Preparation and characterization of in(OH)3: Eu nanostructures obtained by microwave-assisted hydrothermal method

Detalhes bibliográficos
Autor(a) principal: Motta, Fabiana V.
Data de Publicação: 2012
Outros Autores: Marques, Ana Paula A., Paskocimas, Carlos A., Bomio, Mauricio R. D., Abreu, Maria Fernanda C., Li, Máximo S., Leite, Edson R., Varela, José A. [UNESP], Longo, Elson [UNESP]
Tipo de documento: Capítulo de livro
Idioma: eng
Título da fonte: Repositório Institucional da UNESP
Texto Completo: http://hdl.handle.net/11449/232204
Resumo: Crystalline europium-doped indium hydroxide (In(OH)3:Eu) nanostructures were prepared by a rapid and efficient Microwave-Assisted Hydrothermal (MAH) method. Nanostructures were obtained at a low temperature. FE-SEM images confirm that these samples are composed of 3D nanostructures. XRD, optical diffuse reflectance and photoluminescence (PL) measurements were used to characterize the products. Emission spectra of europium-doped indium hydroxide samples under excitation (350.7 nm) presented broad band emission referent to the indium hydroxide (In(OH)3) matrix and 5D0→7F0, 5D0→ 7F1, 5D0→ 7F2, 5D0→ 7F3 and 5D0→ 7F4 europium transitions at 582, 596, 618, 653 and 701 nm, respectively. Relative intensities of the Eu3+ emissions increased as the concentration of this ion increased from 0, 1, 2, 4 and 8 mol %, of Eu3+, but the luminescence is drastically quenched for the In(OH)3 matrix. © 2012 by Nova Science Publishers, Inc. All rights reserved.
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spelling Preparation and characterization of in(OH)3: Eu nanostructures obtained by microwave-assisted hydrothermal methodHydrothermalHydroxideIndiumMicrowaveNanostructuresCrystalline europium-doped indium hydroxide (In(OH)3:Eu) nanostructures were prepared by a rapid and efficient Microwave-Assisted Hydrothermal (MAH) method. Nanostructures were obtained at a low temperature. FE-SEM images confirm that these samples are composed of 3D nanostructures. XRD, optical diffuse reflectance and photoluminescence (PL) measurements were used to characterize the products. Emission spectra of europium-doped indium hydroxide samples under excitation (350.7 nm) presented broad band emission referent to the indium hydroxide (In(OH)3) matrix and 5D0→7F0, 5D0→ 7F1, 5D0→ 7F2, 5D0→ 7F3 and 5D0→ 7F4 europium transitions at 582, 596, 618, 653 and 701 nm, respectively. Relative intensities of the Eu3+ emissions increased as the concentration of this ion increased from 0, 1, 2, 4 and 8 mol %, of Eu3+, but the luminescence is drastically quenched for the In(OH)3 matrix. © 2012 by Nova Science Publishers, Inc. All rights reserved.Laboratório de Síntese Química Departamento de Engenharia de Materiais Universidade Federal do Rio Grande do Norte, Natal, RNDepartamento de Ciências Exatas e da Terra Universidade Federal de São Paulo, Diadema, SPLaboratório Interdisciplinar de Eletroquímica e Cerâmica Departamento de Química Universidade Federal de São Carlos, São Carlos, SPInstituto de Física de São Carlos Universidade de São Paulo, São Carlos, SPLaboratório Interdisciplinar de Eletroquímica e Cerâmica Instituto de Química Universidade Estadual Paulista, Araraquara, SPLaboratório Interdisciplinar de Eletroquímica e Cerâmica Instituto de Química Universidade Estadual Paulista, Araraquara, SPUniversidade Federal do Rio Grande do NorteUniversidade Federal de São Paulo (UNIFESP)Universidade Federal de São Carlos (UFSCar)Universidade de São Paulo (USP)Universidade Estadual Paulista (UNESP)Motta, Fabiana V.Marques, Ana Paula A.Paskocimas, Carlos A.Bomio, Mauricio R. D.Abreu, Maria Fernanda C.Li, Máximo S.Leite, Edson R.Varela, José A. [UNESP]Longo, Elson [UNESP]2022-04-29T09:12:37Z2022-04-29T09:12:37Z2012-03-01info:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/bookPart255-266Hydroxides: Synthesis, Types and Applications, p. 255-266.http://hdl.handle.net/11449/2322042-s2.0-84892030385Scopusreponame:Repositório Institucional da UNESPinstname:Universidade Estadual Paulista (UNESP)instacron:UNESPengHydroxides: Synthesis, Types and Applicationsinfo:eu-repo/semantics/openAccess2022-04-29T09:12:37Zoai:repositorio.unesp.br:11449/232204Repositório InstitucionalPUBhttp://repositorio.unesp.br/oai/requestopendoar:29462024-08-05T20:56:37.138995Repositório Institucional da UNESP - Universidade Estadual Paulista (UNESP)false
dc.title.none.fl_str_mv Preparation and characterization of in(OH)3: Eu nanostructures obtained by microwave-assisted hydrothermal method
title Preparation and characterization of in(OH)3: Eu nanostructures obtained by microwave-assisted hydrothermal method
spellingShingle Preparation and characterization of in(OH)3: Eu nanostructures obtained by microwave-assisted hydrothermal method
Motta, Fabiana V.
