Resin-modified glass ionomer containing calcium glycerophosphate: Physico-mechanical properties and enamel demineralization

Detalhes bibliográficos
Autor(a) principal: Santos, Sâmia Sass [UNESP]
Data de Publicação: 2019
Outros Autores: Delbem, Alberto Carlos Botazzo [UNESP], Moraes, João Carlos Silos [UNESP], Souza, José Antônio Santos [UNESP], Oliveira, Lenara Queiroz Chaves [UNESP], Pedrini, Denise [UNESP]
Tipo de documento: Artigo
Idioma: eng
Título da fonte: Repositório Institucional da UNESP
Texto Completo: http://dx.doi.org/10.1590/1678-7757-2018-0188
http://hdl.handle.net/11449/190151
Resumo: Sources of calcium and phosphate have been added to dental restorative materials to improve their anticaries effect. Objective: This study evaluated the effect of adding calcium glycerophosphate (CaGP) to resin-modified glass ionomer cement (RMGIC) on the physico-mechanical properties, ion release, and enamel demineralization. Material and Methods: Specimens were fabricated for each experimental group: RMGIC without CaGP (Control), RMGIC with 1, 3 and 9% CaGP. To determine the release of fluoride (F), calcium (Ca) and phosphorus (P), six specimens were immersed in demineralization and remineralization solutions for 15 days. In another experimental trial, the following physico-mechanical properties were evaluated at time intervals of 1 and 7 days after fabrication: compressive strength (n=12), diametral tensile strength (n=12), surface hardness of material (n=6) and the degree of conversion of monomers (n=8). To study enamel demineralization, specimens (n=12) were attached to enamel blocks and submitted to pH-cycling. Subsequently, surface and cross-sectional hardness and the concentration of F, Ca and P in enamel were determined. Results: The addition of CaGP to RMGIC led to higher mean release of F, Ca and P when compared with control (p<0.001). Mechanical properties were within the range of those of the ionomer cements after addition of 1% and 3% CaGP. The degree of conversion did not differ between groups at the 1st and the 7th day (p>0.439). The addition of 3% and 9% CaGP reduced mineral loss and increased F, Ca and P in the enamel when compared with control (p<0.05). Conclusion: The addition of 3% CaGP in RMGIC increased the release of F, P and Ca, reduced enamel demineralization, and maintained the physico-mechanical properties within the parameters for this material.
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spelling Resin-modified glass ionomer containing calcium glycerophosphate: Physico-mechanical properties and enamel demineralizationCompressive strengthGlass ionomer cementsPhosphatesPolymerizationTooth demineralizationSources of calcium and phosphate have been added to dental restorative materials to improve their anticaries effect. Objective: This study evaluated the effect of adding calcium glycerophosphate (CaGP) to resin-modified glass ionomer cement (RMGIC) on the physico-mechanical properties, ion release, and enamel demineralization. Material and Methods: Specimens were fabricated for each experimental group: RMGIC without CaGP (Control), RMGIC with 1, 3 and 9% CaGP. To determine the release of fluoride (F), calcium (Ca) and phosphorus (P), six specimens were immersed in demineralization and remineralization solutions for 15 days. In another experimental trial, the following physico-mechanical properties were evaluated at time intervals of 1 and 7 days after fabrication: compressive strength (n=12), diametral tensile strength (n=12), surface hardness of material (n=6) and the degree of conversion of monomers (n=8). To study enamel demineralization, specimens (n=12) were attached to enamel blocks and submitted to pH-cycling. Subsequently, surface and cross-sectional hardness and the concentration of F, Ca and P in enamel were determined. Results: The addition of CaGP to RMGIC led to higher mean release of F, Ca and P when compared with control (p<0.001). Mechanical properties were within the range of those of the ionomer cements after addition of 1% and 3% CaGP. The degree of conversion did not differ between groups at the 1st and the 7th day (p>0.439). The addition of 3% and 9% CaGP reduced mineral loss and increased F, Ca and P in the enamel when compared with control (p<0.05). Conclusion: The addition of 3% CaGP in RMGIC increased the release of F, P and Ca, reduced enamel demineralization, and maintained the physico-mechanical properties within the parameters for this material.Coordenação de Aperfeiçoamento de Pessoal de Nível Superior (CAPES)Universidade Estadual Paulista (UNESP) Faculdade de Odontologia Departamento de Odontopediatria e Odontologia SocialUniversidade Estadual Paulista (UNESP) Faculdade de Engenharia Departamento de Física e QuímicaUniversidade Estadual Paulista (UNESP) Faculdade de Odontologia Departamento de Cirurgia e Clínica IntegradaUniversidade Estadual Paulista (UNESP) Faculdade de Odontologia Departamento de Odontopediatria e Odontologia SocialUniversidade Estadual Paulista (UNESP) Faculdade de Engenharia Departamento de Física e QuímicaUniversidade Estadual Paulista (UNESP) Faculdade de Odontologia Departamento de Cirurgia e Clínica IntegradaUniversidade Estadual Paulista (Unesp)Santos, Sâmia Sass [UNESP]Delbem, Alberto Carlos Botazzo [UNESP]Moraes, João Carlos Silos [UNESP]Souza, José Antônio Santos [UNESP]Oliveira, Lenara Queiroz Chaves [UNESP]Pedrini, Denise [UNESP]2019-10-06T17:04:01Z2019-10-06T17:04:01Z2019-01-01info:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/articleapplication/pdfhttp://dx.doi.org/10.1590/1678-7757-2018-0188Journal of Applied Oral Science, v. 27.1678-77651678-7757http://hdl.handle.net/11449/19015110.1590/1678-7757-2018-0188S1678-775720190001004302-s2.0-85062291965S1678-77572019000100430.pdfScopusreponame:Repositório Institucional da UNESPinstname:Universidade Estadual Paulista (UNESP)instacron:UNESPengJournal of Applied Oral Scienceinfo:eu-repo/semantics/openAccess2024-09-19T17:56:49Zoai:repositorio.unesp.br:11449/190151Repositório InstitucionalPUBhttp://repositorio.unesp.br/oai/requestrepositoriounesp@unesp.bropendoar:29462024-09-19T17:56:49Repositório Institucional da UNESP - Universidade Estadual Paulista (UNESP)false
dc.title.none.fl_str_mv Resin-modified glass ionomer containing calcium glycerophosphate: Physico-mechanical properties and enamel demineralization
title Resin-modified glass ionomer containing calcium glycerophosphate: Physico-mechanical properties and enamel demineralization
spellingShingle Resin-modified glass ionomer containing calcium glycerophosphate: Physico-mechanical properties and enamel demineralization
Santos, Sâmia Sass [UNESP]
Compressive strength
Glass ionomer cements
Phosphates
Polymerization
Tooth demineralization
title_short Resin-modified glass ionomer containing calcium glycerophosphate: Physico-mechanical properties and enamel demineralization
title_full Resin-modified glass ionomer containing calcium glycerophosphate: Physico-mechanical properties and enamel demineralization
title_fullStr Resin-modified glass ionomer containing calcium glycerophosphate: Physico-mechanical properties and enamel demineralization
title_full_unstemmed Resin-modified glass ionomer containing calcium glycerophosphate: Physico-mechanical properties and enamel demineralization
title_sort Resin-modified glass ionomer containing calcium glycerophosphate: Physico-mechanical properties and enamel demineralization
author Santos, Sâmia Sass [UNESP]
author_facet Santos, Sâmia Sass [UNESP]
Delbem, Alberto Carlos Botazzo [UNESP]
Moraes, João Carlos Silos [UNESP]
Souza, José Antônio Santos [UNESP]
Oliveira, Lenara Queiroz Chaves [UNESP]
Pedrini, Denise [UNESP]
author_role author
author2 Delbem, Alberto Carlos Botazzo [UNESP]
Moraes, João Carlos Silos [UNESP]
Souza, José Antônio Santos [UNESP]
Oliveira, Lenara Queiroz Chaves [UNESP]
