Caracterização estrutural e microestrutural da liga Ti-10Mo-40Zr visando aplicações biomédicas

Detalhes bibliográficos
Autor(a) principal: Lopes, Renan Eduardo de Lima
Data de Publicação: 2022
Tipo de documento: Trabalho de conclusão de curso
Idioma: por
Título da fonte: Repositório Institucional da UNESP
Texto Completo: http://hdl.handle.net/11449/217989
Resumo: Faced with the constant increase in the improvement of the population's life, several researches have been carried out to improve biomaterials, which today are responsible for improving the constant quality of life. Titanium alloys are widely used as implants due to properties such as high corrosion resistance, biocompatibility and mechanical strength. The addition of some elements such as molybdenum and zirconium can improve such properties. The present study aims to analyze the Ti-10Mo-40Zr alloy (% by weight) in four different processing conditions, namely melting, homogenization heat treatment, hot rolling and solubilization heat treatment. The chemical characterization of the materials was carried out using the EDS technique and density measurements. The structural analysis was carried out by X-ray diffraction. The microstructural analysis was carried out by optical and scanning electron microscopy techniques. An analysis of the mechanical properties of the alloy was obtained through measurements of Vickers microhardness, modulus of elasticity through the impulse excitation method and tribocorrosion test. Biological analysis was performed using the MTT method. The results of chemical composition by EDS showed that the proposed stoichiometry was respected. The structural and microstructural results indicate that the Ti-10Mo-40Zr alloy has only β phase. The hardness and modulus of elasticity of the alloy are changed through thermomechanical treatments, the hardness and modulus of elasticity decrease as the order of the processing follows. Cell viability tests did not show negative results regarding cytotoxicity, together with cell proliferation tests. The Ti-10Mo-40Zr alloy showed significant potential to be applied as a biomaterial.
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spelling Caracterização estrutural e microestrutural da liga Ti-10Mo-40Zr visando aplicações biomédicasStructural and microstructural characterization of Ti-10Mo-40Zr alloy aiming biomedical applicationsTitanium alloysBiomaterialsLigas de titânioMateriais biomédicosCaracterizaçãoFaced with the constant increase in the improvement of the population's life, several researches have been carried out to improve biomaterials, which today are responsible for improving the constant quality of life. Titanium alloys are widely used as implants due to properties such as high corrosion resistance, biocompatibility and mechanical strength. The addition of some elements such as molybdenum and zirconium can improve such properties. The present study aims to analyze the Ti-10Mo-40Zr alloy (% by weight) in four different processing conditions, namely melting, homogenization heat treatment, hot rolling and solubilization heat treatment. The chemical characterization of the materials was carried out using the EDS technique and density measurements. The structural analysis was carried out by X-ray diffraction. The microstructural analysis was carried out by optical and scanning electron microscopy techniques. An analysis of the mechanical properties of the alloy was obtained through measurements of Vickers microhardness, modulus of elasticity through the impulse excitation method and tribocorrosion test. Biological analysis was performed using the MTT method. The results of chemical composition by EDS showed that the proposed stoichiometry was respected. The structural and microstructural results indicate that the Ti-10Mo-40Zr alloy has only β phase. The hardness and modulus of elasticity of the alloy are changed through thermomechanical treatments, the hardness and modulus of elasticity decrease as the order of the processing follows. Cell viability tests did not show negative results regarding cytotoxicity, together with cell proliferation tests. The Ti-10Mo-40Zr alloy showed significant potential to be applied as a biomaterial.Diante do constante aumento da expectativa de vida da população tem se feito diversas pesquisas para aprimoramento de biomateriais. Assim, foram evoluindo as próteses biomédicas que hoje são responsáveis pela melhora na constante qualidade de vida. As ligas de titânio são muito utilizadas como implantes devido às propriedades como alta resistência à corrosão, biocompatibilidade e resistência mecânica. A adição de alguns elementos como molibdênio e zircônio podem melhorar tais propriedades. O presente trabalho tem por objetivo o processamento e caracterização da liga Ti-10Mo-40Zr (% em peso) em quatro etapas diferentes, sendo elas, bruta de fusão, tratamento térmico de homogeneização, laminação e tratamento térmico de recozimento. A caracterização química dos materiais foi realizada pela técnica de espectroscopia por EDS e medidas de densidade. A análise estrutural foi efetuada por difração de raios X. A análise microestrutural foi realizada pela da técnica de microscopia ótica e eletrônica de varredura. Uma análise das propriedades mecânicas da liga foi obtida por intermédio de medidas de microdureza Vickers, módulo de elasticidade por intermédio do método de excitação por impulso e ensaio de tribocorrosão. A análise biológica foi efetuada através do método do MTT. Os resultados de composição química por EDS mostraram que estequiometria proposta foi