Caracterização de hidrociclones com cilindros e cones permeáveis

Detalhes bibliográficos
Autor(a) principal: Faria, Érica Victor de
Data de Publicação: 2022
Tipo de documento: Tese
Idioma: por
Título da fonte: Repositório Institucional da UFU
Texto Completo: https://repositorio.ufu.br/handle/123456789/37288
http://doi.org/10.14393/ufu.te.2022.482
Resumo: Published studies on hydrocyclones up to 2022 mostly report their use in the processing of dilute suspensions. However, high concentrations of solids, is more commonly encountered in industrial practices, and the use of hydrocyclones in these cases can result in inefficient separations. Possible changes in the structure of hydrocyclones have been studied to improve the performance of these separators, such as the association of filtration and hydrocycloning operation. The filtering hydrocyclone has a cylindrical wall, conical wall, or both, made of porous material, and has an additional outflow (filtered) for the fluid. Given this context, this experimental study intended to evaluate the performance of optimal geometries of hydrocyclones with filtering cylinders and cones (HCiCoF-OT1 and HCiCoF-OT3, HCoF-OT1 and HCoF-OT3), proposed by Salvador (2017), operating with suspensions with different solids concentrations. For this, an experimental design was developed for each hydrocyclone to evaluate the effects of filtration and three levels of the variables of interest: feed solids concentration (CVA), underflow diameter (DU), and pressure drop (–ΔP). In all cases, it was observed that the energy consumption was reduced for the filtering hydrocyclones; and the increase in the feed solids concentration led to a reduction in the total efficiency. For the hydrocyclones of HCiCoF-OT1 and HCoF-OT1 geometries, the total efficiency was minimized with the increase of CVA and reduction of the variables underflow diameter and pressure drop. The maximum tottal efficiency achieved was 85 % for HCiCoF-OT1 and 86 % for HCoF-OT1 operating with DU of 5 mm, pressure drop of 1.77 bar, and 1.0 %v. of solids in the feed. These hydrocyclones also provided high total efficiencies in suspensions containing 10.0 %v. solids, reaching 79 % (HCiCoF-OT1) and 77 % (HCoF-OT1). The hydrocyclones of HCiCoF-OT3 and HCoF-OT3 geometries showed low split ratios for all concentrations studied. HCiCoF-OT3 presented RL of 0.6 % for the most diluted suspension (CVA = 1.0 %v.), and 4.0 % for the most concentrated (CVA = 10.0 %v.). To these hydrocyclones the split ratio was lower for dilute suspensions, smaller underflow diameters, and conventional equipment; for concentrated suspensions, the filtering equipment presented a better alternative for providing a lower energy consumption and statistically equal RL.
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spelling Caracterização de hidrociclones com cilindros e cones permeáveisCharacterization of hydrocyclones with permeable cylinders and conesSeparação sólido-líquidoFiltraçãoSuspensões concentradasConcentração de sólidosDiâmetro de underflowSolid-liquid separationFiltrationSlurriesSolids concentrationUnderflow diameterCNPQ::ENGENHARIAS::ENGENHARIA QUIMICA::OPERACOES INDUSTRIAIS E EQUIPAMENTOS PARA ENGENHARIA QUIMICA::OPERACOES DE SEPARACAO E MISTURAPublished studies on hydrocyclones up to 2022 mostly report their use in the processing of dilute suspensions. However, high concentrations of solids, is more commonly encountered in industrial practices, and the use of hydrocyclones in these cases can result in inefficient separations. Possible changes in the structure of hydrocyclones have been studied to improve the performance of these separators, such as the association of filtration and hydrocycloning operation. The filtering hydrocyclone has a cylindrical wall, conical wall, or both, made of porous material, and has an additional outflow (filtered) for the fluid. Given this context, this experimental study intended to evaluate the performance of optimal geometries of hydrocyclones