Relationship between Crystal Shape, Photoluminescence, and Local Structure in SrTiO3 Synthesized by Microwave-Assisted Hydrothermal Method
Autor(a) principal: | |
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Data de Publicação: | 2012 |
Outros Autores: | , , , , , , |
Tipo de documento: | Artigo |
Idioma: | eng |
Título da fonte: | Repositório Institucional da UNESP |
Texto Completo: | http://dx.doi.org/10.1155/2012/890397 http://hdl.handle.net/11449/42435 |
Resumo: | This paper describes the effect of using different titanium precursors on the synthesis and physical properties of SrTiO3 powders obtained by microwave-assisted hydrothermal method. X-ray diffraction measurements, X-ray absorption near-edge structure (XANES) spectroscopy, field emission scanning electron microscopy (FE-SEM), and high-resolution transmission electron microscopy (HRTEM) were carried out to investigate the structural and optical properties of the SrTiO3 spherical and cubelike-shaped particles. The appropriate choice of the titanium precursor allowed the control of morphological and photoluminescence (PL) properties of SrTiO3 compound. The PL emission was more intense in SrTiO3 samples composed of spherelike particles. This behavior was attributed to the existence of a lower amount of defects due to the uniformity of the spherical particles. |
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Repositório Institucional da UNESP |
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Relationship between Crystal Shape, Photoluminescence, and Local Structure in SrTiO3 Synthesized by Microwave-Assisted Hydrothermal MethodThis paper describes the effect of using different titanium precursors on the synthesis and physical properties of SrTiO3 powders obtained by microwave-assisted hydrothermal method. X-ray diffraction measurements, X-ray absorption near-edge structure (XANES) spectroscopy, field emission scanning electron microscopy (FE-SEM), and high-resolution transmission electron microscopy (HRTEM) were carried out to investigate the structural and optical properties of the SrTiO3 spherical and cubelike-shaped particles. The appropriate choice of the titanium precursor allowed the control of morphological and photoluminescence (PL) properties of SrTiO3 compound. The PL emission was more intense in SrTiO3 samples composed of spherelike particles. This behavior was attributed to the existence of a lower amount of defects due to the uniformity of the spherical particles.Conselho Nacional de Desenvolvimento Científico e Tecnológico (CNPq)Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)Univ São Paulo, Inst Fis Sao Carlos, BR-13560970 Sao Carlos, SP, BrazilUniv Estadual Paulista, Inst Quim, BR-14800900 Araraquara, SP, BrazilUniv Fed Sao Carlos, Dept Fis, BR-13565905 Sao Carlos, SP, BrazilUniv Fed Goias, Inst Fis, BR-74001970 Goiania, Go, BrazilUniv Jaume 1, Dept Quim Fis & Analit, Castellon de La Plana 12071, SpainUniv Estadual Paulista, Inst Quim, BR-14800900 Araraquara, SP, BrazilCNPq: 70/2008Hindawi Publishing CorporationUniversidade de São Paulo (USP)Universidade Estadual Paulista (Unesp)Universidade Federal de São Carlos (UFSCar)Universidade Federal de Goiás (UFG)Univ Jaume 1da Silva, Luis F.Avansi, Waldir [UNESP]Moreira, Mario L. [UNESP]Mesquita, AlexandreMaia, Lauro J. Q.Andres, JuanLongo, Elson [UNESP]Mastelaro, Valmor R.2014-05-20T15:34:08Z2014-05-20T15:34:08Z2012-01-01info:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/article6application/pdfhttp://dx.doi.org/10.1155/2012/890397Journal of Nanomaterials. New York: Hindawi Publishing Corporation, p. 6, 2012.1687-4110http://hdl.handle.net/11449/4243510.1155/2012/890397WOS:000305028300001WOS000305028300001.pdfWeb of Sciencereponame:Repositório Institucional da UNESPinstname:Universidade Estadual Paulista (UNESP)instacron:UNESPengJournal of Nanomaterials2.2070,360info:eu-repo/semantics/openAccess2023-12-01T06:12:19Zoai:repositorio.unesp.br:11449/42435Repositório InstitucionalPUBhttp://repositorio.unesp.br/oai/requestopendoar:29462024-08-05T19:12:27.913323Repositório Institucional da UNESP - Universidade Estadual Paulista (UNESP)false |
dc.title.none.fl_str_mv |
Relationship between Crystal Shape, Photoluminescence, and Local Structure in SrTiO3 Synthesized by Microwave-Assisted Hydrothermal Method |
title |
Relationship between Crystal Shape, Photoluminescence, and Local Structure in SrTiO3 Synthesized by Microwave-Assisted Hydrothermal Method |
