Microwave-hydrothermal synthesis of Y3Fe3.35Al1.65O12 nanoparticles for magneto-hyperthermia application

Detalhes bibliográficos
Autor(a) principal: Borsari, E. [UNESP]
Data de Publicação: 2018
Outros Autores: Freire, B. G.G. [UNESP], Garcia, F. G., Silva, M. S., Silva, C. C. [UNESP], Simões, A. Z. [UNESP]
Tipo de documento: Artigo
Idioma: eng
Título da fonte: Repositório Institucional da UNESP
Texto Completo: http://dx.doi.org/10.1007/s10854-018-9988-x
http://hdl.handle.net/11449/180158
Resumo: Crystalline aluminum substituted yttrium iron garnet nanoparticles Y3Fe3.35Al1.65O12 (YIG) was synthesized by hydrothermal microwave synthesis at 140 °C with soaking times ranging from 15 to 60 min. X-ray diffraction confirmed the single-phase YIG nanoparticles excluding the presence of any other phases in the reaction products. The Raman spectra revealed that the largest soaking time provides greater energy crystallization causing changes of lattice vibration and a certain degree of disorder in the crystal lattice. Field emission gun-scanning electron microscopy and high resolution transmission electronic microscopic revealed a homogeneous size distribution of nanometric YIG powders with agglomerated particles. Magnetic measurements were achieved by using a vibrating-sample magnetometer unit. YIG nanoparticles have great potential in magneto-hyperthermia application once in vivo applications magnetic induction heating ferromagnetic compounds generate heat in AC magnetic fields.
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spelling Microwave-hydrothermal synthesis of Y3Fe3.35Al1.65O12 nanoparticles for magneto-hyperthermia applicationCrystalline aluminum substituted yttrium iron garnet nanoparticles Y3Fe3.35Al1.65O12 (YIG) was synthesized by hydrothermal microwave synthesis at 140 °C with soaking times ranging from 15 to 60 min. X-ray diffraction confirmed the single-phase YIG nanoparticles excluding the presence of any other phases in the reaction products. The Raman spectra revealed that the largest soaking time provides greater energy crystallization causing changes of lattice vibration and a certain degree of disorder in the crystal lattice. Field emission gun-scanning electron microscopy and high resolution transmission electronic microscopic revealed a homogeneous size distribution of nanometric YIG powders with agglomerated particles. Magnetic measurements were achieved by using a vibrating-sample magnetometer unit. YIG nanoparticles have great potential in magneto-hyperthermia application once in vivo applications magnetic induction heating ferromagnetic compounds generate heat in AC magnetic fields.Faculty of Engineering of Guaratinguetá São Paulo State University - UNESPPhysics and Chemistry Institute Federal University of Itajubá - UNIFEIFaculty of Engineering of Guaratinguetá São Paulo State University - UNESPUniversidade Estadual Paulista (Unesp)Federal University of Itajubá - UNIFEIBorsari, E. [UNESP]Freire, B. G.G. [UNESP]Garcia, F. G.Silva, M. S.Silva, C. C. [UNESP]Simões, A. Z. [UNESP]2018-12-11T17:38:24Z2018-12-11T17:38:24Z2018-01-01info:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/articleapplication/pdfhttp://dx.doi.org/10.1007/s10854-018-9988-xJournal of Materials Science: Materials in Electronics.1573-482X0957-4522http://hdl.handle.net/11449/18015810.1007/s10854-018-9988-x2-s2.0-850529169072-s2.0-85052916907.pdfScopusreponame:Repositório Institucional da UNESPinstname:Universidade Estadual Paulista (UNESP)instacron:UNESPengJournal of Materials Science: Materials in Electronics0,503info:eu-repo/semantics/openAccess2024-07-02T15:04:05Zoai:repositorio.unesp.br:11449/180158Repositório InstitucionalPUBhttp://repositorio.unesp.br/oai/requestopendoar:29462024-08-05T21:18:25.282047Repositório Institucional da UNESP - Universidade Estadual Paulista (UNESP)false
dc.title.none.fl_str_mv Microwave-hydrothermal synthesis of Y3Fe3.35Al1.65O12 nanoparticles for magneto-hyperthermia application
title Microwave-hydrothermal synthesis of Y3Fe3.35Al1.65O12 nanoparticles for magneto-hyperthermia application
spellingShingle Microwave-hydrothermal synthesis of Y3Fe3.35Al1.65O12 nanoparticles for magneto-hyperthermia application
Borsari, E. [UNESP]
title_short Microwave-hydrothermal synthesis of Y3Fe3.35Al1.65O12 nanoparticles for magneto-hyperthermia application
title_full Microwave-hydrothermal synthesis of Y3Fe3.35Al1.65O12 nanoparticles for magneto-hyperthermia application
title_fullStr Microwave-hydrothermal synthesis of Y3Fe3.35Al1.65O12 nanoparticles for magneto-hyperthermia application
title_full_unstemmed Microwave-hydrothermal synthesis of Y3Fe3.35Al1.65O12 nanoparticles for magneto-hyperthermia application
title_sort Microwave-hydrothermal synthesis of Y3Fe3.35Al1.65O12 nanoparticles for magneto-hyperthermia application
author Borsari, E. [UNESP]
author_facet Borsari, E. [UNESP]
Freire, B. G.G. [UNESP]
Garcia, F. G.
