Slurry sample injection for determination of ferrite nanocolloids chemical composition by ICP spectrometry
Autor(a) principal: | |
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Data de Publicação: | 2007 |
Outros Autores: | , , , , , , |
Tipo de documento: | Artigo de conferência |
Idioma: | eng |
Título da fonte: | Repositório Institucional da UNESP |
Texto Completo: | http://www.nsti.org/procs/Nanotech2007v4/2/W78.819 http://hdl.handle.net/11449/69825 |
Resumo: | This work proposes a new method to determine the chemical composition of magnetic ferrite nanoparticles by the slurry injection technique using the inductively coupled plasma optical emission spectroscopy. In this way, experimental conditions such as aerosol gas flow rate and colloidal stability were optimized in order to use aqueous calibration curves in the slurry nebulization and to determine the chemical composition of a series of sols containing chemically synthesized size-tailored NiFe 2O 4 nanograms. Then, the results of direct sampling and those of conventional aqueous introduction analysis are compared, showing the efficiency of the proposed method. |
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Slurry sample injection for determination of ferrite nanocolloids chemical composition by ICP spectrometryFerrite nanoparticleIcp-oesMagnetic colloidSlurry injectionColloidsFerritesFlow of gasesMagnetic materialsNanoparticlesFerrite nanoparticlesMagnetic colloidsSlurriesThis work proposes a new method to determine the chemical composition of magnetic ferrite nanoparticles by the slurry injection technique using the inductively coupled plasma optical emission spectroscopy. In this way, experimental conditions such as aerosol gas flow rate and colloidal stability were optimized in order to use aqueous calibration curves in the slurry nebulization and to determine the chemical composition of a series of sols containing chemically synthesized size-tailored NiFe 2O 4 nanograms. Then, the results of direct sampling and those of conventional aqueous introduction analysis are compared, showing the efficiency of the proposed method.Grupo de Fluidos Complexos Instituto de Química Universidade de Brasília, CP 04478, CEP 70904-970, Brasília-DFGrupo de Fluidos Complexos Instituto de Física Universidade de Brasília, CP 04455, CEP 70904-970, Brasília-DFDepartamento de Física e Química Universidade Estadual Paulista, CP 31, CEP 15385-000, Ilha Solteira-SPLaboratório de Espectroscopia Aplicada Universidade Católica de Brasília Campus I, QS 07 Lote 01, CEP 71966-700, Brasília-DFDepartamento de Física e Química Universidade Estadual Paulista, CP 31, CEP 15385-000, Ilha Solteira-SPUniversidade de Brasília (UnB)Universidade Estadual Paulista (Unesp)Universidade Católica de Brasília Campus ISousa, M. H.Lins, E. S.Tourinho, F. A.Depeyrot, J.De Castro, G. R. [UNESP]Martins, W. D.Castro, C. F SZara, L. F.2014-05-27T11:22:33Z2014-05-27T11:22:33Z2007-08-23info:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/conferenceObject393-396application/pdfhttp://www.nsti.org/procs/Nanotech2007v4/2/W78.8192007 NSTI Nanotechnology Conference and Trade Show - NSTI Nanotech 2007, Technical Proceedings, v. 4, p. 393-396.http://hdl.handle.net/11449/698252-s2.0-345479660682-s2.0-34547966068.pdfScopusreponame:Repositório Institucional da UNESPinstname:Universidade Estadual Paulista (UNESP)instacron:UNESPeng2007 NSTI Nanotechnology Conference and Trade Show - NSTI Nanotech 2007, Technical Proceedingsinfo:eu-repo/semantics/openAccess2024-07-10T14:08:21Zoai:repositorio.unesp.br:11449/69825Repositório InstitucionalPUBhttp://repositorio.unesp.br/oai/requestopendoar:29462024-08-05T17:51:55.794080Repositório Institucional da UNESP - Universidade Estadual Paulista (UNESP)false |
dc.title.none.fl_str_mv |
Slurry sample injection for determination of ferrite nanocolloids chemical composition by ICP spectrometry |
title |
Slurry sample injection for determination of ferrite nanocolloids chemical composition by ICP spectrometry |
spellingShingle |
Slurry sample injection for determination of ferrite nanocolloids chemical composition by ICP spectrometry Sousa, M. H. Ferrite nanoparticle Icp-oes Magnetic colloid Slurry injection Colloids Ferrites Flow of gases Magnetic materials Nanoparticles Ferrite nanoparticles Magnetic colloids Slurries |
