Microwave-hydrothermal synthesis of Y3Fe3.35Al1.65O12 nanoparticles for magneto-hyperthermia application
Autor(a) principal: | |
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Data de Publicação: | 2018 |
Outros Autores: | , , , , |
Tipo de documento: | Artigo |
Idioma: | eng |
Título da fonte: | Repositório Institucional da UNESP |
Texto Completo: | http://dx.doi.org/10.1007/s10854-018-9988-x http://hdl.handle.net/11449/180158 |
Resumo: | Crystalline aluminum substituted yttrium iron garnet nanoparticles Y3Fe3.35Al1.65O12 (YIG) was synthesized by hydrothermal microwave synthesis at 140 °C with soaking times ranging from 15 to 60 min. X-ray diffraction confirmed the single-phase YIG nanoparticles excluding the presence of any other phases in the reaction products. The Raman spectra revealed that the largest soaking time provides greater energy crystallization causing changes of lattice vibration and a certain degree of disorder in the crystal lattice. Field emission gun-scanning electron microscopy and high resolution transmission electronic microscopic revealed a homogeneous size distribution of nanometric YIG powders with agglomerated particles. Magnetic measurements were achieved by using a vibrating-sample magnetometer unit. YIG nanoparticles have great potential in magneto-hyperthermia application once in vivo applications magnetic induction heating ferromagnetic compounds generate heat in AC magnetic fields. |
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Repositório Institucional da UNESP |
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Microwave-hydrothermal synthesis of Y3Fe3.35Al1.65O12 nanoparticles for magneto-hyperthermia applicationCrystalline aluminum substituted yttrium iron garnet nanoparticles Y3Fe3.35Al1.65O12 (YIG) was synthesized by hydrothermal microwave synthesis at 140 °C with soaking times ranging from 15 to 60 min. X-ray diffraction confirmed the single-phase YIG nanoparticles excluding the presence of any other phases in the reaction products. The Raman spectra revealed that the largest soaking time provides greater energy crystallization causing changes of lattice vibration and a certain degree of disorder in the crystal lattice. Field emission gun-scanning electron microscopy and high resolution transmission electronic microscopic revealed a homogeneous size distribution of nanometric YIG powders with agglomerated particles. Magnetic measurements were achieved by using a vibrating-sample magnetometer unit. YIG nanoparticles have great potential in magneto-hyperthermia application once in vivo applications magnetic induction heating ferromagnetic compounds generate heat in AC magnetic fields.Faculty of Engineering of Guaratinguetá São Paulo State University - UNESPPhysics and Chemistry Institute Federal University of Itajubá - UNIFEIFaculty of Engineering of Guaratinguetá São Paulo State University - UNESPUniversidade Estadual Paulista (Unesp)Federal University of Itajubá - UNIFEIBorsari, E. [UNESP]Freire, B. G.G. [UNESP]Garcia, F. G.Silva, M. S.Silva, C. C. [UNESP]Simões, A. Z. [UNESP]2018-12-11T17:38:24Z2018-12-11T17:38:24Z2018-01-01info:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/articleapplication/pdfhttp://dx.doi.org/10.1007/s10854-018-9988-xJournal of Materials Science: Materials in Electronics.1573-482X0957-4522http://hdl.handle.net/11449/18015810.1007/s10854-018-9988-x2-s2.0-850529169072-s2.0-85052916907.pdfScopusreponame:Repositório Institucional da UNESPinstname:Universidade Estadual Paulista (UNESP)instacron:UNESPengJournal of Materials Science: Materials in Electronics0,503info:eu-repo/semantics/openAccess2024-07-02T15:04:05Zoai:repositorio.unesp.br:11449/180158Repositório InstitucionalPUBhttp://repositorio.unesp.br/oai/requestopendoar:29462024-08-05T21:18:25.282047Repositório Institucional da UNESP - Universidade Estadual Paulista (UNESP)false |
dc.title.none.fl_str_mv |
Microwave-hydrothermal synthesis of Y3Fe3.35Al1.65O12 nanoparticles for magneto-hyperthermia application |
title |