Hydrothermal
Hydroxide
Indium
Microwave
Nanostructures
title_short Preparation and characterization of in(OH)3: Eu nanostructures obtained by microwave-assisted hydrothermal method
title_full Preparation and characterization of in(OH)3: Eu nanostructures obtained by microwave-assisted hydrothermal method
title_fullStr Preparation and characterization of in(OH)3: Eu nanostructures obtained by microwave-assisted hydrothermal method
title_full_unstemmed Preparation and characterization of in(OH)3: Eu nanostructures obtained by microwave-assisted hydrothermal method
title_sort Preparation and characterization of in(OH)3: Eu nanostructures obtained by microwave-assisted hydrothermal method
author Motta, Fabiana V.
author_facet Motta, Fabiana V.
Marques, Ana Paula A.
Paskocimas, Carlos A.
Bomio, Mauricio R. D.
Abreu, Maria Fernanda C.
Li, Máximo S.
Leite, Edson R.
Varela, José A. [UNESP]
Longo, Elson [UNESP]
author_role author
author2 Marques, Ana Paula A.
Paskocimas, Carlos A.
Bomio, Mauricio R. D.
Abreu, Maria Fernanda C.
Li, Máximo S.
Leite, Edson R.
Varela, José A. [UNESP]
Longo, Elson [UNESP]
author2_role author
author
author
author
author
author
author
author
dc.contributor.none.fl_str_mv Universidade Federal do Rio Grande do Norte
Universidade Federal de São Paulo (UNIFESP)
Universidade Federal de São Carlos (UFSCar)
Universidade de São Paulo (USP)
Universidade Estadual Paulista (UNESP)
dc.contributor.author.fl_str_mv Motta, Fabiana V.
Marques, Ana Paula A.
Paskocimas, Carlos A.
Bomio, Mauricio R. D.
Abreu, Maria Fernanda C.
Li, Máximo S.
Leite, Edson R.
Varela, José A. [UNESP]
Longo, Elson [UNESP]
dc.subject.por.fl_str_mv Hydrothermal
Hydroxide
Indium
Microwave
Nanostructures
topic Hydrothermal
Hydroxide
Indium
Microwave
Nanostructures
description Crystalline europium-doped indium hydroxide (In(OH)3:Eu) nanostructures were prepared by a rapid and efficient Microwave-Assisted Hydrothermal (MAH) method. Nanostructures were obtained at a low temperature. FE-SEM images confirm that these samples are composed of 3D nanostructures. XRD, optical diffuse reflectance and photoluminescence (PL) measurements were used to characterize the products. Emission spectra of europium-doped indium hydroxide samples under excitation (350.7 nm) presented broad band emission referent to the indium hydroxide (In(OH)3) matrix and 5D0→7F0, 5D0→ 7F1, 5D0→ 7F2, 5D0→ 7F3 and 5D0→ 7F4 europium transitions at 582, 596, 618, 653 and 701 nm, respectively. Relative intensities of the Eu3+ emissions increased as the concentration of this ion increased from 0, 1, 2, 4 and 8 mol %, of Eu3+, but the luminescence is drastically quenched for the In(OH)3 matrix. © 2012 by Nova Science Publishers, Inc. All rights reserved.
publishDate 2012
dc.date.none.fl_str_mv 2012-03-01
2022-04-29T09:12:37Z
2022-04-29T09:12:37Z
dc.type.status.fl_str_mv info:eu-repo/semantics/publishedVersion
dc.type.driver.fl_str_mv info:eu-repo/semantics/bookPart
format bookPart
status_str publishedVersion
dc.identifier.uri.fl_str_mv Hydroxides: Synthesis, Types and Applications, p. 255-266.
http://hdl.handle.net/11449/232204
2-s2.0-84892030385
identifier_str_mv Hydroxides: Synthesis, Types and Applications, p. 255-266.
2-s2.0-84892030385
url http://hdl.handle.net/11449/232204
dc.language.iso.fl_str_mv eng
language eng
dc.relation.none.fl_str_mv Hydroxides: Synthesis, Types and Applications
dc.rights.driver.fl_str_mv info:eu-repo/semantics/openAccess
eu_rights_str_mv openAccess
dc.format.none.fl_str_mv 255-266
dc.source.none.fl_str_mv Scopus
reponame:Repositório Institucional da UNESP
instname:Universidade Estadual Paulista (UNESP)
instacron:UNESP
instname_str Universidade Estadual Paulista (UNESP)
instacron_str UNESP
institution UNESP
reponame_str Repositório Institucional da UNESP
collection Repositório Institucional da UNESP
repository.name.fl_str_mv Repositório Institucional da UNESP - Universidade Estadual Paulista (UNESP)
repository.mail.fl_str_mv
_version_ 1808129265102749696

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