Thermal and chemical characterization of Dicksonia sellowiana extract by means of thermal analysis.

Detalhes bibliográficos
Autor(a) principal: MALUCELLI, L. C.
Data de Publicação: 2018
Outros Autores: MASSULO, T., MAGALHAES, W. L. E., STOFELLA, N. C. F., VASCONCELOS, E. C., CARVALHO FILHO, M. A. S., MURAKAMI, F. S.
Tipo de documento: Artigo
Idioma: eng
Título da fonte: Repositório Institucional da EMBRAPA (Repository Open Access to Scientific Information from EMBRAPA - Alice)
Texto Completo: http://www.alice.cnptia.embrapa.br/alice/handle/doc/1110898
Resumo: Dicksonia sellowiana Hook., Dicksoniaceae, is a tree-fern which is being recently used in medicine mainly for its phytotherapic activities. While several other studies have focused on D. sellowiana extract characterization in terms of its biological and antioxidant activity, the novelty of this work aims to understand the fate of this extract during thermal disposal through thermogravimetry/differential thermal analysis, thermogravimetry/mass spectrometry, Fourier transform infrared spectroscopy and elemental analysis, to further characterize this plant?s extract. Thermal analysis revealed mass loss within three welldefined steps, with the respective mass signals represented generated during heating. Light-volatiles were released during the first step, with release of NO2, CO2, and ethanol in the following, as a result of extract pyrolytic decomposition. Furthermore, mass signals variation during heating indicated the release of harmless by products in contrast to other pharmaceutical and personal care products. Finally, chemical characterization confirmed the observed under thermal analysis suggesting a highly polar structure within extract?s composition.
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spelling Thermal and chemical characterization of Dicksonia sellowiana extract by means of thermal analysis.Thermal behavior pyrolysisThermal disposalTG-MSPharmaceutical excipientsPyrolisisSpectometryCompatibilityPiróliseEspectometriaTermogravimetriaDicksonia sellowianaThermogravimetryDicksonia sellowiana Hook., Dicksoniaceae, is a tree-fern which is being recently used in medicine mainly for its phytotherapic activities. While several other studies have focused on D. sellowiana extract characterization in terms of its biological and antioxidant activity, the novelty of this work aims to understand the fate of this extract during thermal disposal through thermogravimetry/differential thermal analysis, thermogravimetry/mass spectrometry, Fourier transform infrared spectroscopy and elemental analysis, to further characterize this plant?s extract. Thermal analysis revealed mass loss within three welldefined steps, with the respective mass signals represented generated during heating. Light-volatiles were released during the first step, with release of NO2, CO2, and ethanol in the following, as a result of extract pyrolytic decomposition. Furthermore, mass signals variation during heating indicated the release of harmless by products in contrast to other pharmaceutical and personal care products. Finally, chemical characterization confirmed the observed under thermal analysis suggesting a highly polar structure within extract?s composition.Lucca C. Malucelli, Programa de Pós-graduação em Gestão Ambiental, Universidade Positivo; Tadeu Massulo, Programa de Pós-graduação em Biotecnologia Industrial, Universidade Positivo; WASHINGTON LUIZ ESTEVES MAGALHAES, CNPF; Nayana C. F. Stofella, Programa de Pós-graduação em Ciências Farmacêuticas, Universidade Federal do Paraná; Eliane C. Vasconcelos, Programa de Pós-graduação, Universidade Positivo; Marco Aurélio S. Carvalho Filho, Programa de Pós-graduação, Universidade Positivo; Fábio S. Murakami, Programa de Pós-graduação em Ciências Farmacêuticas, Universidade Federal do Paraná.MALUCELLI, L. C.MASSULO, T.MAGALHAES, W. L. E.STOFELLA, N. C. F.VASCONCELOS, E. C.CARVALHO FILHO, M. A. S.MURAKAMI, F. S.2019-07-27T00:53:14Z2019-07-27T00:53:14Z2019-07-2620182019-07-27T00:53:14Zinfo:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/articleRevista Brasileira de Farmacognosia, v. 28, p. 626-630, 2018.http://www.alice.cnptia.embrapa.br/alice/handle/doc/111089810.1016/j.bjp.2018.07.001enginfo:eu-repo/semantics/openAccessreponame:Repositório Institucional da EMBRAPA (Repository Open Access to Scientific Information from EMBRAPA - Alice)instname:Empresa Brasileira de Pesquisa Agropecuária (Embrapa)instacron:EMBRAPA2019-07-27T00:53:22Zoai:www.alice.cnptia.embrapa.br:doc/1110898Repositório InstitucionalPUBhttps://www.alice.cnptia.embrapa.br/oai/requestopendoar:21542019-07-27T00:53:22falseRepositório InstitucionalPUBhttps://www.alice.cnptia.embrapa.br/oai/requestcg-riaa@embrapa.bropendoar:21542019-07-27T00:53:22Repositório Institucional da EMBRAPA (Repository Open Access to Scientific Information from EMBRAPA - Alice) - Empresa Brasileira de Pesquisa Agropecuária (Embrapa)false
dc.title.none.fl_str_mv Thermal and chemical characterization of Dicksonia sellowiana extract by means of thermal analysis.
title Thermal and chemical characterization of Dicksonia sellowiana extract by means of thermal analysis.
spellingShingle Thermal and chemical characterization of Dicksonia sellowiana extract by means of thermal analysis.
MALUCELLI, L. C.