with filtering cylinders and cones (HCiCoF-OT1 and HCiCoF-OT3, HCoF-OT1 and HCoF-OT3), proposed by Salvador (2017), operating with suspensions with different solids concentrations. For this, an experimental design was developed for each hydrocyclone to evaluate the effects of filtration and three levels of the variables of interest: feed solids concentration (CVA), underflow diameter (DU), and pressure drop (–ΔP). In all cases, it was observed that the energy consumption was reduced for the filtering hydrocyclones; and the increase in the feed solids concentration led to a reduction in the total efficiency. For the hydrocyclones of HCiCoF-OT1 and HCoF-OT1 geometries, the total efficiency was minimized with the increase of CVA and reduction of the variables underflow diameter and pressure drop. The maximum tottal efficiency achieved was 85 % for HCiCoF-OT1 and 86 % for HCoF-OT1 operating with DU of 5 mm, pressure drop of 1.77 bar, and 1.0 %v. of solids in the feed. These hydrocyclones also provided high total efficiencies in suspensions containing 10.0 %v. solids, reaching 79 % (HCiCoF-OT1) and 77 % (HCoF-OT1). The hydrocyclones of HCiCoF-OT3 and HCoF-OT3 geometries showed low split ratios for all concentrations studied. HCiCoF-OT3 presented RL of 0.6 % for the most diluted suspension (CVA = 1.0 %v.), and 4.0 % for the most concentrated (CVA = 10.0 %v.). To these hydrocyclones the split ratio was lower for dilute suspensions, smaller underflow diameters, and conventional equipment; for concentrated suspensions, the filtering equipment presented a better alternative for providing a lower energy consumption and statistically equal RL.CAPES - Coordenação de Aperfeiçoamento de Pessoal de Nível SuperiorTese (Doutorado)Estudos publicados sobre hidrociclones até o ano de 2022 relatam seu uso majoritariamente no processamento de suspensões diluídas. No entanto, suspensões com altas concentrações de sólidos são mais comumente encontradas em práticas industriais e o uso de hidrociclones nesses casos pode resultar em separações pouco eficientes. Com o propósito de melhorar o desempenho desses separadores, modificações em sua estrutura têm sido estudadas, como a associação da operação de filtração à hidrociclonagem. O hidrociclone filtrante apresenta a parede cilíndrica, cônica ou ambas, constituídas em material poroso, e apresenta uma saída adicional (filtrado) para o fluido. Diante desse contexto, um estudo experimental foi proposto para avaliar o desempenho de geometrias otimizadas de hidrociclones com cilindros e/ou cones filtrantes (HCiCoF-OT1 e HCiCoF-OT3, HCoF-OT1 e HCoF-OT3), sugeridas por Salvador (2017), operando suspensões contendo até 10,0 % de sólidos em volume. Para isso, desenvolveu-se um planejamento experimental para cada equipamento, no qual foram avaliados três níveis das variáveis de interesse: concentração volumétrica de sólidos na alimentação (CVA), diâmetro de underflow (DU) e queda de pressão (–ΔP). Os efeitos da filtração foram estimados através da comparação com equipamentos convencionais (paredes totalmente maciças) de mesma geometria. Em todos os casos observou-se que o consumo energético foi reduzido para os hidrociclones filtrantes; e que o aumento de CVA levou à redução da eficiência total. Para os hidrociclones de geometrias HCiCoF-OT1 e HCoF-OT1 a eficiência total foi maximizada com o aumento dos níveis de DU e –ΔP. Esses equipamentos foram capazes de promover altas eficiências totais de separação, obtendo-se ET = 85 % para HCiCoF-OT1 e ET = 86 % para HCoF-OT1 com o processamento de suspensões diluídas (CVA = 1,0 %v.); e foram alcançadas eficiências de 79 % (HiCoF-OT1) e 77 % (HCoF-OT1) para suspensões concentradas (CVA = 10,0 %v.). Os hidrociclones de geometrias HCiCoF-OT3 e HCoF-OT3 proporcionaram baixas razões de líquido para todas as concentrações estudadas. Sendo que HCiCoF-OT3 apresentou RL de 0,6 % para a suspensão diluída (CVA = 1,0 %v.), e de 4,0 % para a mais concentrada (CVA = 10,0 %), o que ratifica o alto potencial