Synthesis, characterization and thermal studies on solid state 3-methoxybenzoate of lighter trivalent lanthanides

Detalhes bibliográficos
Autor(a) principal: Dametto,P. R.
Data de Publicação: 2007
Outros Autores: Siqueira,A. B., Carvalho,C. T., Ionashiro,M.
Tipo de documento: Artigo
Idioma: eng
Título da fonte: Eclética Química
Texto Completo: http://old.scielo.br/scielo.php?script=sci_arttext&pid=S0100-46702007000200003
Resumo: Solid-state Ln -3-MeO-Bz compounds, where Ln stands for lighter trivalent lanthanides (La Sm) and 3-methoxybenzoate, have been synthesized. Thermogravimetry (TG), differential scanning calorimetry (DSC), X-ray powder diffractometry, infrared spectroscopy, and complexometry were used to characterize and to study the thermal behaviour of these compounds. The results led to information concerning the composition, dehydration, polymorphic transformation, thermal behaviour and thermal decomposition of the synthesized compounds.
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spelling Synthesis, characterization and thermal studies on solid state 3-methoxybenzoate of lighter trivalent lanthanidesLigther lanthanides3-MethoxybenzoateCharacterizationThermal behaviourSolid-state Ln -3-MeO-Bz compounds, where Ln stands for lighter trivalent lanthanides (La Sm) and 3-methoxybenzoate, have been synthesized. Thermogravimetry (TG), differential scanning calorimetry (DSC), X-ray powder diffractometry, infrared spectroscopy, and complexometry were used to characterize and to study the thermal behaviour of these compounds. The results led to information concerning the composition, dehydration, polymorphic transformation, thermal behaviour and thermal decomposition of the synthesized compounds.Fundação Editora da Universidade Estadual Paulista Júlio de Mesquita Filho - UNESP2007-01-01info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersiontext/htmlhttp://old.scielo.br/scielo.php?script=sci_arttext&pid=S0100-46702007000200003Eclética Química v.32 n.2 2007reponame:Eclética Químicainstname:Universidade Estadual Paulista Júlio de Mesquita Filho (UNESP)instacron:UNESP10.1590/S0100-46702007000200003info:eu-repo/semantics/openAccessDametto,P. R.Siqueira,A. B.Carvalho,C. T.Ionashiro,M.eng2007-10-01T00:00:00Zoai:scielo:S0100-46702007000200003Revistahttp://revista.iq.unesp.br/ojs/index.php/ecletica/PUBhttps://revista.iq.unesp.br/ojs/index.php/ecletica/oaiecletica@ctrlk.com.br||ecletica@iq.unesp.br1678-46181678-4618opendoar:2007-10-01T00:00Eclética Química - Universidade Estadual Paulista Júlio de Mesquita Filho (UNESP)false
dc.title.none.fl_str_mv Synthesis, characterization and thermal studies on solid state 3-methoxybenzoate of lighter trivalent lanthanides
title Synthesis, characterization and thermal studies on solid state 3-methoxybenzoate of lighter trivalent lanthanides
spellingShingle Synthesis, characterization and thermal studies on solid state 3-methoxybenzoate of lighter trivalent lanthanides
Dametto,P. R.
Ligther lanthanides
3-Methoxybenzoate
Characterization
Thermal behaviour
title_short Synthesis, characterization and thermal studies on solid state 3-methoxybenzoate of lighter trivalent lanthanides
title_full Synthesis, characterization and thermal studies on solid state 3-methoxybenzoate of lighter trivalent lanthanides
title_fullStr Synthesis, characterization and thermal studies on solid state 3-methoxybenzoate of lighter trivalent lanthanides
title_full_unstemmed Synthesis, characterization and thermal studies on solid state 3-methoxybenzoate of lighter trivalent lanthanides
title_sort Synthesis, characterization and thermal studies on solid state 3-methoxybenzoate of lighter trivalent lanthanides
author Dametto,P. R.
author_facet Dametto,P. R.
Siqueira,A. B.
Carvalho,C. T.
Ionashiro,M.
author_role author
author2 Siqueira,A. B.
Carvalho,C. T.
Ionashiro,M.
author2_role author
author
author
dc.contributor.author.fl_str_mv Dametto,P. R.
Siqueira,A. B.
Carvalho,C. T.
Ionashiro,M.
dc.subject.por.fl_str_mv Ligther lanthanides
3-Methoxybenzoate
Characterization
Thermal behaviour
topic Ligther lanthanides
3-Methoxybenzoate
Characterization
Thermal behaviour
description Solid-state Ln -3-MeO-Bz compounds, where Ln stands for lighter trivalent lanthanides (La Sm) and 3-methoxybenzoate, have been synthesized. Thermogravimetry (TG), differential scanning calorimetry (DSC), X-ray powder diffractometry, infrared spectroscopy, and complexometry were used to characterize and to study the thermal behaviour of these compounds. The results led to information concerning the composition, dehydration, polymorphic transformation, thermal behaviour and thermal decomposition of the synthesized compounds.
publishDate 2007
dc.date.none.fl_str_mv 2007-01-01
dc.type.driver.fl_str_mv info:eu-repo/semantics/article
dc.type.status.fl_str_mv info:eu-repo/semantics/publishedVersion
format article
status_str publishedVersion
dc.identifier.uri.fl_str_mv http://old.scielo.br/scielo.php?script=sci_arttext&pid=S0100-46702007000200003
url http://old.scielo.br/scielo.php?script=sci_arttext&pid=S0100-46702007000200003
dc.language.iso.fl_str_mv eng
language eng
dc.relation.none.fl_str_mv 10.1590/S0100-46702007000200003
dc.rights.driver.fl_str_mv info:eu-repo/semantics/openAccess
eu_rights_str_mv openAccess
dc.format.none.fl_str_mv text/html
dc.publisher.none.fl_str_mv Fundação Editora da Universidade Estadual Paulista Júlio de Mesquita Filho - UNESP
publisher.none.fl_str_mv Fundação Editora da Universidade Estadual Paulista Júlio de Mesquita Filho - UNESP
dc.source.none.fl_str_mv Eclética Química v.32 n.2 2007
reponame:Eclética Química
instname:Universidade Estadual Paulista Júlio de Mesquita Filho (UNESP)
instacron:UNESP
instname_str Universidade Estadual Paulista Júlio de Mesquita Filho (UNESP)
instacron_str UNESP
institution UNESP
reponame_str Eclética Química
collection Eclética Química
repository.name.fl_str_mv Eclética Química - Universidade Estadual Paulista Júlio de Mesquita Filho (UNESP)
repository.mail.fl_str_mv ecletica@ctrlk.com.br||ecletica@iq.unesp.br
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