Droplet counter-current chromatography of indole alkaloids from Tabernaemontana hilariana

Detalhes bibliográficos
Autor(a) principal: Cardoso, CAL
Data de Publicação: 1999
Outros Autores: Vilegas, Wagner [UNESP]
Tipo de documento: Artigo
Idioma: eng
Título da fonte: Repositório Institucional da UNESP
Texto Completo: http://dx.doi.org/10.1002/(SICI)1099-1565(199903/04)10:2<60
http://hdl.handle.net/11449/32273
Resumo: This paper reports the separation of the indole alkaloids from the benzene extract of the root barks of Tabernaemontana hilariana (Apocynaceae). The crude alkaloid fraction was fractionated by droplet counter-current chromatography using a low polarity mixture (hexane:ethyl acetate:ethanol:water). Nine indole alkaloids (3-hydroxycoronaridine, coronaridine, voacangine, 3-(2-oxopropyl) coronaridine, voacangine hydroxyindolenine, ibogamine, voacangine pseudoindoxyl, coronaridine pseudoindoxyl and tabernanthine) were identified using thin laver chromatography gas chromatography coupled with mass spectrometry and nuclear magnetic resonance spectroscopy. Copyright (C) 1999 John Wiley & Sons, Ltd.
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spelling Droplet counter-current chromatography of indole alkaloids from Tabernaemontana hilarianaTabernaemontana hilarianaApocynacenedroplet counter-current chromatographyindole alkaloidsThis paper reports the separation of the indole alkaloids from the benzene extract of the root barks of Tabernaemontana hilariana (Apocynaceae). The crude alkaloid fraction was fractionated by droplet counter-current chromatography using a low polarity mixture (hexane:ethyl acetate:ethanol:water). Nine indole alkaloids (3-hydroxycoronaridine, coronaridine, voacangine, 3-(2-oxopropyl) coronaridine, voacangine hydroxyindolenine, ibogamine, voacangine pseudoindoxyl, coronaridine pseudoindoxyl and tabernanthine) were identified using thin laver chromatography gas chromatography coupled with mass spectrometry and nuclear magnetic resonance spectroscopy. Copyright (C) 1999 John Wiley & Sons, Ltd.UNESP, Inst Quim, Dept Quim Organ, BR-14800900 Araraquara, SP, BrazilUNESP, Inst Quim, Dept Quim Analit, BR-14800900 Araraquara, SP, BrazilUNESP, Inst Quim, Dept Quim Organ, BR-14800900 Araraquara, SP, BrazilUNESP, Inst Quim, Dept Quim Analit, BR-14800900 Araraquara, SP, BrazilWiley-BlackwellUniversidade Estadual Paulista (Unesp)Cardoso, CALVilegas, Wagner [UNESP]2014-05-20T15:21:06Z2014-05-20T15:21:06Z1999-03-01info:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/article60-63http://dx.doi.org/10.1002/(SICI)1099-1565(199903/04)10:2<60Phytochemical Analysis. W Sussex: John Wiley & Sons Ltd, v. 10, n. 2, p. 60-63, 1999.0958-0344http://hdl.handle.net/11449/3227310.1002/(SICI)1099-1565(199903/04)10:2<60WOS:0000794899000020000-0003-3032-2556Web of Sciencereponame:Repositório Institucional da UNESPinstname:Universidade Estadual Paulista (UNESP)instacron:UNESPengPhytochemical Analysis2.3370,841info:eu-repo/semantics/openAccess2021-10-23T10:49:21Zoai:repositorio.unesp.br:11449/32273Repositório InstitucionalPUBhttp://repositorio.unesp.br/oai/requestopendoar:29462024-08-05T19:53:32.599691Repositório Institucional da UNESP - Universidade Estadual Paulista (UNESP)false
dc.title.none.fl_str_mv Droplet counter-current chromatography of indole alkaloids from Tabernaemontana hilariana
title Droplet counter-current chromatography of indole alkaloids from Tabernaemontana hilariana
spellingShingle Droplet counter-current chromatography of indole alkaloids from Tabernaemontana hilariana
