially reacted with the pozzolan. In FTIR, the REF mixture showed low peaks of portlandite, the opposite behavior of mixtures with mineral additions. In SEM, it was found that mixtures with mineral additions showed higher levels of Ca / Si ratio when compared to the reference concrete.
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spelling Avaliação das propriedades mecânicas e microestrutura de concreto de ultra alto desempenho com adições minerais e resíduos industriaisEvaluation of mechanical properties and microstructure of ultra high performance concrete with mineral additions and industrial wasteConcreto de ultra alto desempenhoPropriedades mecânicasMicroestruturaSustentabilidadePozolanasEmpacotamento de partículasMicrostructureUltra high performance concreteMechanical propertiesSustainabilityPozzolansParticles packingCNPQ::ENGENHARIAS::ENGENHARIA CIVILWith the increase in the world population, civil construction is the largest consumer of resources, with great environmental impact. One of the ways to reduce this impact is to increase the mechanical strength of the concrete, reducing the resistant sections of the structural parts, dematerializing them from the emanation of greenhouse gases. The use of industrial and pozzolan waste in concrete, in addition to the packaging of particles, are concrete actions that reduce environmental impacts, increasing sustainability. Thus, the general objective of this research was to analyze the microstructure and physical-mechanical properties of ultra high performance concrete (UHPC) with hydrated lime, foundry sand, pozzolanic and inert mineral additions, through the packaging effects of the particles. The specific objectives were: to evaluate the workability of UHPC with rice husk ash (RHA), fly ash (FA), lime CH I, limestone filler (LF), quartz powder and foundry sand, in relation to the reference concrete, with structural white cement, silica fume (SF), quartz powder and sand industrial; study the packaging of particles by the modified Andreassen method; analyze the performance of variables related to the mechanical strength of concrete in wet and thermal cures: axial compression, modulus of elasticity and instrumented breaks; and analyze the microstructure of UHPC mixtures by: X-Ray Diffraction (XRD), Thermogravimetric Analysis (TG/DTG), Fourier Transform Infrared (FTIR) and Scanning Electron Microscopy (SEM/EDS). The greatest resistance for all ages was the REF mixture. The efficiency of thermal curing was verified, mainly in early ages, with emphasis on the mixture with 15% partial replacement of cement with rice husk ash (RHA15). For mixtures with mineral additions, the similar behavior was noticeable. This performance confirms that the physical effect was representative, because, even with changes in levels and types of mineral additions, the average clinker intensity did not vary significantly. The elasticity modules showed the same trend of resistance behavior. In instrumented breaks, the stresses were proportional to the specific deformations in almost the entire test. In mixtures with mineral additions (RHA15, FA15, RHA10-FA5 and RHA10-LF5), the deformations were greater, attesting to the less fragile behavior. In XRD, the presence of non-hydrated compounds (alite and belite) was observed due to the low a / mc ratio. In mixtures with the addition of lime there was an increase in the peaks of portlandite and calcite, showing that a portion of the lime did not react with the pozzolana. In TG-DTG, mixtures with mineral additions had higher levels of combined water, calcium hydroxide (CH) and carbonates than REF, attesting that the lime partially reacted with the pozzolan. In FTIR, the REF mixture showed low peaks of portlandite, the opposite behavior of mixtures with mineral additions. In SEM, it was found that mixtures with mineral additions showed higher levels of Ca / Si ratio when compared to the reference concrete.Com o aumento da população