respeitada. Os resultados estruturais e microestruturais indicam que a liga Ti10Mo-40Zr possui apenas fase β. Os valores de dureza e módulo de elasticidade da liga são alterados através de tratamentos termomecânicos, a dureza e o módulo de elasticidade diminuem conforme se segue a ordem do processamento. Os testes de viabilidade celular não mostraram resultados negativos quanto à citotoxicidade, juntamente com os testes de proliferação celular. A liga Ti-10Mo-40Zr mostrou significativo potencial para ser aplicada como biomaterial.Não recebi financiamentoUniversidade Estadual Paulista (Unesp)Grandini, Carlos Roberto [UNESP]Universidade Estadual Paulista (Unesp)Lopes, Renan Eduardo de Lima2022-04-25T16:45:59Z2022-04-25T16:45:59Z2022-02-24info:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/bachelorThesisapplication/pdfhttp://hdl.handle.net/11449/217989porinfo:eu-repo/semantics/openAccessreponame:Repositório Institucional da UNESPinstname:Universidade Estadual Paulista (UNESP)instacron:UNESP2023-10-07T06:03:12Zoai:repositorio.unesp.br:11449/217989Repositório InstitucionalPUBhttp://repositorio.unesp.br/oai/requestopendoar:29462024-08-05T14:12:56.149061Repositório Institucional da UNESP - Universidade Estadual Paulista (UNESP)false
dc.title.none.fl_str_mv Caracterização estrutural e microestrutural da liga Ti-10Mo-40Zr visando aplicações biomédicas
Structural and microstructural characterization of Ti-10Mo-40Zr alloy aiming biomedical applications
title Caracterização estrutural e microestrutural da liga Ti-10Mo-40Zr visando aplicações biomédicas
spellingShingle Caracterização estrutural e microestrutural da liga Ti-10Mo-40Zr visando aplicações biomédicas
Lopes, Renan Eduardo de Lima
Titanium alloys
Biomaterials
Ligas de titânio
Materiais biomédicos
Caracterização
title_short Caracterização estrutural e microestrutural da liga Ti-10Mo-40Zr visando aplicações biomédicas
title_full Caracterização estrutural e microestrutural da liga Ti-10Mo-40Zr visando aplicações biomédicas
title_fullStr Caracterização estrutural e microestrutural da liga Ti-10Mo-40Zr visando aplicações biomédicas
title_full_unstemmed Caracterização estrutural e microestrutural da liga Ti-10Mo-40Zr visando aplicações biomédicas
title_sort Caracterização estrutural e microestrutural da liga Ti-10Mo-40Zr visando aplicações biomédicas
author Lopes, Renan Eduardo de Lima
author_facet Lopes, Renan Eduardo de Lima
author_role author
dc.contributor.none.fl_str_mv Grandini, Carlos Roberto [UNESP]
Universidade Estadual Paulista (Unesp)
dc.contributor.author.fl_str_mv Lopes, Renan Eduardo de Lima
dc.subject.por.fl_str_mv Titanium alloys
Biomaterials
Ligas de titânio
Materiais biomédicos
Caracterização
topic Titanium alloys
Biomaterials
Ligas de titânio
Materiais biomédicos
Caracterização
description Faced with the constant increase in the improvement of the population's life, several researches have been carried out to improve biomaterials, which today are responsible for improving the constant quality of life. Titanium alloys are widely used as implants due to properties such as high corrosion resistance, biocompatibility and mechanical strength. The addition of some elements such as molybdenum and zirconium can improve such properties. The present study aims to analyze the Ti-10Mo-40Zr alloy (% by weight) in four different processing conditions, namely melting, homogenization heat treatment, hot rolling and solubilization heat treatment. The chemical characterization of the materials was carried out using the EDS technique and density measurements. The structural analysis was carried out by X-ray diffraction. The microstructural analysis was carried out by optical and scanning electron microscopy techniques. An analysis of the mechanical properties of the alloy was obtained through measurements of Vickers microhardness, modulus of elasticity through the impulse excitation method and tribocorrosion test. Biological analysis was performed using the MTT method. The results of chemical composition by EDS showed that the proposed stoichiometry was respected. The structural and microstructural results indicate that the Ti-10Mo-40Zr alloy has only β phase. The hardness and modulus of elasticity of the alloy are changed through thermomechanical treatments, the hardness and modulus of elasticity decrease as the order of the processing follows. Cell viability tests did not show negative results regarding cytotoxicity, together with cell proliferation tests. The Ti-10Mo-40Zr alloy showed significant potential to be applied as a biomaterial.
publishDate 2022
dc.date.none.fl_str_mv 2022-04-25T16:45:59Z
2022-04-25T16:45:59Z
2022-02-24
dc.type.status.fl_str_mv info:eu-repo/semantics/publishedVersion
dc.type.driver.fl_str_mv info:eu-repo/semantics/bachelorThesis
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url http://hdl.handle.net/11449/217989
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dc.publisher.none.fl_str_mv Universidade Estadual Paulista (Unesp)
publisher.none.fl_str_mv Universidade Estadual Paulista (Unesp)
dc.source.none.fl_str_mv reponame:Repositório Institucional da UNESP
instname:Universidade Estadual Paulista (UNESP)
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instname_str Universidade Estadual Paulista (UNESP)
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institution UNESP
reponame_str Repositório Institucional da UNESP
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repository.name.fl_str_mv Repositório Institucional da UNESP - Universidade Estadual Paulista (UNESP)
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