Urea-Based Synthesis of Zinc Oxide Nanostructures at Low Temperature

Detalhes bibliográficos
Autor(a) principal: Marinho, J. Z.
Data de Publicação: 2012
Outros Autores: Romeiro, F. C., Lemos, S. C. S., Motta, F. V., Riccardi, C. S. [UNESP], Li, M. S., Longo, Elson [UNESP], Lima, R. C.
Tipo de documento: Artigo
Idioma: eng
Título da fonte: Repositório Institucional da UNESP
Texto Completo: http://dx.doi.org/10.1155/2012/427172
http://hdl.handle.net/11449/42434
Resumo: The preparation of nanometer-sized structures of zinc oxide (ZnO) from zinc acetate and urea as raw materials was performed using conventional water bath heating and a microwave hydrothermal (MH) method in an aqueous solution. The oxide formation is controlled by decomposition of the added urea in the sealed autoclave. The influence of urea and the synthesis method on the final product formation are discussed. Broadband photoluminescence (PL) behavior in visible-range spectra was observed with a maximum peak centered in the green region which was attributed to different defects and the structural changes involved with ZnO crystals which were produced during the nucleation process.
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spelling Urea-Based Synthesis of Zinc Oxide Nanostructures at Low TemperatureThe preparation of nanometer-sized structures of zinc oxide (ZnO) from zinc acetate and urea as raw materials was performed using conventional water bath heating and a microwave hydrothermal (MH) method in an aqueous solution. The oxide formation is controlled by decomposition of the added urea in the sealed autoclave. The influence of urea and the synthesis method on the final product formation are discussed. Broadband photoluminescence (PL) behavior in visible-range spectra was observed with a maximum peak centered in the green region which was attributed to different defects and the structural changes involved with ZnO crystals which were produced during the nucleation process.Univ Fed Uberlandia, Inst Quim, BR-38400902 Uberlandia, MG, BrazilUniv Fed Rio Grande do Norte, Dept Mat Engn, BR-59072970 Natal, RN, BrazilUniv Estadual Paulista, Inst Quim, BR-14800900 Araraquara, SP, BrazilUniv São Paulo, Inst Fis Sao Carlos, BR-13566590 Sao Carlos, SP, BrazilUniv Estadual Paulista, Inst Quim, BR-14800900 Araraquara, SP, BrazilHindawi Publishing CorporationUniversidade Federal de Uberlândia (UFU)Universidade Federal do Rio Grande do Norte (UFRN)Universidade Estadual Paulista (Unesp)Universidade de São Paulo (USP)Marinho, J. Z.Romeiro, F. C.Lemos, S. C. S.Motta, F. V.Riccardi, C. S. [UNESP]Li, M. S.Longo, Elson [UNESP]Lima, R. C.2014-05-20T15:34:08Z2014-05-20T15:34:08Z2012-01-01info:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/article7application/pdfhttp://dx.doi.org/10.1155/2012/427172Journal of Nanomaterials. New York: Hindawi Publishing Corporation, p. 7, 2012.1687-4110http://hdl.handle.net/11449/4243410.1155/2012/427172WOS:000304981900001WOS000304981900001.pdfWeb of Sciencereponame:Repositório Institucional da UNESPinstname:Universidade Estadual Paulista (UNESP)instacron:UNESPengJournal of Nanomaterials2.2070,360info:eu-repo/semantics/openAccess2024-12-03T13:43:14Zoai:repositorio.unesp.br:11449/42434Repositório InstitucionalPUBhttp://repositorio.unesp.br/oai/requestrepositoriounesp@unesp.bropendoar:29462024-12-03T13:43:14Repositório Institucional da UNESP - Universidade Estadual Paulista (UNESP)false
dc.title.none.fl_str_mv Urea-Based Synthesis of Zinc Oxide Nanostructures at Low Temperature
title Urea-Based Synthesis of Zinc Oxide Nanostructures at Low Temperature
spellingShingle Urea-Based Synthesis of Zinc Oxide Nanostructures at Low Temperature
Marinho, J. Z.
title_short Urea-Based Synthesis of Zinc Oxide Nanostructures at Low Temperature
title_full Urea-Based Synthesis of Zinc Oxide Nanostructures at Low Temperature
title_fullStr Urea-Based Synthesis of Zinc Oxide Nanostructures at Low Temperature
title_full_unstemmed Urea-Based Synthesis of Zinc Oxide Nanostructures at Low Temperature
title_sort Urea-Based Synthesis of Zinc Oxide Nanostructures at Low Temperature
author Marinho, J. Z.
author_facet Marinho, J. Z.