Pedrini, Denise [UNESP]
author2_role author
author
author
author
author
dc.contributor.none.fl_str_mv Universidade Estadual Paulista (Unesp)
dc.contributor.author.fl_str_mv Santos, Sâmia Sass [UNESP]
Delbem, Alberto Carlos Botazzo [UNESP]
Moraes, João Carlos Silos [UNESP]
Souza, José Antônio Santos [UNESP]
Oliveira, Lenara Queiroz Chaves [UNESP]
Pedrini, Denise [UNESP]
dc.subject.por.fl_str_mv Compressive strength
Glass ionomer cements
Phosphates
Polymerization
Tooth demineralization
topic Compressive strength
Glass ionomer cements
Phosphates
Polymerization
Tooth demineralization
description Sources of calcium and phosphate have been added to dental restorative materials to improve their anticaries effect. Objective: This study evaluated the effect of adding calcium glycerophosphate (CaGP) to resin-modified glass ionomer cement (RMGIC) on the physico-mechanical properties, ion release, and enamel demineralization. Material and Methods: Specimens were fabricated for each experimental group: RMGIC without CaGP (Control), RMGIC with 1, 3 and 9% CaGP. To determine the release of fluoride (F), calcium (Ca) and phosphorus (P), six specimens were immersed in demineralization and remineralization solutions for 15 days. In another experimental trial, the following physico-mechanical properties were evaluated at time intervals of 1 and 7 days after fabrication: compressive strength (n=12), diametral tensile strength (n=12), surface hardness of material (n=6) and the degree of conversion of monomers (n=8). To study enamel demineralization, specimens (n=12) were attached to enamel blocks and submitted to pH-cycling. Subsequently, surface and cross-sectional hardness and the concentration of F, Ca and P in enamel were determined. Results: The addition of CaGP to RMGIC led to higher mean release of F, Ca and P when compared with control (p<0.001). Mechanical properties were within the range of those of the ionomer cements after addition of 1% and 3% CaGP. The degree of conversion did not differ between groups at the 1st and the 7th day (p>0.439). The addition of 3% and 9% CaGP reduced mineral loss and increased F, Ca and P in the enamel when compared with control (p<0.05). Conclusion: The addition of 3% CaGP in RMGIC increased the release of F, P and Ca, reduced enamel demineralization, and maintained the physico-mechanical properties within the parameters for this material.
publishDate 2019
dc.date.none.fl_str_mv 2019-10-06T17:04:01Z
2019-10-06T17:04:01Z
2019-01-01
dc.type.status.fl_str_mv info:eu-repo/semantics/publishedVersion
dc.type.driver.fl_str_mv info:eu-repo/semantics/article
format article
status_str publishedVersion
dc.identifier.uri.fl_str_mv http://dx.doi.org/10.1590/1678-7757-2018-0188
Journal of Applied Oral Science, v. 27.
1678-7765
1678-7757
http://hdl.handle.net/11449/190151
10.1590/1678-7757-2018-0188
S1678-77572019000100430
2-s2.0-85062291965
S1678-77572019000100430.pdf
url http://dx.doi.org/10.1590/1678-7757-2018-0188
http://hdl.handle.net/11449/190151
identifier_str_mv Journal of Applied Oral Science, v. 27.
1678-7765
1678-7757
10.1590/1678-7757-2018-0188
S1678-77572019000100430
2-s2.0-85062291965
S1678-77572019000100430.pdf
dc.language.iso.fl_str_mv eng
language eng
dc.relation.none.fl_str_mv Journal of Applied Oral Science
dc.rights.driver.fl_str_mv info:eu-repo/semantics/openAccess
eu_rights_str_mv openAccess
dc.format.none.fl_str_mv application/pdf
dc.source.none.fl_str_mv Scopus
reponame:Repositório Institucional da UNESP
instname:Universidade Estadual Paulista (UNESP)
instacron:UNESP
instname_str Universidade Estadual Paulista (UNESP)
instacron_str UNESP
institution UNESP
reponame_str Repositório Institucional da UNESP
collection Repositório Institucional da UNESP
repository.name.fl_str_mv Repositório Institucional da UNESP - Universidade Estadual Paulista (UNESP)
repository.mail.fl_str_mv repositoriounesp@unesp.br
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