Microwave-hydrothermal synthesis of Y3Fe3.35Al1.65O12 nanoparticles for magneto-hyperthermia application |
spellingShingle |
Microwave-hydrothermal synthesis of Y3Fe3.35Al1.65O12 nanoparticles for magneto-hyperthermia application Borsari, E. [UNESP] |
title_short |
Microwave-hydrothermal synthesis of Y3Fe3.35Al1.65O12 nanoparticles for magneto-hyperthermia application |
title_full |
Microwave-hydrothermal synthesis of Y3Fe3.35Al1.65O12 nanoparticles for magneto-hyperthermia application |
title_fullStr |
Microwave-hydrothermal synthesis of Y3Fe3.35Al1.65O12 nanoparticles for magneto-hyperthermia application |
title_full_unstemmed |
Microwave-hydrothermal synthesis of Y3Fe3.35Al1.65O12 nanoparticles for magneto-hyperthermia application |
title_sort |
Microwave-hydrothermal synthesis of Y3Fe3.35Al1.65O12 nanoparticles for magneto-hyperthermia application |
author |
Borsari, E. [UNESP] |
author_facet |
Borsari, E. [UNESP] Freire, B. G.G. [UNESP] Garcia, F. G. Silva, M. S. Silva, C. C. [UNESP] Simões, A. Z. [UNESP] |
author_role |
author |
author2 |
Freire, B. G.G. [UNESP] Garcia, F. G. Silva, M. S. Silva, C. C. [UNESP] Simões, A. Z. [UNESP] |
author2_role |
author author author author author |
dc.contributor.none.fl_str_mv |
Universidade Estadual Paulista (Unesp) Federal University of Itajubá - UNIFEI |
dc.contributor.author.fl_str_mv |
Borsari, E. [UNESP] Freire, B. G.G. [UNESP] Garcia, F. G. Silva, M. S. Silva, C. C. [UNESP] Simões, A. Z. [UNESP] |
description |
Crystalline aluminum substituted yttrium iron garnet nanoparticles Y3Fe3.35Al1.65O12 (YIG) was synthesized by hydrothermal microwave synthesis at 140 °C with soaking times ranging from 15 to 60 min. X-ray diffraction confirmed the single-phase YIG nanoparticles excluding the presence of any other phases in the reaction products. The Raman spectra revealed that the largest soaking time provides greater energy crystallization causing changes of lattice vibration and a certain degree of disorder in the crystal lattice. Field emission gun-scanning electron microscopy and high resolution transmission electronic microscopic revealed a homogeneous size distribution of nanometric YIG powders with agglomerated particles. Magnetic measurements were achieved by using a vibrating-sample magnetometer unit. YIG nanoparticles have great potential in magneto-hyperthermia application once in vivo applications magnetic induction heating ferromagnetic compounds generate heat in AC magnetic fields. |
publishDate |
2018 |
dc.date.none.fl_str_mv |
2018-12-11T17:38:24Z 2018-12-11T17:38:24Z 2018-01-01 |
dc.type.status.fl_str_mv |
info:eu-repo/semantics/publishedVersion |
dc.type.driver.fl_str_mv |
info:eu-repo/semantics/article |
format |
article |
status_str |
publishedVersion |
dc.identifier.uri.fl_str_mv |
http://dx.doi.org/10.1007/s10854-018-9988-x Journal of Materials Science: Materials in Electronics. 1573-482X 0957-4522 http://hdl.handle.net/11449/180158 10.1007/s10854-018-9988-x 2-s2.0-85052916907 2-s2.0-85052916907.pdf |
url |
http://dx.doi.org/10.1007/s10854-018-9988-x http://hdl.handle.net/11449/180158 |
identifier_str_mv |
Journal of Materials Science: Materials in Electronics. 1573-482X 0957-4522 10.1007/s10854-018-9988-x 2-s2.0-85052916907 2-s2.0-85052916907.pdf |
dc.language.iso.fl_str_mv |
eng |
language |
eng |
dc.relation.none.fl_str_mv |
Journal of Materials Science: Materials in Electronics 0,503 |
dc.rights.driver.fl_str_mv |
info:eu-repo/semantics/openAccess |
eu_rights_str_mv |
openAccess |
dc.format.none.fl_str_mv |
application/pdf |
dc.source.none.fl_str_mv |
Scopus reponame:Repositório Institucional da UNESP instname:Universidade Estadual Paulista (UNESP) instacron:UNESP |
instname_str |
Universidade Estadual Paulista (UNESP) |
instacron_str |
UNESP |
institution |
UNESP |
reponame_str |
Repositório Institucional da UNESP |
collection |
Repositório Institucional da UNESP |
repository.name.fl_str_mv |
Repositório Institucional da UNESP - Universidade Estadual Paulista (UNESP) |
repository.mail.fl_str_mv |
|
_version_ |
1808129307165327360 |