Romeiro, F. C.
Lemos, S. C. S.
Motta, F. V.
Riccardi, C. S. [UNESP]
Li, M. S.
Longo, Elson [UNESP]
Lima, R. C.
author_role author
author2 Romeiro, F. C.
Lemos, S. C. S.
Motta, F. V.
Riccardi, C. S. [UNESP]
Li, M. S.
Longo, Elson [UNESP]
Lima, R. C.
author2_role author
author
author
author
author
author
author
dc.contributor.none.fl_str_mv Universidade Federal de Uberlândia (UFU)
Universidade Federal do Rio Grande do Norte (UFRN)
Universidade Estadual Paulista (Unesp)
Universidade de São Paulo (USP)
dc.contributor.author.fl_str_mv Marinho, J. Z.
Romeiro, F. C.
Lemos, S. C. S.
Motta, F. V.
Riccardi, C. S. [UNESP]
Li, M. S.
Longo, Elson [UNESP]
Lima, R. C.
description The preparation of nanometer-sized structures of zinc oxide (ZnO) from zinc acetate and urea as raw materials was performed using conventional water bath heating and a microwave hydrothermal (MH) method in an aqueous solution. The oxide formation is controlled by decomposition of the added urea in the sealed autoclave. The influence of urea and the synthesis method on the final product formation are discussed. Broadband photoluminescence (PL) behavior in visible-range spectra was observed with a maximum peak centered in the green region which was attributed to different defects and the structural changes involved with ZnO crystals which were produced during the nucleation process.
publishDate 2012
dc.date.none.fl_str_mv 2012-01-01
2014-05-20T15:34:08Z
2014-05-20T15:34:08Z
dc.type.status.fl_str_mv info:eu-repo/semantics/publishedVersion
dc.type.driver.fl_str_mv info:eu-repo/semantics/article
format article
status_str publishedVersion
dc.identifier.uri.fl_str_mv http://dx.doi.org/10.1155/2012/427172
Journal of Nanomaterials. New York: Hindawi Publishing Corporation, p. 7, 2012.
1687-4110
http://hdl.handle.net/11449/42434
10.1155/2012/427172
WOS:000304981900001
WOS000304981900001.pdf
url http://dx.doi.org/10.1155/2012/427172
http://hdl.handle.net/11449/42434
identifier_str_mv Journal of Nanomaterials. New York: Hindawi Publishing Corporation, p. 7, 2012.
1687-4110
10.1155/2012/427172
WOS:000304981900001
WOS000304981900001.pdf
dc.language.iso.fl_str_mv eng
language eng
dc.relation.none.fl_str_mv Journal of Nanomaterials
2.207
0,360
dc.rights.driver.fl_str_mv info:eu-repo/semantics/openAccess
eu_rights_str_mv openAccess
dc.format.none.fl_str_mv 7
application/pdf
dc.publisher.none.fl_str_mv Hindawi Publishing Corporation
publisher.none.fl_str_mv Hindawi Publishing Corporation
dc.source.none.fl_str_mv Web of Science
reponame:Repositório Institucional da UNESP
instname:Universidade Estadual Paulista (UNESP)
instacron:UNESP
instname_str Universidade Estadual Paulista (UNESP)
instacron_str UNESP
institution UNESP
reponame_str Repositório Institucional da UNESP
collection Repositório Institucional da UNESP
repository.name.fl_str_mv Repositório Institucional da UNESP - Universidade Estadual Paulista (UNESP)
repository.mail.fl_str_mv repositoriounesp@unesp.br
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