Characterization of the particles surface of dried dairy products

Detalhes bibliográficos
Autor(a) principal: Toledo, Paulo Henrique de Melo
Data de Publicação: 2020
Outros Autores: Pereira, João Pablo Fortes, Perrone, Ítalo Tuler, Carvalho, Antônio Fernandes, Oliveira, Luiz Fernando Cappa, Stephani, Rodrigo
Tipo de documento: Artigo
Idioma: por
Título da fonte: Revista do Instituto de Laticínios Cândido Tostes
Texto Completo: https://www.revistadoilct.com.br/rilct/article/view/755
Resumo: During production or storage of dehydrated dairy products, milk constituents may undergo redistribution, resulting in heterogeneity between the surface and its interior. The main objective of this work was to map the surfaces of different dehydrated dairy products, with the combined use of Raman spectroscopy and scanning electron microscopy (SEM) coupled with energy dispersive spectroscopy (EDS). It was intended to characterize the surfaces of the particles of interest in both instruments and to perform the mapping of these, within specific populations. The proposal to combine different techniques aimed, in addition to obtaining complementary data, to show that it is possible to advance in the research of dairy products when analyzing the particles under different analytical perspectives. All analyzes were carried out from industrialized products with lots, manufacture and validity dates monitored. From the spectroscopic profiles of the particles, it was possible to verify differences when the set of particles was analyzed, as well the target particles alone. It was possible to perform the characterization of the particles using different analytical techniques providing a data set that expands information about the particles of the dairy powders analyzed.
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spelling Characterization of the particles surface of dried dairy productsCaracterização da superfície de partículas de produtos lácteos desidratadosenergy dispersive spectroscopy; Raman mapping; scanning electron microscopy.Físico química, química de lácteos; Concentrados, desidratados, soroespectroscopia por energia dispersiva; mapeamento Raman; microscopia eletrônica de varredura.During production or storage of dehydrated dairy products, milk constituents may undergo redistribution, resulting in heterogeneity between the surface and its interior. The main objective of this work was to map the surfaces of different dehydrated dairy products, with the combined use of Raman spectroscopy and scanning electron microscopy (SEM) coupled with energy dispersive spectroscopy (EDS). It was intended to characterize the surfaces of the particles of interest in both instruments and to perform the mapping of these, within specific populations. The proposal to combine different techniques aimed, in addition to obtaining complementary data, to show that it is possible to advance in the research of dairy products when analyzing the particles under different analytical perspectives. All analyzes were carried out from industrialized products with lots, manufacture and validity dates monitored. From the spectroscopic profiles of the particles, it was possible to verify differences when the set of particles was analyzed, as well the target particles alone. It was possible to perform the characterization of the particles using different analytical techniques providing a data set that expands information about the particles of the dairy powders analyzed.Durante o processo de produção ou estocagem dos lácteos desidratados, os constituintes do leite podem sofrer redistribuições, resultando em uma heterogeneidade entre a superfície e seu interior. O principal objetivo deste trabalho foi realizar o mapeamento das superfícies de diferentes produtos lácteos desidratados, com o uso combinado da espectroscopia Raman e a microscopia eletrônica de varredura (MEV) acoplada à espectroscopia por energia dispersiva (EDS). Caracterizou-se as superfícies das partículas em ambos os instrumentos e realizou-se o mapeamento, dentro de populações específicas. A proposta de associar as diferentes técnicas visou, além de obter dados complementares, mostrar que é possível avançar na pesquisa dos produtos lácteos, quando se analisa as partículas sob diferentes perspectivas analíticas. Todas as análises foram realizadas a partir de produtos industrializados com lotes, datas de fabricação e validade monitoradas. A partir da análise dos perfis espectroscópicos das partículas foi possível verificar diferenças tanto do conjunto de partículas bem como das partículas alvo isoladamente. Foi possível realizar a caracterização das partículas utilizando diferentes técnicas analíticas fornecendo um conjunto de dados que amplia informações acerca das partículas dos pós estudados.ILCTCNPq, CAPES e FAPEMIGToledo, Paulo Henrique de MeloPereira, João Pablo FortesPerrone, Ítalo TulerCarvalho, Antônio FernandesOliveira, Luiz Fernando CappaStephani, Rodrigo2020-10-01info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersionapplication/pdfhttps://www.revistadoilct.com.br/rilct/article/view/75510.14295/2238-6416.v75i1.755Journal of Candido Tostes Dairy Institute; v. 75, n. 1 (2020); 10-21Revista do Instituto de Laticínios Cândido Tostes; v. 75, n. 1 (2020); 10-212238-64160100-3674reponame:Revista do Instituto de Laticínios Cândido Tostesinstname:Empresa de Pesquisa Agropecuária de Minas Gerais (EPAMIG)instacron:EPAMIGporhttps://www.revistadoilct.com.br/rilct/article/view/755/522Direitos autorais 2020 Revista do Instituto de Laticínios Cândido Tosteshttp://creativecommons.org/licenses/by/4.0info:eu-repo/semantics/openAccess2020-10-01T04:24:04Zoai:oai.rilct.emnuvens.com.br:article/755Revistahttp://www.revistadoilct.com.br/ONGhttps://www.revistadoilct.com.br/rilct/oai||revistadoilct@epamig.br|| revistadoilct@oi.com.br2238-64160100-3674opendoar:2020-10-01T04:24:04Revista do Instituto de Laticínios Cândido Tostes - Empresa de Pesquisa Agropecuária de Minas Gerais (EPAMIG)false
dc.title.none.fl_str_mv Characterization of the particles surface of dried dairy products
Caracterização da superfície de partículas de produtos lácteos desidratados
title Characterization of the particles surface of dried dairy products
spellingShingle Characterization of the particles surface of dried dairy products
Toledo, Paulo Henrique de Melo
energy dispersive spectroscopy; Raman mapping; scanning electron microscopy.
