Statistical evaluation of the effect of ultrasound on the synthesis of calcium phosphates
Autor(a) principal: | |
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Data de Publicação: | 2019 |
Outros Autores: | , , |
Tipo de documento: | Artigo |
Idioma: | eng |
Título da fonte: | Repositório Institucional da UNESP |
Texto Completo: | http://dx.doi.org/10.33263/BRIAC95345348 http://hdl.handle.net/11449/194898 |
Resumo: | Calcium phosphates are widely used materials in tissue engineering due to their biocompativility and bioactivity. They are present in the bone along with the hydroxyapatite, which facilitates its use as a bioceramic. The mechanical and biological properties of the material obtained in the synthesis process are determined by the size of the particles. There are different ways to decrease the particle size of the materials. Among the methodologies used is the application of ultrasonic radiation. The objective of this work was to statistically evaluate the influence of the ultrasonic application during the synthesis of different phases of calcium phosphates, as well as the type of drying. The particle size determination was performed by scanning electron microscopy. The statistical comparison was made using one way ANOVA. Previously, the hypotheses necessary to validate the model were evaluated. The results were interpreted through its implementation in a statistical software InfoStat (2017 version). The results allow us to conclude that the application of ultrasound during the synthesis process significantly influences the particle size. The type of drying had no significant influence on the particle size. |
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Repositório Institucional da UNESP |
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Statistical evaluation of the effect of ultrasound on the synthesis of calcium phosphatesCalcium phosphatesParticle sizeUltrasonic methodStatistical evaluationCalcium phosphates are widely used materials in tissue engineering due to their biocompativility and bioactivity. They are present in the bone along with the hydroxyapatite, which facilitates its use as a bioceramic. The mechanical and biological properties of the material obtained in the synthesis process are determined by the size of the particles. There are different ways to decrease the particle size of the materials. Among the methodologies used is the application of ultrasonic radiation. The objective of this work was to statistically evaluate the influence of the ultrasonic application during the synthesis of different phases of calcium phosphates, as well as the type of drying. The particle size determination was performed by scanning electron microscopy. The statistical comparison was made using one way ANOVA. Previously, the hypotheses necessary to validate the model were evaluated. The results were interpreted through its implementation in a statistical software InfoStat (2017 version). The results allow us to conclude that the application of ultrasound during the synthesis process significantly influences the particle size. The type of drying had no significant influence on the particle size.Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)Natl Univ Salta, Sci Fac, Math Dept, RA-4400 Salta, ArgentinaUniv Estadual Paulista, Inst Chem, Araraquara, BrazilUniv Estadual Paulista, Inst Chem, Araraquara, BrazilCAPES: 186/13FAPESP: 2017/15487-3Biointerface Research Applied ChemistryNatl Univ SaltaUniversidade Estadual Paulista (Unesp)Tolaba, Angel G.Pellizaro, Thales A. G. [UNESP]Rodriguez-Chanfrau, Jorge E. [UNESP]Guastaldi, Antonio C. [UNESP]2020-12-10T16:58:01Z2020-12-10T16:58:01Z2019-10-15info:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/article4345-4348http://dx.doi.org/10.33263/BRIAC95345348Biointerface Research In Applied Chemistry. Bucuresti: Biointerface Research Applied Chemistry, v. 9, n. 5, p. 4345-4348, 2019.2069-5837http://hdl.handle.net/11449/19489810.33263/BRIAC95345348WOS:000489980300021Web of Sciencereponame:Repositório Institucional da UNESPinstname:Universidade Estadual Paulista (UNESP)instacron:UNESPengBiointerface Research In Applied Chemistryinfo:eu-repo/semantics/openAccess2021-10-23T00:57:10Zoai:repositorio.unesp.br:11449/194898Repositório InstitucionalPUBhttp://repositorio.unesp.br/oai/requestopendoar:29462024-08-05T15:05:11.734056Repositório Institucional da UNESP - Universidade Estadual Paulista (UNESP)false |
dc.title.none.fl_str_mv |
Statistical evaluation of the effect of ultrasound on the synthesis of calcium phosphates |
title |