title_short |
Slurry sample injection for determination of ferrite nanocolloids chemical composition by ICP spectrometry |
title_full |
Slurry sample injection for determination of ferrite nanocolloids chemical composition by ICP spectrometry |
title_fullStr |
Slurry sample injection for determination of ferrite nanocolloids chemical composition by ICP spectrometry |
title_full_unstemmed |
Slurry sample injection for determination of ferrite nanocolloids chemical composition by ICP spectrometry |
title_sort |
Slurry sample injection for determination of ferrite nanocolloids chemical composition by ICP spectrometry |
author |
Sousa, M. H. |
author_facet |
Sousa, M. H. Lins, E. S. Tourinho, F. A. Depeyrot, J. De Castro, G. R. [UNESP] Martins, W. D. Castro, C. F S Zara, L. F. |
author_role |
author |
author2 |
Lins, E. S. Tourinho, F. A. Depeyrot, J. De Castro, G. R. [UNESP] Martins, W. D. Castro, C. F S Zara, L. F. |
author2_role |
author author author author author author author |
dc.contributor.none.fl_str_mv |
Universidade de Brasília (UnB) Universidade Estadual Paulista (Unesp) Universidade Católica de Brasília Campus I |
dc.contributor.author.fl_str_mv |
Sousa, M. H. Lins, E. S. Tourinho, F. A. Depeyrot, J. De Castro, G. R. [UNESP] Martins, W. D. Castro, C. F S Zara, L. F. |
dc.subject.por.fl_str_mv |
Ferrite nanoparticle Icp-oes Magnetic colloid Slurry injection Colloids Ferrites Flow of gases Magnetic materials Nanoparticles Ferrite nanoparticles Magnetic colloids Slurries |
topic |
Ferrite nanoparticle Icp-oes Magnetic colloid Slurry injection Colloids Ferrites Flow of gases Magnetic materials Nanoparticles Ferrite nanoparticles Magnetic colloids Slurries |
description |
This work proposes a new method to determine the chemical composition of magnetic ferrite nanoparticles by the slurry injection technique using the inductively coupled plasma optical emission spectroscopy. In this way, experimental conditions such as aerosol gas flow rate and colloidal stability were optimized in order to use aqueous calibration curves in the slurry nebulization and to determine the chemical composition of a series of sols containing chemically synthesized size-tailored NiFe 2O 4 nanograms. Then, the results of direct sampling and those of conventional aqueous introduction analysis are compared, showing the efficiency of the proposed method. |
publishDate |
2007 |
dc.date.none.fl_str_mv |
2007-08-23 2014-05-27T11:22:33Z 2014-05-27T11:22:33Z |
dc.type.status.fl_str_mv |
info:eu-repo/semantics/publishedVersion |
dc.type.driver.fl_str_mv |
info:eu-repo/semantics/conferenceObject |
format |
conferenceObject |
status_str |
publishedVersion |
dc.identifier.uri.fl_str_mv |
http://www.nsti.org/procs/Nanotech2007v4/2/W78.819 2007 NSTI Nanotechnology Conference and Trade Show - NSTI Nanotech 2007, Technical Proceedings, v. 4, p. 393-396. http://hdl.handle.net/11449/69825 2-s2.0-34547966068 2-s2.0-34547966068.pdf |
url |
http://www.nsti.org/procs/Nanotech2007v4/2/W78.819 http://hdl.handle.net/11449/69825 |
identifier_str_mv |
2007 NSTI Nanotechnology Conference and Trade Show - NSTI Nanotech 2007, Technical Proceedings, v. 4, p. 393-396. 2-s2.0-34547966068 2-s2.0-34547966068.pdf |
dc.language.iso.fl_str_mv |
eng |
language |
eng |
dc.relation.none.fl_str_mv |
2007 NSTI Nanotechnology Conference and Trade Show - NSTI Nanotech 2007, Technical Proceedings |
dc.rights.driver.fl_str_mv |
info:eu-repo/semantics/openAccess |
eu_rights_str_mv |
openAccess |
dc.format.none.fl_str_mv |
393-396 application/pdf |
dc.source.none.fl_str_mv |
Scopus reponame:Repositório Institucional da UNESP instname:Universidade Estadual Paulista (UNESP) instacron:UNESP |
instname_str |
Universidade Estadual Paulista (UNESP) |
instacron_str |
UNESP |
institution |
UNESP |
reponame_str |
Repositório Institucional da UNESP |
collection |
Repositório Institucional da UNESP |
repository.name.fl_str_mv |
Repositório Institucional da UNESP - Universidade Estadual Paulista (UNESP) |
repository.mail.fl_str_mv |
|
_version_ |
1808128868437983232 |