Mechanical damping of the snoek peak in tantalum - Oxygen system

• Autor(a) principal: Florêncio, Odila
• Data de Publicação: 2008
• Outros Autores: Silva Jr., Paulo S., Barbosa, Geovani F., Melo, Fábio X., Grandini, Carlos Roberto [UNESP], Ishikawa, Tomaz T.
• Tipo de documento: Artigo de conferência
• Idioma: eng
• Título da fonte: Repositório Institucional da UNESP
• Texto Completo: http://dx.doi.org/10.4028/www.scientific.net/DDF.273-276.239; http://hdl.handle.net/11449/70349
• topic: Internal friction; Oxygen; Tantalum; Anelastic relaxation measurements; Body-centered cubic metals; Matrix-interstitial interaction; Oscillation frequencies; Annealing; Concentration (process); Dislocations (crystals); Relaxation processes; Solid solutions; Tantalum compounds; Crystal structure

Interstitial solutes in body-centered cubic metals, such as oxygen in tantalum, produce ideally Snoek effects when they are in solutions enough diluted. However, for higher concentration of these solutes, more complex relaxation process can occur, as interaction between interstitial solutes and dislocations. Anelastic relaxation measurements were carried out in polycrystalline tantalum samples, using torsion pendulum inverted, operating between 300 K and 680 K and oscillation frequencies in the hertz bandwidth, for three different experimental sample conditions: as received sample, annealed and annealed followed by a treatment in an oxygen atmosphere. These measurements have revealed the following behavior: the intensity of the internal friction peak associated to matrix-interstitial interaction Ta-O decreased between the first run and the next runs, and this phenomenon did not occur for the others conditions. The variation of relaxation strength of Ta-O peak, with number of runs is due to a decrease of an amount of oxygen in solid solution, which can be associated with the precipitation of new phases in Ta sample and with the trapping of oxygen atoms by dislocations.