Cardoso, CAL
Tabernaemontana hilariana
Apocynacene
droplet counter-current chromatography
indole alkaloids
title_short Droplet counter-current chromatography of indole alkaloids from Tabernaemontana hilariana
title_full Droplet counter-current chromatography of indole alkaloids from Tabernaemontana hilariana
title_fullStr Droplet counter-current chromatography of indole alkaloids from Tabernaemontana hilariana
title_full_unstemmed Droplet counter-current chromatography of indole alkaloids from Tabernaemontana hilariana
title_sort Droplet counter-current chromatography of indole alkaloids from Tabernaemontana hilariana
author Cardoso, CAL
author_facet Cardoso, CAL
Vilegas, Wagner [UNESP]
author_role author
author2 Vilegas, Wagner [UNESP]
author2_role author
dc.contributor.none.fl_str_mv Universidade Estadual Paulista (Unesp)
dc.contributor.author.fl_str_mv Cardoso, CAL
Vilegas, Wagner [UNESP]
dc.subject.por.fl_str_mv Tabernaemontana hilariana
Apocynacene
droplet counter-current chromatography
indole alkaloids
topic Tabernaemontana hilariana
Apocynacene
droplet counter-current chromatography
indole alkaloids
description This paper reports the separation of the indole alkaloids from the benzene extract of the root barks of Tabernaemontana hilariana (Apocynaceae). The crude alkaloid fraction was fractionated by droplet counter-current chromatography using a low polarity mixture (hexane:ethyl acetate:ethanol:water). Nine indole alkaloids (3-hydroxycoronaridine, coronaridine, voacangine, 3-(2-oxopropyl) coronaridine, voacangine hydroxyindolenine, ibogamine, voacangine pseudoindoxyl, coronaridine pseudoindoxyl and tabernanthine) were identified using thin laver chromatography gas chromatography coupled with mass spectrometry and nuclear magnetic resonance spectroscopy. Copyright (C) 1999 John Wiley & Sons, Ltd.
publishDate 1999
dc.date.none.fl_str_mv 1999-03-01
2014-05-20T15:21:06Z
2014-05-20T15:21:06Z
dc.type.status.fl_str_mv info:eu-repo/semantics/publishedVersion
dc.type.driver.fl_str_mv info:eu-repo/semantics/article
format article
status_str publishedVersion
dc.identifier.uri.fl_str_mv http://dx.doi.org/10.1002/(SICI)1099-1565(199903/04)10:2<60
Phytochemical Analysis. W Sussex: John Wiley & Sons Ltd, v. 10, n. 2, p. 60-63, 1999.
0958-0344
http://hdl.handle.net/11449/32273
10.1002/(SICI)1099-1565(199903/04)10:2<60
WOS:000079489900002
0000-0003-3032-2556
url http://dx.doi.org/10.1002/(SICI)1099-1565(199903/04)10:2<60
http://hdl.handle.net/11449/32273
identifier_str_mv Phytochemical Analysis. W Sussex: John Wiley & Sons Ltd, v. 10, n. 2, p. 60-63, 1999.
0958-0344
10.1002/(SICI)1099-1565(199903/04)10:2<60
WOS:000079489900002
0000-0003-3032-2556
dc.language.iso.fl_str_mv eng
language eng
dc.relation.none.fl_str_mv Phytochemical Analysis
2.337
0,841
dc.rights.driver.fl_str_mv info:eu-repo/semantics/openAccess
eu_rights_str_mv openAccess
dc.format.none.fl_str_mv 60-63
dc.publisher.none.fl_str_mv Wiley-Blackwell
publisher.none.fl_str_mv Wiley-Blackwell
dc.source.none.fl_str_mv Web of Science
reponame:Repositório Institucional da UNESP
instname:Universidade Estadual Paulista (UNESP)
instacron:UNESP
instname_str Universidade Estadual Paulista (UNESP)
instacron_str UNESP
institution UNESP
reponame_str Repositório Institucional da UNESP
collection Repositório Institucional da UNESP
repository.name.fl_str_mv Repositório Institucional da UNESP - Universidade Estadual Paulista (UNESP)
repository.mail.fl_str_mv
_version_ 1808129135111831552

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