concentrador desses separadores. A razão de líquido nesses equipamentos foi minorada para menores diâmetros de underflow. Para suspensões diluídas, a razão de líquido foi minorada para os hidrociclones convencionais; já para suspensões concentradas os equipamentos filtrantes apresentaram uma melhor alternativa por proporcionar um menor consumo energético e RL estatisticamente iguais.Universidade Federal de UberlândiaBrasilPrograma de Pós-graduação em Engenharia QuímicaBarrozo, Marcos Antonio de Souzahttp://lattes.cnpq.br/7024983341494297Vieira, Luiz Gustavo Martinshttp://lattes.cnpq.br/6266547523604644Bicalho, Isabele Cristinahttp://lattes.cnpq.br/3296524340665201Tanabe, Eduardo Hiromitsuhttp://lattes.cnpq.br/9778700143605069Kyriakidis, Yanne Novaishttp://lattes.cnpq.br/4496520699221094Silva, Danylo de Oliveirahttp://lattes.cnpq.br/8216573686887098Faria, Érica Victor de2023-02-23T18:21:47Z2023-02-23T18:21:47Z2022-08-29info:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/doctoralThesisapplication/pdfFARIA, Érica Victor de. Caracterização de hidrociclones com cilindros e cones permeáveis. 2022. 181 f. Tese (Doutorado em Engenharia Química) - Universidade Federal de Uberlândia, Uberlândia, 2022. DOI http://doi.org/10.14393/ufu.te.2022.482https://repositorio.ufu.br/handle/123456789/37288http://doi.org/10.14393/ufu.te.2022.482porhttp://creativecommons.org/licenses/by-nc-nd/3.0/us/info:eu-repo/semantics/embargoedAccessreponame:Repositório Institucional da UFUinstname:Universidade Federal de Uberlândia (UFU)instacron:UFU2023-02-24T06:21:19Zoai:repositorio.ufu.br:123456789/37288Repositório InstitucionalONGhttp://repositorio.ufu.br/oai/requestdiinf@dirbi.ufu.bropendoar:2023-02-24T06:21:19Repositório Institucional da UFU - Universidade Federal de Uberlândia (UFU)false
dc.title.none.fl_str_mv Caracterização de hidrociclones com cilindros e cones permeáveis
Characterization of hydrocyclones with permeable cylinders and cones
title Caracterização de hidrociclones com cilindros e cones permeáveis
spellingShingle Caracterização de hidrociclones com cilindros e cones permeáveis
Faria, Érica Victor de
Separação sólido-líquido
Filtração
Suspensões concentradas
Concentração de sólidos
Diâmetro de underflow
Solid-liquid separation
Filtration
Slurries
Solids concentration
Underflow diameter
CNPQ::ENGENHARIAS::ENGENHARIA QUIMICA::OPERACOES INDUSTRIAIS E EQUIPAMENTOS PARA ENGENHARIA QUIMICA::OPERACOES DE SEPARACAO E MISTURA
title_short Caracterização de hidrociclones com cilindros e cones permeáveis
title_full Caracterização de hidrociclones com cilindros e cones permeáveis
title_fullStr Caracterização de hidrociclones com cilindros e cones permeáveis
title_full_unstemmed Caracterização de hidrociclones com cilindros e cones permeáveis
title_sort Caracterização de hidrociclones com cilindros e cones permeáveis
author Faria, Érica Victor de
author_facet Faria, Érica Victor de
author_role author
dc.contributor.none.fl_str_mv Barrozo, Marcos Antonio de Souza
http://lattes.cnpq.br/7024983341494297
Vieira, Luiz Gustavo Martins
http://lattes.cnpq.br/6266547523604644
Bicalho, Isabele Cristina
http://lattes.cnpq.br/3296524340665201
Tanabe, Eduardo Hiromitsu
http://lattes.cnpq.br/9778700143605069
Kyriakidis, Yanne Novais
http://lattes.cnpq.br/4496520699221094
Silva, Danylo de Oliveira
http://lattes.cnpq.br/8216573686887098
dc.contributor.author.fl_str_mv Faria, Érica Victor de
dc.subject.por.fl_str_mv Separação sólido-líquido
Filtração
Suspensões concentradas
Concentração de sólidos
Diâmetro de underflow
Solid-liquid separation
Filtration
Slurries
Solids concentration
Underflow diameter
CNPQ::ENGENHARIAS::ENGENHARIA QUIMICA::OPERACOES INDUSTRIAIS E EQUIPAMENTOS PARA ENGENHARIA QUIMICA::OPERACOES DE SEPARACAO E MISTURA
topic Separação sólido-líquido
Filtração
Suspensões concentradas
Concentração de sólidos
Diâmetro de underflow
Solid-liquid separation
Filtration
Slurries
Solids concentration
Underflow diameter
