Corrosion behavior of zirconia in acidulated phosphate fluoride
Autor(a) principal: | |
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Data de Publicação: | 2016 |
Outros Autores: | , , , , , |
Tipo de documento: | Artigo |
Idioma: | eng |
Título da fonte: | Journal of applied oral science (Online) |
Texto Completo: | https://www.revistas.usp.br/jaos/article/view/112884 |
Resumo: | Objective The corrosion behavior of zirconia in acidulated phosphate fluoride (APF) representing acidic environments and fluoride treatments was studied. Material and Methods Zirconia rods were immersed in 1.23% and 0.123% APF solutions and maintained at 37°C for determined periods of time. Surfaces of all specimens were imaged using digital microscopy and scanning electron microscopy (SEM). Sample mass and dimensions were measured for mass loss determination. Samples were characterized by powder X-ray diffraction (XRD) to detect changes in crystallinity. A biosensor based on electrochemical impedance spectroscopy (EIS) was used to detect ion dissolution of material into the immersion media. Results Digital microscopy revealed diminishing luster of the materials and SEM showed increased superficial corrosion of zirconia submerged in 1.23% APF. Although no structural change was found, the absorption of salts (sodium phosphate) onto the surface of the materials bathed in 0.123% APF was significant. EIS indicated a greater change of impedance for the immersion solutions with increasing bathing time. Conclusion Immersion of zirconia in APF solutions showed deterioration limited to the surface, not extending to the bulk of the material. Inferences on zirconia performance in acidic oral environment can be elucidated from the study. |
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Journal of applied oral science (Online) |
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Corrosion behavior of zirconia in acidulated phosphate fluoride Objective The corrosion behavior of zirconia in acidulated phosphate fluoride (APF) representing acidic environments and fluoride treatments was studied. Material and Methods Zirconia rods were immersed in 1.23% and 0.123% APF solutions and maintained at 37°C for determined periods of time. Surfaces of all specimens were imaged using digital microscopy and scanning electron microscopy (SEM). Sample mass and dimensions were measured for mass loss determination. Samples were characterized by powder X-ray diffraction (XRD) to detect changes in crystallinity. A biosensor based on electrochemical impedance spectroscopy (EIS) was used to detect ion dissolution of material into the immersion media. Results Digital microscopy revealed diminishing luster of the materials and SEM showed increased superficial corrosion of zirconia submerged in 1.23% APF. Although no structural change was found, the absorption of salts (sodium phosphate) onto the surface of the materials bathed in 0.123% APF was significant. EIS indicated a greater change of impedance for the immersion solutions with increasing bathing time. Conclusion Immersion of zirconia in APF solutions showed deterioration limited to the surface, not extending to the bulk of the material. Inferences on zirconia performance in acidic oral environment can be elucidated from the study. Universidade de São Paulo. Faculdade de Odontologia de Bauru2016-02-01info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersionapplication/pdfhttps://www.revistas.usp.br/jaos/article/view/11288410.1590/1678-775720150435Journal of Applied Oral Science; Vol. 24 No. 1 (2016); 52-60Journal of Applied Oral Science; Vol. 24 Núm. 1 (2016); 52-60Journal of Applied Oral Science; v. 24 n. 1 (2016); 52-601678-77651678-7757reponame:Journal of applied oral science (Online)instname:Universidade de São Paulo (USP)instacron:USPenghttps://www.revistas.usp.br/jaos/article/view/112884/110827Copyright (c) 2016 Journal of Applied Oral Scienceinfo:eu-repo/semantics/openAccessThomas, Anie Sridhar, Sathyanarayanan Aghyarian, Shant Watkins-curry, Pilanda Chan, Julia Y.Pozzi, Alessandro Rodrigues, Danieli C.2016-03-23T18:16:02Zoai:revistas.usp.br:article/112884Revistahttp://www.scielo.br/jaosPUBhttps://www.revistas.usp.br/jaos/oai||jaos@usp.br1678-77651678-7757opendoar:2016-03-23T18:16:02Journal of applied oral science (Online) - Universidade de São Paulo (USP)false |
