Synthesis, characterization and thermal studies on solid 3-methoxybenzoate of some bivalent transition metal ions
Autor(a) principal: | |
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Data de Publicação: | 2005 |
Outros Autores: | , , , , |
Tipo de documento: | Artigo |
Idioma: | eng |
Título da fonte: | Eclética Química |
Texto Completo: | http://old.scielo.br/scielo.php?script=sci_arttext&pid=S0100-46702005000300001 |
Resumo: | Solid-state M-3-MeO-Bz compounds, where M stands for bivalent Mn, Co, Ni, Cu and Zn and 3-MeO-Bz is 3-methoxybenzoate, have been synthesized. Simultaneous thermogravimetry and differential thermal analysis (TG-DTA), differential scanning calorimetry (DSC), X-ray powder diffractometry, infrared spectroscopy, and chemical analysis were used to characterize and to study the thermal behaviour of these compounds. The results led to information about the composition, dehydration, thermal stability and thermal decomposition of the isolated compounds. |
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Eclética Química |
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Synthesis, characterization and thermal studies on solid 3-methoxybenzoate of some bivalent transition metal ionsbivalent transition metals3-methoxybenzoatethermal behaviourSolid-state M-3-MeO-Bz compounds, where M stands for bivalent Mn, Co, Ni, Cu and Zn and 3-MeO-Bz is 3-methoxybenzoate, have been synthesized. Simultaneous thermogravimetry and differential thermal analysis (TG-DTA), differential scanning calorimetry (DSC), X-ray powder diffractometry, infrared spectroscopy, and chemical analysis were used to characterize and to study the thermal behaviour of these compounds. The results led to information about the composition, dehydration, thermal stability and thermal decomposition of the isolated compounds.Fundação Editora da Universidade Estadual Paulista Júlio de Mesquita Filho - UNESP2005-09-01info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersiontext/htmlhttp://old.scielo.br/scielo.php?script=sci_arttext&pid=S0100-46702005000300001Eclética Química v.30 n.3 2005reponame:Eclética Químicainstname:Universidade Estadual Paulista Júlio de Mesquita Filho (UNESP)instacron:UNESP10.1590/S0100-46702005000300001info:eu-repo/semantics/openAccessVallejo,A. C.Siqueira,A. B.Rodrigues,E. C.Ionashiro,E.Y.Bannach,G.Ionashiro,M.eng2005-11-17T00:00:00Zoai:scielo:S0100-46702005000300001Revistahttp://revista.iq.unesp.br/ojs/index.php/ecletica/PUBhttps://revista.iq.unesp.br/ojs/index.php/ecletica/oaiecletica@ctrlk.com.br||ecletica@iq.unesp.br1678-46181678-4618opendoar:2005-11-17T00:00Eclética Química - Universidade Estadual Paulista Júlio de Mesquita Filho (UNESP)false |
dc.title.none.fl_str_mv |
Synthesis, characterization and thermal studies on solid 3-methoxybenzoate of some bivalent transition metal ions |
title |
Synthesis, characterization and thermal studies on solid 3-methoxybenzoate of some bivalent transition metal ions |
spellingShingle |
Synthesis, characterization and thermal studies on solid 3-methoxybenzoate of some bivalent transition metal ions Vallejo,A. C. bivalent transition metals 3-methoxybenzoate thermal behaviour |
title_short |
Synthesis, characterization and thermal studies on solid 3-methoxybenzoate of some bivalent transition metal ions |
title_full |
Synthesis, characterization and thermal studies on solid 3-methoxybenzoate of some bivalent transition metal ions |
title_fullStr |
Synthesis, characterization and thermal studies on solid 3-methoxybenzoate of some bivalent transition metal ions |
title_full_unstemmed |
Synthesis, characterization and thermal studies on solid 3-methoxybenzoate of some bivalent transition metal ions |
title_sort |
Synthesis, characterization and thermal studies on solid 3-methoxybenzoate of some bivalent transition metal ions |
author |
Vallejo,A. C. |
author_facet |
Vallejo,A. C. Siqueira,A. B. Rodrigues,E. C. Ionashiro,E.Y. Bannach,G. Ionashiro,M. |
author_role |
author |
author2 |
Siqueira,A. B. Rodrigues,E. C. Ionashiro,E.Y. Bannach,G. Ionashiro,M. |
author2_role |
author author author author author |
dc.contributor.author.fl_str_mv |
Vallejo,A. C. Siqueira,A. B. Rodrigues,E. C. Ionashiro,E.Y. Bannach,G. Ionashiro,M. |
dc.subject.por.fl_str_mv |
bivalent transition metals 3-methoxybenzoate thermal behaviour |
topic |
bivalent transition metals 3-methoxybenzoate thermal behaviour |
description |
Solid-state M-3-MeO-Bz compounds, where M stands for bivalent Mn, Co, Ni, Cu and Zn and 3-MeO-Bz is 3-methoxybenzoate, have been synthesized. Simultaneous thermogravimetry and differential thermal analysis (TG-DTA), differential scanning calorimetry (DSC), X-ray powder diffractometry, infrared spectroscopy, and chemical analysis were used to characterize and to study the thermal behaviour of these compounds. The results led to information about the composition, dehydration, thermal stability and thermal decomposition of the isolated compounds. |
publishDate |
2005 |
dc.date.none.fl_str_mv |
2005-09-01 |
dc.type.driver.fl_str_mv |
info:eu-repo/semantics/article |
dc.type.status.fl_str_mv |
info:eu-repo/semantics/publishedVersion |
format |
article |
status_str |
publishedVersion |
dc.identifier.uri.fl_str_mv |
http://old.scielo.br/scielo.php?script=sci_arttext&pid=S0100-46702005000300001 |
url |
http://old.scielo.br/scielo.php?script=sci_arttext&pid=S0100-46702005000300001 |
dc.language.iso.fl_str_mv |
eng |
language |
eng |
dc.relation.none.fl_str_mv |
10.1590/S0100-46702005000300001 |
dc.rights.driver.fl_str_mv |
info:eu-repo/semantics/openAccess |
eu_rights_str_mv |
openAccess |
dc.format.none.fl_str_mv |
text/html |
dc.publisher.none.fl_str_mv |
Fundação Editora da Universidade Estadual Paulista Júlio de Mesquita Filho - UNESP |
publisher.none.fl_str_mv |
Fundação Editora da Universidade Estadual Paulista Júlio de Mesquita Filho - UNESP |
dc.source.none.fl_str_mv |
Eclética Química v.30 n.3 2005 reponame:Eclética Química instname:Universidade Estadual Paulista Júlio de Mesquita Filho (UNESP) instacron:UNESP |
instname_str |
Universidade Estadual Paulista Júlio de Mesquita Filho (UNESP) |
instacron_str |
UNESP |
institution |
UNESP |
reponame_str |
Eclética Química |
collection |
Eclética Química |
repository.name.fl_str_mv |
Eclética Química - Universidade Estadual Paulista Júlio de Mesquita Filho (UNESP) |
repository.mail.fl_str_mv |
ecletica@ctrlk.com.br||ecletica@iq.unesp.br |
_version_ |
1754734617711083520 |