Mechanochemical method: a powerful tool to obtain ω-poly(ethylene glycol)-functionalized structures and curcumin analogues
Autor(a) principal: | |
---|---|
Data de Publicação: | 2023 |
Outros Autores: | , , , |
Tipo de documento: | Artigo |
Idioma: | eng |
Título da fonte: | Repositório Institucional da UNESP |
Texto Completo: | http://dx.doi.org/10.1039/d3nj01016c http://hdl.handle.net/11449/247326 |
Resumo: | This work reports the mechanochemical synthesis of organic compounds involving carbon-carbon (C-C), carbon-nitrogen (C-N), and carbon-oxygen (C-O). The solid-state synthesis of ω-poly(ethylene glycols) functionalized with different cyclic anhydrides and the obtainment of curcumin Schiff bases and curcumin multicomponent derivatives are also reported. The mechanochemical method was also used in the Steglich esterification using curcumin derivatives. 1H NMR, 13C NMR, MIR, XRPD, and HPLC techniques were performed to confirm the synthesis of each compound. |
id |
UNSP_44fb4755321053a686cece31a1a266c4 |
---|---|
oai_identifier_str |
oai:repositorio.unesp.br:11449/247326 |
network_acronym_str |
UNSP |
network_name_str |
Repositório Institucional da UNESP |
repository_id_str |
2946 |
spelling |
Mechanochemical method: a powerful tool to obtain ω-poly(ethylene glycol)-functionalized structures and curcumin analoguesThis work reports the mechanochemical synthesis of organic compounds involving carbon-carbon (C-C), carbon-nitrogen (C-N), and carbon-oxygen (C-O). The solid-state synthesis of ω-poly(ethylene glycols) functionalized with different cyclic anhydrides and the obtainment of curcumin Schiff bases and curcumin multicomponent derivatives are also reported. The mechanochemical method was also used in the Steglich esterification using curcumin derivatives. 1H NMR, 13C NMR, MIR, XRPD, and HPLC techniques were performed to confirm the synthesis of each compound.School of Sciences Chemistry Department UNESP São Paulo State University, São PauloInstitute of Chemistry UNESP-São Paulo State University, São PauloSchool of Sciences Chemistry Department UNESP São Paulo State University, São PauloInstitute of Chemistry UNESP-São Paulo State University, São PauloUniversidade Estadual Paulista (UNESP)de Moura, Aniele [UNESP]Gaglieri, Caroline [UNESP]Terciotti, Luiz Octavio [UNESP]Rinaldo, Daniel [UNESP]Caires, Flávio Junior [UNESP]2023-07-29T13:13:02Z2023-07-29T13:13:02Z2023-04-18info:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/article9392-9400http://dx.doi.org/10.1039/d3nj01016cNew Journal of Chemistry, v. 47, n. 19, p. 9392-9400, 2023.1369-92611144-0546http://hdl.handle.net/11449/24732610.1039/d3nj01016c2-s2.0-85158860085Scopusreponame:Repositório Institucional da UNESPinstname:Universidade Estadual Paulista (UNESP)instacron:UNESPengNew Journal of Chemistryinfo:eu-repo/semantics/openAccess2023-07-29T13:13:02Zoai:repositorio.unesp.br:11449/247326Repositório InstitucionalPUBhttp://repositorio.unesp.br/oai/requestopendoar:29462024-08-05T20:14:39.662763Repositório Institucional da UNESP - Universidade Estadual Paulista (UNESP)false |
dc.title.none.fl_str_mv |
Mechanochemical method: a powerful tool to obtain ω-poly(ethylene glycol)-functionalized structures and curcumin analogues |
title |
Mechanochemical method: a powerful tool to obtain ω-poly(ethylene glycol)-functionalized structures and curcumin analogues |
spellingShingle |
Mechanochemical method: a powerful tool to obtain ω-poly(ethylene glycol)-functionalized structures and curcumin analogues de Moura, Aniele [UNESP] |