dc.title.none.fl_str_mv |
Corrosion behavior of zirconia in acidulated phosphate fluoride |
title |
Corrosion behavior of zirconia in acidulated phosphate fluoride |
spellingShingle |
Corrosion behavior of zirconia in acidulated phosphate fluoride Thomas, Anie |
title_short |
Corrosion behavior of zirconia in acidulated phosphate fluoride |
title_full |
Corrosion behavior of zirconia in acidulated phosphate fluoride |
title_fullStr |
Corrosion behavior of zirconia in acidulated phosphate fluoride |
title_full_unstemmed |
Corrosion behavior of zirconia in acidulated phosphate fluoride |
title_sort |
Corrosion behavior of zirconia in acidulated phosphate fluoride |
author |
Thomas, Anie |
author_facet |
Thomas, Anie Sridhar, Sathyanarayanan Aghyarian, Shant Watkins-curry, Pilanda Chan, Julia Y. Pozzi, Alessandro Rodrigues, Danieli C. |
author_role |
author |
author2 |
Sridhar, Sathyanarayanan Aghyarian, Shant Watkins-curry, Pilanda Chan, Julia Y. Pozzi, Alessandro Rodrigues, Danieli C. |
author2_role |
author author author author author author |
dc.contributor.author.fl_str_mv |
Thomas, Anie Sridhar, Sathyanarayanan Aghyarian, Shant Watkins-curry, Pilanda Chan, Julia Y. Pozzi, Alessandro Rodrigues, Danieli C. |
description |
Objective The corrosion behavior of zirconia in acidulated phosphate fluoride (APF) representing acidic environments and fluoride treatments was studied. Material and Methods Zirconia rods were immersed in 1.23% and 0.123% APF solutions and maintained at 37°C for determined periods of time. Surfaces of all specimens were imaged using digital microscopy and scanning electron microscopy (SEM). Sample mass and dimensions were measured for mass loss determination. Samples were characterized by powder X-ray diffraction (XRD) to detect changes in crystallinity. A biosensor based on electrochemical impedance spectroscopy (EIS) was used to detect ion dissolution of material into the immersion media. Results Digital microscopy revealed diminishing luster of the materials and SEM showed increased superficial corrosion of zirconia submerged in 1.23% APF. Although no structural change was found, the absorption of salts (sodium phosphate) onto the surface of the materials bathed in 0.123% APF was significant. EIS indicated a greater change of impedance for the immersion solutions with increasing bathing time. Conclusion Immersion of zirconia in APF solutions showed deterioration limited to the surface, not extending to the bulk of the material. Inferences on zirconia performance in acidic oral environment can be elucidated from the study. |
publishDate |
2016 |
dc.date.none.fl_str_mv |
2016-02-01 |
dc.type.driver.fl_str_mv |
info:eu-repo/semantics/article info:eu-repo/semantics/publishedVersion |
format |
article |
status_str |
publishedVersion |
dc.identifier.uri.fl_str_mv |
https://www.revistas.usp.br/jaos/article/view/112884 10.1590/1678-775720150435 |
url |
https://www.revistas.usp.br/jaos/article/view/112884 |
identifier_str_mv |
10.1590/1678-775720150435 |
dc.language.iso.fl_str_mv |
eng |
language |
eng |
dc.relation.none.fl_str_mv |
https://www.revistas.usp.br/jaos/article/view/112884/110827 |
dc.rights.driver.fl_str_mv |
Copyright (c) 2016 Journal of Applied Oral Science info:eu-repo/semantics/openAccess |
rights_invalid_str_mv |
Copyright (c) 2016 Journal of Applied Oral Science |
eu_rights_str_mv |
openAccess |
dc.format.none.fl_str_mv |
application/pdf |
dc.publisher.none.fl_str_mv |
Universidade de São Paulo. Faculdade de Odontologia de Bauru |
publisher.none.fl_str_mv |
Universidade de São Paulo. Faculdade de Odontologia de Bauru |
dc.source.none.fl_str_mv |
Journal of Applied Oral Science; Vol. 24 No. 1 (2016); 52-60 Journal of Applied Oral Science; Vol. 24 Núm. 1 (2016); 52-60 Journal of Applied Oral Science; v. 24 n. 1 (2016); 52-60 1678-7765 1678-7757 reponame:Journal of applied oral science (Online) instname:Universidade de São Paulo (USP) instacron:USP |
instname_str |
Universidade de São Paulo (USP) |
instacron_str |
USP |
institution |
USP |
reponame_str |
Journal of applied oral science (Online) |
collection |
Journal of applied oral science (Online) |
repository.name.fl_str_mv |
Journal of applied oral science (Online) - Universidade de São Paulo (USP) |
repository.mail.fl_str_mv |
||jaos@usp.br |
_version_ |
1800221679595552768 |