Físico química, química de lácteos; Concentrados, desidratados, soro
espectroscopia por energia dispersiva; mapeamento Raman; microscopia eletrônica de varredura.
title_short Characterization of the particles surface of dried dairy products
title_full Characterization of the particles surface of dried dairy products
title_fullStr Characterization of the particles surface of dried dairy products
title_full_unstemmed Characterization of the particles surface of dried dairy products
title_sort Characterization of the particles surface of dried dairy products
author Toledo, Paulo Henrique de Melo
author_facet Toledo, Paulo Henrique de Melo
Pereira, João Pablo Fortes
Perrone, Ítalo Tuler
Carvalho, Antônio Fernandes
Oliveira, Luiz Fernando Cappa
Stephani, Rodrigo
author_role author
author2 Pereira, João Pablo Fortes
Perrone, Ítalo Tuler
Carvalho, Antônio Fernandes
Oliveira, Luiz Fernando Cappa
Stephani, Rodrigo
author2_role author
author
author
author
author
dc.contributor.none.fl_str_mv
CNPq, CAPES e FAPEMIG
dc.contributor.author.fl_str_mv Toledo, Paulo Henrique de Melo
Pereira, João Pablo Fortes
Perrone, Ítalo Tuler
Carvalho, Antônio Fernandes
Oliveira, Luiz Fernando Cappa
Stephani, Rodrigo
dc.subject.none.fl_str_mv
dc.subject.por.fl_str_mv energy dispersive spectroscopy; Raman mapping; scanning electron microscopy.
Físico química, química de lácteos; Concentrados, desidratados, soro
espectroscopia por energia dispersiva; mapeamento Raman; microscopia eletrônica de varredura.
topic energy dispersive spectroscopy; Raman mapping; scanning electron microscopy.
Físico química, química de lácteos; Concentrados, desidratados, soro
espectroscopia por energia dispersiva; mapeamento Raman; microscopia eletrônica de varredura.
description During production or storage of dehydrated dairy products, milk constituents may undergo redistribution, resulting in heterogeneity between the surface and its interior. The main objective of this work was to map the surfaces of different dehydrated dairy products, with the combined use of Raman spectroscopy and scanning electron microscopy (SEM) coupled with energy dispersive spectroscopy (EDS). It was intended to characterize the surfaces of the particles of interest in both instruments and to perform the mapping of these, within specific populations. The proposal to combine different techniques aimed, in addition to obtaining complementary data, to show that it is possible to advance in the research of dairy products when analyzing the particles under different analytical perspectives. All analyzes were carried out from industrialized products with lots, manufacture and validity dates monitored. From the spectroscopic profiles of the particles, it was possible to verify differences when the set of particles was analyzed, as well the target particles alone. It was possible to perform the characterization of the particles using different analytical techniques providing a data set that expands information about the particles of the dairy powders analyzed.
publishDate 2020
dc.date.none.fl_str_mv 2020-10-01
dc.type.none.fl_str_mv
dc.type.driver.fl_str_mv info:eu-repo/semantics/article
info:eu-repo/semantics/publishedVersion
format article
status_str publishedVersion
dc.identifier.uri.fl_str_mv https://www.revistadoilct.com.br/rilct/article/view/755
10.14295/2238-6416.v75i1.755
url https://www.revistadoilct.com.br/rilct/article/view/755
identifier_str_mv 10.14295/2238-6416.v75i1.755
dc.language.iso.fl_str_mv por
language por
dc.relation.none.fl_str_mv https://www.revistadoilct.com.br/rilct/article/view/755/522
dc.rights.driver.fl_str_mv Direitos autorais 2020 Revista do Instituto de Laticínios Cândido Tostes
http://creativecommons.org/licenses/by/4.0
info:eu-repo/semantics/openAccess
rights_invalid_str_mv Direitos autorais 2020 Revista do Instituto de Laticínios Cândido Tostes
http://creativecommons.org/licenses/by/4.0
eu_rights_str_mv openAccess
dc.format.none.fl_str_mv application/pdf
dc.publisher.none.fl_str_mv ILCT
publisher.none.fl_str_mv ILCT
dc.source.none.fl_str_mv Journal of Candido Tostes Dairy Institute; v. 75, n. 1 (2020); 10-21
Revista do Instituto de Laticínios Cândido Tostes; v. 75, n. 1 (2020); 10-21
2238-6416
0100-3674
reponame:Revista do Instituto de Laticínios Cândido Tostes
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instname_str Empresa de Pesquisa Agropecuária de Minas Gerais (EPAMIG)
instacron_str EPAMIG
institution EPAMIG
reponame_str Revista do Instituto de Laticínios Cândido Tostes
collection Revista do Instituto de Laticínios Cândido Tostes
repository.name.fl_str_mv Revista do Instituto de Laticínios Cândido Tostes - Empresa de Pesquisa Agropecuária de Minas Gerais (EPAMIG)
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