mundial, a construção civil é a maior consumidora de recursos, com grande impacto ambiental. Uma das maneiras de diminuir esse impacto é aumentar a resistência mecânica do concreto, reduzindo as seções resistentes das peças estruturais, desmaterializando-as da emanação dos gases do efeito estufa. A utilização no concreto de resíduos industriais e pozolana, além do empacotamento das partículas, são ações concretas que diminuem os impactos ambientais, aumentando a sustentabilidade. Assim, o objetivo geral desta pesquisa foi analisar a microestrutura e propriedades físico-mecânicas de concreto de ultra alto desempenho (CUAD) com cal hidratada, areia de fundição, adições minerais pozolânicas e inerte, através dos efeitos de empacotamento das partículas. Os objetivos específicos foram: avaliar a trabalhabilidade do CUAD com cinza de casca de arroz (CCA), cinza volante (CV), cal CH I, fíler calcário, pó de quartzo e areia de fundição, em relação ao concreto de referência, com cimento branco estrutural, sílica ativa, pó de quartzo e areia industrial; estudar o empacotamento das partículas pelo método de Andreassen modificado; analisar o desempenho das variáveis relacionadas com a resistência mecânica do concreto em curas úmida e térmica: compressão axial, módulo de elasticidade e rompimentos instrumentados; analisar a microestrutura das misturas do CUAD por: Difração de Raios X (DRX), Análise termogravimétrica (TG/DTG), Infravermelho com transformada de Fourier (FTIR) e Microscopia Eletrônica de Varredura MEV/EDS. As maiores resistências para todas as idades foram da mistura REF. Verificou-se a eficiência da cura térmica, principalmente em idades iniciais, com destaque para a mistura com 15% de substituição parcial de cimento por cinza de casca de arroz (CCA15). Para as misturas com adições minerais, ficou perceptível o comportamento semelhante. Esse desempenho ratifica que o efeito físico foi representativo, pois, mesmo com alterações de teores e de tipos de adições minerais, a intensidade de clínquer média não variou significativamente. Os módulos de elasticidade apresentaram a mesma tendência de comportamento da resistência. Nos rompimentos instrumentados as tensões foram proporcionais às deformações específicas em quase todo o ensaio. Nas misturas com adições minerais (CCA15, CV15, CCA10-CV5 e CCA10-FC5), as deformações foram maiores, atestando o comportamento menos frágil. No DRX, observou-se presença de compostos não hidratados (alita e belita) devido à baixa relação a/mc. Nas misturas com adição de cal houve acréscimo nos picos de portlandita e calcita, evidenciando que uma parcela da cal não reagiu com a pozolana. No TG-DTG as misturas com adições minerais tiveram maiores níveis de água combinada, hidróxido de cálcio (CH) e carbonatos que a REF, atestando que a cal reagiu parcialmente com a pozolana. No FTIR a mistura REF apresentou baixos picos de portlandita, comportamento oposto das misturas com adições minerais. No MEV, verificou-se que as misturas com adições minerais apresentaram níveis mais elevados de relação Ca/Si quando comparados ao concreto referência.Universidade Federal de Santa MariaBrasilEngenharia CivilUFSMPrograma de Pós-Graduação em Engenharia CivilCentro de TecnologiaIsaia, Geraldo Cechellahttp://lattes.cnpq.br/8260652949733370Tutikian, Bernardo Fonsecahttp://lattes.cnpq.br/9916860252080305Hoppe Filho, Juarezhttp://lattes.cnpq.br/8692521256968834Vargas, Alexandre Silva dehttp://lattes.cnpq.br/6501148372644975Lübeck, Andréhttp://lattes.cnpq.br/7511022637484145Sokolovicz, Bóris Casanova2020-05-15T16:18:15Z2020-05-15T16:18:15Z2020-01-07info:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/doctoralThesisapplication/pdfhttp://repositorio.ufsm.br/handle/1/19866ark:/26339/001300001165sporAttribution-NonCommercial-NoDerivatives 4.0 Internationalhttp://creativecommons.org/licenses/by-nc-nd/4.0/info:eu-repo/semantics/openAccessreponame:Manancial - Repositório Digital da UFSMinstname:Universidade Federal de Santa Maria (UFSM)instacron:UFSM2021-04-26T18:05:20Zoai:repositorio.ufsm.br:1/19866Biblioteca Digital de Teses e Dissertaçõeshttps://repositorio.ufsm.br/ONGhttps://repositorio.ufsm.br/oai/requestatendimento.sib@ufsm.br||tedebc@gmail.comopendoar:2021-04-26T18:05:20Manancial - Repositório Digital da UFSM - Universidade Federal de Santa Maria (UFSM)false