Silva, M. S.
Silva, C. C. [UNESP]
Simões, A. Z. [UNESP]
author_role author
author2 Freire, B. G.G. [UNESP]
Garcia, F. G.
Silva, M. S.
Silva, C. C. [UNESP]
Simões, A. Z. [UNESP]
author2_role author
author
author
author
author
dc.contributor.none.fl_str_mv Universidade Estadual Paulista (Unesp)
Federal University of Itajubá - UNIFEI
dc.contributor.author.fl_str_mv Borsari, E. [UNESP]
Freire, B. G.G. [UNESP]
Garcia, F. G.
Silva, M. S.
Silva, C. C. [UNESP]
Simões, A. Z. [UNESP]
description Crystalline aluminum substituted yttrium iron garnet nanoparticles Y3Fe3.35Al1.65O12 (YIG) was synthesized by hydrothermal microwave synthesis at 140 °C with soaking times ranging from 15 to 60 min. X-ray diffraction confirmed the single-phase YIG nanoparticles excluding the presence of any other phases in the reaction products. The Raman spectra revealed that the largest soaking time provides greater energy crystallization causing changes of lattice vibration and a certain degree of disorder in the crystal lattice. Field emission gun-scanning electron microscopy and high resolution transmission electronic microscopic revealed a homogeneous size distribution of nanometric YIG powders with agglomerated particles. Magnetic measurements were achieved by using a vibrating-sample magnetometer unit. YIG nanoparticles have great potential in magneto-hyperthermia application once in vivo applications magnetic induction heating ferromagnetic compounds generate heat in AC magnetic fields.
publishDate 2018
dc.date.none.fl_str_mv 2018-12-11T17:38:24Z
2018-12-11T17:38:24Z
2018-01-01
dc.type.status.fl_str_mv info:eu-repo/semantics/publishedVersion
dc.type.driver.fl_str_mv info:eu-repo/semantics/article
format article
status_str publishedVersion
dc.identifier.uri.fl_str_mv http://dx.doi.org/10.1007/s10854-018-9988-x
Journal of Materials Science: Materials in Electronics.
1573-482X
0957-4522
http://hdl.handle.net/11449/180158
10.1007/s10854-018-9988-x
2-s2.0-85052916907
2-s2.0-85052916907.pdf
url http://dx.doi.org/10.1007/s10854-018-9988-x
http://hdl.handle.net/11449/180158
identifier_str_mv Journal of Materials Science: Materials in Electronics.
1573-482X
0957-4522
10.1007/s10854-018-9988-x
2-s2.0-85052916907
2-s2.0-85052916907.pdf
dc.language.iso.fl_str_mv eng
language eng
dc.relation.none.fl_str_mv Journal of Materials Science: Materials in Electronics
0,503
dc.rights.driver.fl_str_mv info:eu-repo/semantics/openAccess
eu_rights_str_mv openAccess
dc.format.none.fl_str_mv application/pdf
dc.source.none.fl_str_mv Scopus
reponame:Repositório Institucional da UNESP
instname:Universidade Estadual Paulista (UNESP)
instacron:UNESP
instname_str Universidade Estadual Paulista (UNESP)
instacron_str UNESP
institution UNESP
reponame_str Repositório Institucional da UNESP
collection Repositório Institucional da UNESP
repository.name.fl_str_mv Repositório Institucional da UNESP - Universidade Estadual Paulista (UNESP)
repository.mail.fl_str_mv
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