CNPQ::ENGENHARIAS::ENGENHARIA QUIMICA::OPERACOES INDUSTRIAIS E EQUIPAMENTOS PARA ENGENHARIA QUIMICA::OPERACOES DE SEPARACAO E MISTURA
description Published studies on hydrocyclones up to 2022 mostly report their use in the processing of dilute suspensions. However, high concentrations of solids, is more commonly encountered in industrial practices, and the use of hydrocyclones in these cases can result in inefficient separations. Possible changes in the structure of hydrocyclones have been studied to improve the performance of these separators, such as the association of filtration and hydrocycloning operation. The filtering hydrocyclone has a cylindrical wall, conical wall, or both, made of porous material, and has an additional outflow (filtered) for the fluid. Given this context, this experimental study intended to evaluate the performance of optimal geometries of hydrocyclones with filtering cylinders and cones (HCiCoF-OT1 and HCiCoF-OT3, HCoF-OT1 and HCoF-OT3), proposed by Salvador (2017), operating with suspensions with different solids concentrations. For this, an experimental design was developed for each hydrocyclone to evaluate the effects of filtration and three levels of the variables of interest: feed solids concentration (CVA), underflow diameter (DU), and pressure drop (–ΔP). In all cases, it was observed that the energy consumption was reduced for the filtering hydrocyclones; and the increase in the feed solids concentration led to a reduction in the total efficiency. For the hydrocyclones of HCiCoF-OT1 and HCoF-OT1 geometries, the total efficiency was minimized with the increase of CVA and reduction of the variables underflow diameter and pressure drop. The maximum tottal efficiency achieved was 85 % for HCiCoF-OT1 and 86 % for HCoF-OT1 operating with DU of 5 mm, pressure drop of 1.77 bar, and 1.0 %v. of solids in the feed. These hydrocyclones also provided high total efficiencies in suspensions containing 10.0 %v. solids, reaching 79 % (HCiCoF-OT1) and 77 % (HCoF-OT1). The hydrocyclones of HCiCoF-OT3 and HCoF-OT3 geometries showed low split ratios for all concentrations studied. HCiCoF-OT3 presented RL of 0.6 % for the most diluted suspension (CVA = 1.0 %v.), and 4.0 % for the most concentrated (CVA = 10.0 %v.). To these hydrocyclones the split ratio was lower for dilute suspensions, smaller underflow diameters, and conventional equipment; for concentrated suspensions, the filtering equipment presented a better alternative for providing a lower energy consumption and statistically equal RL.
publishDate 2022
dc.date.none.fl_str_mv 2022-08-29
2023-02-23T18:21:47Z
2023-02-23T18:21:47Z
dc.type.status.fl_str_mv info:eu-repo/semantics/publishedVersion
dc.type.driver.fl_str_mv info:eu-repo/semantics/doctoralThesis
format doctoralThesis
status_str publishedVersion
dc.identifier.uri.fl_str_mv FARIA, Érica Victor de. Caracterização de hidrociclones com cilindros e cones permeáveis. 2022. 181 f. Tese (Doutorado em Engenharia Química) - Universidade Federal de Uberlândia, Uberlândia, 2022. DOI http://doi.org/10.14393/ufu.te.2022.482
https://repositorio.ufu.br/handle/123456789/37288
http://doi.org/10.14393/ufu.te.2022.482
identifier_str_mv FARIA, Érica Victor de. Caracterização de hidrociclones com cilindros e cones permeáveis. 2022. 181 f. Tese (Doutorado em Engenharia Química) - Universidade Federal de Uberlândia, Uberlândia, 2022. DOI http://doi.org/10.14393/ufu.te.2022.482
url https://repositorio.ufu.br/handle/123456789/37288
http://doi.org/10.14393/ufu.te.2022.482
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dc.publisher.none.fl_str_mv Universidade Federal de Uberlândia
Brasil
Programa de Pós-graduação em Engenharia Química
publisher.none.fl_str_mv Universidade Federal de Uberlândia
Brasil
Programa de Pós-graduação em Engenharia Química
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instname:Universidade Federal de Uberlândia (UFU)
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instname_str Universidade Federal de Uberlândia (UFU)
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