dc.title.none.fl_str_mv Avaliação das propriedades mecânicas e microestrutura de concreto de ultra alto desempenho com adições minerais e resíduos industriais
Evaluation of mechanical properties and microstructure of ultra high performance concrete with mineral additions and industrial waste
title Avaliação das propriedades mecânicas e microestrutura de concreto de ultra alto desempenho com adições minerais e resíduos industriais
spellingShingle Avaliação das propriedades mecânicas e microestrutura de concreto de ultra alto desempenho com adições minerais e resíduos industriais
Sokolovicz, Bóris Casanova
Concreto de ultra alto desempenho
Propriedades mecânicas
Microestrutura
Sustentabilidade
Pozolanas
Empacotamento de partículas
Microstructure
Ultra high performance concrete
Mechanical properties
Sustainability
Pozzolans
Particles packing
CNPQ::ENGENHARIAS::ENGENHARIA CIVIL
title_short Avaliação das propriedades mecânicas e microestrutura de concreto de ultra alto desempenho com adições minerais e resíduos industriais
title_full Avaliação das propriedades mecânicas e microestrutura de concreto de ultra alto desempenho com adições minerais e resíduos industriais
title_fullStr Avaliação das propriedades mecânicas e microestrutura de concreto de ultra alto desempenho com adições minerais e resíduos industriais
title_full_unstemmed Avaliação das propriedades mecânicas e microestrutura de concreto de ultra alto desempenho com adições minerais e resíduos industriais
title_sort Avaliação das propriedades mecânicas e microestrutura de concreto de ultra alto desempenho com adições minerais e resíduos industriais
author Sokolovicz, Bóris Casanova
author_facet Sokolovicz, Bóris Casanova
author_role author
dc.contributor.none.fl_str_mv Isaia, Geraldo Cechella
http://lattes.cnpq.br/8260652949733370
Tutikian, Bernardo Fonseca
http://lattes.cnpq.br/9916860252080305
Hoppe Filho, Juarez
http://lattes.cnpq.br/8692521256968834
Vargas, Alexandre Silva de
http://lattes.cnpq.br/6501148372644975
Lübeck, André
http://lattes.cnpq.br/7511022637484145
dc.contributor.author.fl_str_mv Sokolovicz, Bóris Casanova
dc.subject.por.fl_str_mv Concreto de ultra alto desempenho
Propriedades mecânicas
Microestrutura
Sustentabilidade
Pozolanas
Empacotamento de partículas
Microstructure
Ultra high performance concrete
Mechanical properties
Sustainability
Pozzolans
Particles packing
CNPQ::ENGENHARIAS::ENGENHARIA CIVIL
topic Concreto de ultra alto desempenho
Propriedades mecânicas
Microestrutura
Sustentabilidade
Pozolanas
Empacotamento de partículas
Microstructure
Ultra high performance concrete
Mechanical properties
Sustainability
Pozzolans
Particles packing
CNPQ::ENGENHARIAS::ENGENHARIA CIVIL
description With the increase in the world population, civil construction is the largest consumer of resources, with great environmental impact. One of the ways to reduce this impact is to increase the mechanical strength of the concrete, reducing the resistant sections of the structural parts, dematerializing them from the emanation of greenhouse gases. The use of industrial and pozzolan waste in concrete, in addition to the packaging of particles, are concrete actions that reduce environmental impacts, increasing sustainability. Thus, the general objective of this research was to analyze the microstructure and physical-mechanical properties of ultra high performance concrete (UHPC) with hydrated lime, foundry sand, pozzolanic and inert mineral additions, through the packaging effects of the particles. The specific objectives were: to evaluate the workability of UHPC with rice