Thermal behavior pyrolysis
Thermal disposal
TG-MS
Pharmaceutical excipients
Pyrolisis
Spectometry
Compatibility
Pirólise
Espectometria
Termogravimetria
Dicksonia sellowiana
Thermogravimetry
title_short Thermal and chemical characterization of Dicksonia sellowiana extract by means of thermal analysis.
title_full Thermal and chemical characterization of Dicksonia sellowiana extract by means of thermal analysis.
title_fullStr Thermal and chemical characterization of Dicksonia sellowiana extract by means of thermal analysis.
title_full_unstemmed Thermal and chemical characterization of Dicksonia sellowiana extract by means of thermal analysis.
title_sort Thermal and chemical characterization of Dicksonia sellowiana extract by means of thermal analysis.
author MALUCELLI, L. C.
author_facet MALUCELLI, L. C.
MASSULO, T.
MAGALHAES, W. L. E.
STOFELLA, N. C. F.
VASCONCELOS, E. C.
CARVALHO FILHO, M. A. S.
MURAKAMI, F. S.
author_role author
author2 MASSULO, T.
MAGALHAES, W. L. E.
STOFELLA, N. C. F.
VASCONCELOS, E. C.
CARVALHO FILHO, M. A. S.
MURAKAMI, F. S.
author2_role author
author
author
author
author
author
dc.contributor.none.fl_str_mv Lucca C. Malucelli, Programa de Pós-graduação em Gestão Ambiental, Universidade Positivo; Tadeu Massulo, Programa de Pós-graduação em Biotecnologia Industrial, Universidade Positivo; WASHINGTON LUIZ ESTEVES MAGALHAES, CNPF; Nayana C. F. Stofella, Programa de Pós-graduação em Ciências Farmacêuticas, Universidade Federal do Paraná; Eliane C. Vasconcelos, Programa de Pós-graduação, Universidade Positivo; Marco Aurélio S. Carvalho Filho, Programa de Pós-graduação, Universidade Positivo; Fábio S. Murakami, Programa de Pós-graduação em Ciências Farmacêuticas, Universidade Federal do Paraná.
dc.contributor.author.fl_str_mv MALUCELLI, L. C.
MASSULO, T.
MAGALHAES, W. L. E.
STOFELLA, N. C. F.
VASCONCELOS, E. C.
CARVALHO FILHO, M. A. S.
MURAKAMI, F. S.
dc.subject.por.fl_str_mv Thermal behavior pyrolysis
Thermal disposal
TG-MS
Pharmaceutical excipients
Pyrolisis
Spectometry
Compatibility
Pirólise
Espectometria
Termogravimetria
Dicksonia sellowiana
Thermogravimetry
topic Thermal behavior pyrolysis
Thermal disposal
TG-MS
Pharmaceutical excipients
Pyrolisis
Spectometry
Compatibility
Pirólise
Espectometria
Termogravimetria
Dicksonia sellowiana
Thermogravimetry
description Dicksonia sellowiana Hook., Dicksoniaceae, is a tree-fern which is being recently used in medicine mainly for its phytotherapic activities. While several other studies have focused on D. sellowiana extract characterization in terms of its biological and antioxidant activity, the novelty of this work aims to understand the fate of this extract during thermal disposal through thermogravimetry/differential thermal analysis, thermogravimetry/mass spectrometry, Fourier transform infrared spectroscopy and elemental analysis, to further characterize this plant?s extract. Thermal analysis revealed mass loss within three welldefined steps, with the respective mass signals represented generated during heating. Light-volatiles were released during the first step, with release of NO2, CO2, and ethanol in the following, as a result of extract pyrolytic decomposition. Furthermore, mass signals variation during heating indicated the release of harmless by products in contrast to other pharmaceutical and personal care products. Finally, chemical characterization confirmed the observed under thermal analysis suggesting a highly polar structure within extract?s composition.
publishDate 2018
dc.date.none.fl_str_mv 2018
2019-07-27T00:53:14Z
2019-07-27T00:53:14Z
2019-07-26
2019-07-27T00:53:14Z
dc.type.driver.fl_str_mv info:eu-repo/semantics/publishedVersion
info:eu-repo/semantics/article
format article
status_str publishedVersion
dc.identifier.uri.fl_str_mv Revista Brasileira de Farmacognosia, v. 28, p. 626-630, 2018.
http://www.alice.cnptia.embrapa.br/alice/handle/doc/1110898
10.1016/j.bjp.2018.07.001
identifier_str_mv Revista Brasileira de Farmacognosia, v. 28, p. 626-630, 2018.
10.1016/j.bjp.2018.07.001
url http://www.alice.cnptia.embrapa.br/alice/handle/doc/1110898
dc.language.iso.fl_str_mv eng
language eng
dc.rights.driver.fl_str_mv info:eu-repo/semantics/openAccess
eu_rights_str_mv openAccess
dc.source.none.fl_str_mv reponame:Repositório Institucional da EMBRAPA (Repository Open Access to Scientific Information from EMBRAPA - Alice)
instname:Empresa Brasileira de Pesquisa Agropecuária (Embrapa)
instacron:EMBRAPA
instname_str Empresa Brasileira de Pesquisa Agropecuária (Embrapa)
instacron_str EMBRAPA
institution EMBRAPA
reponame_str Repositório Institucional da EMBRAPA (Repository Open Access to Scientific Information from EMBRAPA - Alice)
collection Repositório Institucional da EMBRAPA (Repository Open Access to Scientific Information from EMBRAPA - Alice)
repository.name.fl_str_mv Repositório Institucional da EMBRAPA (Repository Open Access to Scientific Information from EMBRAPA - Alice) - Empresa Brasileira de Pesquisa Agropecuária (Embrapa)
repository.mail.fl_str_mv cg-riaa@embrapa.br
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