spellingShingle |
Relationship between Crystal Shape, Photoluminescence, and Local Structure in SrTiO3 Synthesized by Microwave-Assisted Hydrothermal Method da Silva, Luis F. |
title_short |
Relationship between Crystal Shape, Photoluminescence, and Local Structure in SrTiO3 Synthesized by Microwave-Assisted Hydrothermal Method |
title_full |
Relationship between Crystal Shape, Photoluminescence, and Local Structure in SrTiO3 Synthesized by Microwave-Assisted Hydrothermal Method |
title_fullStr |
Relationship between Crystal Shape, Photoluminescence, and Local Structure in SrTiO3 Synthesized by Microwave-Assisted Hydrothermal Method |
title_full_unstemmed |
Relationship between Crystal Shape, Photoluminescence, and Local Structure in SrTiO3 Synthesized by Microwave-Assisted Hydrothermal Method |
title_sort |
Relationship between Crystal Shape, Photoluminescence, and Local Structure in SrTiO3 Synthesized by Microwave-Assisted Hydrothermal Method |
author |
da Silva, Luis F. |
author_facet |
da Silva, Luis F. Avansi, Waldir [UNESP] Moreira, Mario L. [UNESP] Mesquita, Alexandre Maia, Lauro J. Q. Andres, Juan Longo, Elson [UNESP] Mastelaro, Valmor R. |
author_role |
author |
author2 |
Avansi, Waldir [UNESP] Moreira, Mario L. [UNESP] Mesquita, Alexandre Maia, Lauro J. Q. Andres, Juan Longo, Elson [UNESP] Mastelaro, Valmor R. |
author2_role |
author author author author author author author |
dc.contributor.none.fl_str_mv |
Universidade de São Paulo (USP) Universidade Estadual Paulista (Unesp) Universidade Federal de São Carlos (UFSCar) Universidade Federal de Goiás (UFG) Univ Jaume 1 |
dc.contributor.author.fl_str_mv |
da Silva, Luis F. Avansi, Waldir [UNESP] Moreira, Mario L. [UNESP] Mesquita, Alexandre Maia, Lauro J. Q. Andres, Juan Longo, Elson [UNESP] Mastelaro, Valmor R. |
description |
This paper describes the effect of using different titanium precursors on the synthesis and physical properties of SrTiO3 powders obtained by microwave-assisted hydrothermal method. X-ray diffraction measurements, X-ray absorption near-edge structure (XANES) spectroscopy, field emission scanning electron microscopy (FE-SEM), and high-resolution transmission electron microscopy (HRTEM) were carried out to investigate the structural and optical properties of the SrTiO3 spherical and cubelike-shaped particles. The appropriate choice of the titanium precursor allowed the control of morphological and photoluminescence (PL) properties of SrTiO3 compound. The PL emission was more intense in SrTiO3 samples composed of spherelike particles. This behavior was attributed to the existence of a lower amount of defects due to the uniformity of the spherical particles. |
publishDate |
2012 |
dc.date.none.fl_str_mv |
2012-01-01 2014-05-20T15:34:08Z 2014-05-20T15:34:08Z |
dc.type.status.fl_str_mv |
info:eu-repo/semantics/publishedVersion |
dc.type.driver.fl_str_mv |
info:eu-repo/semantics/article |
format |
article |
status_str |
publishedVersion |
dc.identifier.uri.fl_str_mv |
http://dx.doi.org/10.1155/2012/890397 Journal of Nanomaterials. New York: Hindawi Publishing Corporation, p. 6, 2012. 1687-4110 http://hdl.handle.net/11449/42435 10.1155/2012/890397 WOS:000305028300001 WOS000305028300001.pdf |
url |
http://dx.doi.org/10.1155/2012/890397 http://hdl.handle.net/11449/42435 |
identifier_str_mv |
Journal of Nanomaterials. New York: Hindawi Publishing Corporation, p. 6, 2012. 1687-4110 10.1155/2012/890397 WOS:000305028300001 WOS000305028300001.pdf |
dc.language.iso.fl_str_mv |
eng |
language |
eng |
dc.relation.none.fl_str_mv |
Journal of Nanomaterials 2.207 0,360 |
dc.rights.driver.fl_str_mv |
info:eu-repo/semantics/openAccess |
eu_rights_str_mv |
openAccess |
dc.format.none.fl_str_mv |
6 application/pdf |
dc.publisher.none.fl_str_mv |
Hindawi Publishing Corporation |
publisher.none.fl_str_mv |
Hindawi Publishing Corporation |
dc.source.none.fl_str_mv |
Web of Science reponame:Repositório Institucional da UNESP instname:Universidade Estadual Paulista (UNESP) instacron:UNESP |
instname_str |
Universidade Estadual Paulista (UNESP) |
instacron_str |
UNESP |
institution |
UNESP |
reponame_str |
Repositório Institucional da UNESP |
collection |
Repositório Institucional da UNESP |
repository.name.fl_str_mv |
Repositório Institucional da UNESP - Universidade Estadual Paulista (UNESP) |
repository.mail.fl_str_mv |
|
_version_ |
1808129032953266176 |