Statistical evaluation of the effect of ultrasound on the synthesis of calcium phosphates |
spellingShingle |
Statistical evaluation of the effect of ultrasound on the synthesis of calcium phosphates Tolaba, Angel G. Calcium phosphates Particle size Ultrasonic method Statistical evaluation |
title_short |
Statistical evaluation of the effect of ultrasound on the synthesis of calcium phosphates |
title_full |
Statistical evaluation of the effect of ultrasound on the synthesis of calcium phosphates |
title_fullStr |
Statistical evaluation of the effect of ultrasound on the synthesis of calcium phosphates |
title_full_unstemmed |
Statistical evaluation of the effect of ultrasound on the synthesis of calcium phosphates |
title_sort |
Statistical evaluation of the effect of ultrasound on the synthesis of calcium phosphates |
author |
Tolaba, Angel G. |
author_facet |
Tolaba, Angel G. Pellizaro, Thales A. G. [UNESP] Rodriguez-Chanfrau, Jorge E. [UNESP] Guastaldi, Antonio C. [UNESP] |
author_role |
author |
author2 |
Pellizaro, Thales A. G. [UNESP] Rodriguez-Chanfrau, Jorge E. [UNESP] Guastaldi, Antonio C. [UNESP] |
author2_role |
author author author |
dc.contributor.none.fl_str_mv |
Natl Univ Salta Universidade Estadual Paulista (Unesp) |
dc.contributor.author.fl_str_mv |
Tolaba, Angel G. Pellizaro, Thales A. G. [UNESP] Rodriguez-Chanfrau, Jorge E. [UNESP] Guastaldi, Antonio C. [UNESP] |
dc.subject.por.fl_str_mv |
Calcium phosphates Particle size Ultrasonic method Statistical evaluation |
topic |
Calcium phosphates Particle size Ultrasonic method Statistical evaluation |
description |
Calcium phosphates are widely used materials in tissue engineering due to their biocompativility and bioactivity. They are present in the bone along with the hydroxyapatite, which facilitates its use as a bioceramic. The mechanical and biological properties of the material obtained in the synthesis process are determined by the size of the particles. There are different ways to decrease the particle size of the materials. Among the methodologies used is the application of ultrasonic radiation. The objective of this work was to statistically evaluate the influence of the ultrasonic application during the synthesis of different phases of calcium phosphates, as well as the type of drying. The particle size determination was performed by scanning electron microscopy. The statistical comparison was made using one way ANOVA. Previously, the hypotheses necessary to validate the model were evaluated. The results were interpreted through its implementation in a statistical software InfoStat (2017 version). The results allow us to conclude that the application of ultrasound during the synthesis process significantly influences the particle size. The type of drying had no significant influence on the particle size. |
publishDate |
2019 |
dc.date.none.fl_str_mv |
2019-10-15 2020-12-10T16:58:01Z 2020-12-10T16:58:01Z |
dc.type.status.fl_str_mv |
info:eu-repo/semantics/publishedVersion |
dc.type.driver.fl_str_mv |
info:eu-repo/semantics/article |
format |
article |
status_str |
publishedVersion |
dc.identifier.uri.fl_str_mv |
http://dx.doi.org/10.33263/BRIAC95345348 Biointerface Research In Applied Chemistry. Bucuresti: Biointerface Research Applied Chemistry, v. 9, n. 5, p. 4345-4348, 2019. 2069-5837 http://hdl.handle.net/11449/194898 10.33263/BRIAC95345348 WOS:000489980300021 |
url |
http://dx.doi.org/10.33263/BRIAC95345348 http://hdl.handle.net/11449/194898 |
identifier_str_mv |
Biointerface Research In Applied Chemistry. Bucuresti: Biointerface Research Applied Chemistry, v. 9, n. 5, p. 4345-4348, 2019. 2069-5837 10.33263/BRIAC95345348 WOS:000489980300021 |
dc.language.iso.fl_str_mv |
eng |
language |
eng |
dc.relation.none.fl_str_mv |
Biointerface Research In Applied Chemistry |
dc.rights.driver.fl_str_mv |
info:eu-repo/semantics/openAccess |
eu_rights_str_mv |
openAccess |
dc.format.none.fl_str_mv |
4345-4348 |
dc.publisher.none.fl_str_mv |
Biointerface Research Applied Chemistry |
publisher.none.fl_str_mv |
Biointerface Research Applied Chemistry |
dc.source.none.fl_str_mv |
Web of Science reponame:Repositório Institucional da UNESP instname:Universidade Estadual Paulista (UNESP) instacron:UNESP |
instname_str |
Universidade Estadual Paulista (UNESP) |
instacron_str |
UNESP |
institution |
UNESP |
reponame_str |
Repositório Institucional da UNESP |
collection |
Repositório Institucional da UNESP |
repository.name.fl_str_mv |
Repositório Institucional da UNESP - Universidade Estadual Paulista (UNESP) |
repository.mail.fl_str_mv |
|
_version_ |
1808128457124610048 |