husk ash (RHA), fly ash (FA), lime CH I, limestone filler (LF), quartz powder and foundry sand, in relation to the reference concrete, with structural white cement, silica fume (SF), quartz powder and sand industrial; study the packaging of particles by the modified Andreassen method; analyze the performance of variables related to the mechanical strength of concrete in wet and thermal cures: axial compression, modulus of elasticity and instrumented breaks; and analyze the microstructure of UHPC mixtures by: X-Ray Diffraction (XRD), Thermogravimetric Analysis (TG/DTG), Fourier Transform Infrared (FTIR) and Scanning Electron Microscopy (SEM/EDS). The greatest resistance for all ages was the REF mixture. The efficiency of thermal curing was verified, mainly in early ages, with emphasis on the mixture with 15% partial replacement of cement with rice husk ash (RHA15). For mixtures with mineral additions, the similar behavior was noticeable. This performance confirms that the physical effect was representative, because, even with changes in levels and types of mineral additions, the average clinker intensity did not vary significantly. The elasticity modules showed the same trend of resistance behavior. In instrumented breaks, the stresses were proportional to the specific deformations in almost the entire test. In mixtures with mineral additions (RHA15, FA15, RHA10-FA5 and RHA10-LF5), the deformations were greater, attesting to the less fragile behavior. In XRD, the presence of non-hydrated compounds (alite and belite) was observed due to the low a / mc ratio. In mixtures with the addition of lime there was an increase in the peaks of portlandite and calcite, showing that a portion of the lime did not react with the pozzolana. In TG-DTG, mixtures with mineral additions had higher levels of combined water, calcium hydroxide (CH) and carbonates than REF, attesting that the lime partially reacted with the pozzolan. In FTIR, the REF mixture showed low peaks of portlandite, the opposite behavior of mixtures with mineral additions. In SEM, it was found that mixtures with mineral additions showed higher levels of Ca / Si ratio when compared to the reference concrete.
publishDate 2020
dc.date.none.fl_str_mv 2020-05-15T16:18:15Z
2020-05-15T16:18:15Z
2020-01-07
dc.type.status.fl_str_mv info:eu-repo/semantics/publishedVersion
dc.type.driver.fl_str_mv info:eu-repo/semantics/doctoralThesis
format doctoralThesis
status_str publishedVersion
dc.identifier.uri.fl_str_mv http://repositorio.ufsm.br/handle/1/19866
dc.identifier.dark.fl_str_mv ark:/26339/001300001165s
url http://repositorio.ufsm.br/handle/1/19866
identifier_str_mv ark:/26339/001300001165s
dc.language.iso.fl_str_mv por
language por
dc.rights.driver.fl_str_mv Attribution-NonCommercial-NoDerivatives 4.0 International
http://creativecommons.org/licenses/by-nc-nd/4.0/
info:eu-repo/semantics/openAccess
rights_invalid_str_mv Attribution-NonCommercial-NoDerivatives 4.0 International
http://creativecommons.org/licenses/by-nc-nd/4.0/
eu_rights_str_mv openAccess
dc.format.none.fl_str_mv application/pdf
dc.publisher.none.fl_str_mv Universidade Federal de Santa Maria
Brasil
Engenharia Civil
UFSM
Programa de Pós-Graduação em Engenharia Civil
Centro de Tecnologia
publisher.none.fl_str_mv Universidade Federal de Santa Maria
Brasil
Engenharia Civil
UFSM
Programa de Pós-Graduação em Engenharia Civil
Centro de Tecnologia
dc.source.none.fl_str_mv reponame:Manancial - Repositório Digital da UFSM
instname:Universidade Federal de Santa Maria (UFSM)
instacron:UFSM
instname_str Universidade Federal de Santa Maria (UFSM)
instacron_str UFSM
institution UFSM
reponame_str Manancial - Repositório Digital da UFSM
collection Manancial - Repositório Digital da UFSM
repository.name.fl_str_mv Manancial - Repositório Digital da UFSM - Universidade Federal de Santa Maria (UFSM)
repository.mail.fl_str_mv atendimento.sib@ufsm.br||tedebc@gmail.com
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