title_short |
Mechanochemical method: a powerful tool to obtain ω-poly(ethylene glycol)-functionalized structures and curcumin analogues |
title_full |
Mechanochemical method: a powerful tool to obtain ω-poly(ethylene glycol)-functionalized structures and curcumin analogues |
title_fullStr |
Mechanochemical method: a powerful tool to obtain ω-poly(ethylene glycol)-functionalized structures and curcumin analogues |
title_full_unstemmed |
Mechanochemical method: a powerful tool to obtain ω-poly(ethylene glycol)-functionalized structures and curcumin analogues |
title_sort |
Mechanochemical method: a powerful tool to obtain ω-poly(ethylene glycol)-functionalized structures and curcumin analogues |
author |
de Moura, Aniele [UNESP] |
author_facet |
de Moura, Aniele [UNESP] Gaglieri, Caroline [UNESP] Terciotti, Luiz Octavio [UNESP] Rinaldo, Daniel [UNESP] Caires, Flávio Junior [UNESP] |
author_role |
author |
author2 |
Gaglieri, Caroline [UNESP] Terciotti, Luiz Octavio [UNESP] Rinaldo, Daniel [UNESP] Caires, Flávio Junior [UNESP] |
author2_role |
author author author author |
dc.contributor.none.fl_str_mv |
Universidade Estadual Paulista (UNESP) |
dc.contributor.author.fl_str_mv |
de Moura, Aniele [UNESP] Gaglieri, Caroline [UNESP] Terciotti, Luiz Octavio [UNESP] Rinaldo, Daniel [UNESP] Caires, Flávio Junior [UNESP] |
description |
This work reports the mechanochemical synthesis of organic compounds involving carbon-carbon (C-C), carbon-nitrogen (C-N), and carbon-oxygen (C-O). The solid-state synthesis of ω-poly(ethylene glycols) functionalized with different cyclic anhydrides and the obtainment of curcumin Schiff bases and curcumin multicomponent derivatives are also reported. The mechanochemical method was also used in the Steglich esterification using curcumin derivatives. 1H NMR, 13C NMR, MIR, XRPD, and HPLC techniques were performed to confirm the synthesis of each compound. |
publishDate |
2023 |
dc.date.none.fl_str_mv |
2023-07-29T13:13:02Z 2023-07-29T13:13:02Z 2023-04-18 |
dc.type.status.fl_str_mv |
info:eu-repo/semantics/publishedVersion |
dc.type.driver.fl_str_mv |
info:eu-repo/semantics/article |
format |
article |
status_str |
publishedVersion |
dc.identifier.uri.fl_str_mv |
http://dx.doi.org/10.1039/d3nj01016c New Journal of Chemistry, v. 47, n. 19, p. 9392-9400, 2023. 1369-9261 1144-0546 http://hdl.handle.net/11449/247326 10.1039/d3nj01016c 2-s2.0-85158860085 |
url |
http://dx.doi.org/10.1039/d3nj01016c http://hdl.handle.net/11449/247326 |
identifier_str_mv |
New Journal of Chemistry, v. 47, n. 19, p. 9392-9400, 2023. 1369-9261 1144-0546 10.1039/d3nj01016c 2-s2.0-85158860085 |
dc.language.iso.fl_str_mv |
eng |
language |
eng |
dc.relation.none.fl_str_mv |
New Journal of Chemistry |
dc.rights.driver.fl_str_mv |
info:eu-repo/semantics/openAccess |
eu_rights_str_mv |
openAccess |
dc.format.none.fl_str_mv |
9392-9400 |
dc.source.none.fl_str_mv |
Scopus reponame:Repositório Institucional da UNESP instname:Universidade Estadual Paulista (UNESP) instacron:UNESP |
instname_str |
Universidade Estadual Paulista (UNESP) |
instacron_str |
UNESP |
institution |
UNESP |
reponame_str |
Repositório Institucional da UNESP |
collection |
Repositório Institucional da UNESP |
repository.name.fl_str_mv |
Repositório Institucional da UNESP - Universidade Estadual Paulista (UNESP) |
repository.mail.fl_str_mv |
|
_version_ |
1808129177771048960 |