Sorption isothermes and physicochemical characterization of dried milk products

Detalhes bibliográficos
Autor(a) principal: Perrone, Ítalo Tuler
Data de Publicação: 2013
Outros Autores: Renhe, Isis Rodrigues Toledo, Pereira, Danielle Braga Chelini, Silva, Paulo Henrique Fonseca da, Carvalho, Antônio Fernandes de
Tipo de documento: Artigo
Idioma: por
Título da fonte: Revista do Instituto de Laticínios Cândido Tostes
Texto Completo: https://www.revistadoilct.com.br/rilct/article/view/48
Resumo: The aim of this study was to determine the composition, establish the isotherms at 25 º C and apply the BET model for instant whole milk powder (LPI), instant skim milk powder (SMP), half skim milk powder (LPSD), pre-crystallized whole whey by primary nucleation (SPNP), pre-crystallized whole whey by adding 0.05% w / w of lactose (SP0, 05) and pre-crystallized whole whey by adding 0.1% w / w lactose (SP0,1). The Brunauer, Emmett and Teller (BET) model was utilized for analysis of the experimental data. Isotherms of the dried milk products evaluated were fitted to the BET model and the moisture contents were higher than those calculated for the monolayer. Water mass in the monolayer calculated by the BET model presented a statistically significant negative correlation (p=0.026) with the fat concentrations. The difference between enthalpy of adsorption in the monolayer and enthalpy of water condensation between water molecules in the monolayer and in the pure solvent presented statistically significant positive correlations with the concentrations of lactose (p=0.001) and negative correlations with moisture content (p=0.005).
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spelling Sorption isothermes and physicochemical characterization of dried milk productsIsotermas de sorção e caracterização físico-química de lácteos desidratadoslactose; crystallization; BET.lactose; cristalização; BET.The aim of this study was to determine the composition, establish the isotherms at 25 º C and apply the BET model for instant whole milk powder (LPI), instant skim milk powder (SMP), half skim milk powder (LPSD), pre-crystallized whole whey by primary nucleation (SPNP), pre-crystallized whole whey by adding 0.05% w / w of lactose (SP0, 05) and pre-crystallized whole whey by adding 0.1% w / w lactose (SP0,1). The Brunauer, Emmett and Teller (BET) model was utilized for analysis of the experimental data. Isotherms of the dried milk products evaluated were fitted to the BET model and the moisture contents were higher than those calculated for the monolayer. Water mass in the monolayer calculated by the BET model presented a statistically significant negative correlation (p=0.026) with the fat concentrations. The difference between enthalpy of adsorption in the monolayer and enthalpy of water condensation between water molecules in the monolayer and in the pure solvent presented statistically significant positive correlations with the concentrations of lactose (p=0.001) and negative correlations with moisture content (p=0.005).O objetivo deste trabalho foi determinar a composição centesimal, construir as isotermas a 25 ºC e aplicar o modelo de BET para leite em pó instantâneo integral (LPI), leite em pó instantâneo desnatado (LPD), leite em pó semidesnatado (LPSD), soro em pó integral pré-cristalizado por nucleação primária (SPNP), soro em pó integral pré-cristalizado por adição de 0,05 % m/m de lactose (SP0,05) e soro em pó pré cristalizado por adição de 0,1 % m/m de lactose (SP0,1). As isotermas dos lácteos desidratados estudados se ajustaram ao modelo de BET e os teores de umidade estão acima dos calculados para a monocamada. A massa de água na monocamada calculada pelo modelo de BET apresenta correlação negativa (p=0,026) estaticamente significativa com os teores de gordura dos pós. A diferença de entalpia de adsorção entre as moléculas de água na monocamada e no solvente puro apresentou correlação positiva estatisticamente significativa com os teores de lactose (p=0,001) e correlação negativa com os teores de umidade dos pós (p=0,005). ILCTPerrone, Ítalo TulerRenhe, Isis Rodrigues ToledoPereira, Danielle Braga CheliniSilva, Paulo Henrique Fonseca daCarvalho, Antônio Fernandes de2013-12-18info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersionapplication/pdfhttps://www.revistadoilct.com.br/rilct/article/view/4810.5935/2238-6416.20130046Journal of Candido Tostes Dairy Institute; v. 68, n. 395 (2013); 33-38Revista do Instituto de Laticínios Cândido Tostes; v. 68, n. 395 (2013); 33-382238-64160100-3674reponame:Revista do Instituto de Laticínios Cândido Tostesinstname:Empresa de Pesquisa Agropecuária de Minas Gerais (EPAMIG)instacron:EPAMIGporhttps://www.revistadoilct.com.br/rilct/article/view/48/54Direitos autorais 2014 Revista do Instituto de Laticínios Cândido Tostesinfo:eu-repo/semantics/openAccess2014-02-27T10:17:49Zoai:oai.rilct.emnuvens.com.br:article/48Revistahttp://www.revistadoilct.com.br/ONGhttps://www.revistadoilct.com.br/rilct/oai||revistadoilct@epamig.br|| revistadoilct@oi.com.br2238-64160100-3674opendoar:2014-02-27T10:17:49Revista do Instituto de Laticínios Cândido Tostes - Empresa de Pesquisa Agropecuária de Minas Gerais (EPAMIG)false
dc.title.none.fl_str_mv Sorption isothermes and physicochemical characterization of dried milk products
Isotermas de sorção e caracterização físico-química de lácteos desidratados
title Sorption isothermes and physicochemical characterization of dried milk products
spellingShingle Sorption isothermes and physicochemical characterization of dried milk products
Perrone, Ítalo Tuler
lactose; crystallization; BET.
lactose; cristalização; BET.
title_short Sorption isothermes and physicochemical characterization of dried milk products
title_full Sorption isothermes and physicochemical characterization of dried milk products
title_fullStr Sorption isothermes and physicochemical characterization of dried milk products
title_full_unstemmed Sorption isothermes and physicochemical characterization of dried milk products
title_sort Sorption isothermes and physicochemical characterization of dried milk products
author Perrone, Ítalo Tuler
author_facet Perrone, Ítalo Tuler
Renhe, Isis Rodrigues Toledo
Pereira, Danielle Braga Chelini
Silva, Paulo Henrique Fonseca da
Carvalho, Antônio Fernandes de
author_role author
author2 Renhe, Isis Rodrigues Toledo
Pereira, Danielle Braga Chelini
Silva, Paulo Henrique Fonseca da
Carvalho, Antônio Fernandes de
author2_role author
author
author
author
dc.contributor.none.fl_str_mv

dc.contributor.author.fl_str_mv Perrone, Ítalo Tuler
Renhe, Isis Rodrigues Toledo
Pereira, Danielle Braga Chelini
Silva, Paulo Henrique Fonseca da
Carvalho, Antônio Fernandes de
dc.subject.none.fl_str_mv

dc.subject.por.fl_str_mv lactose; crystallization; BET.
lactose; cristalização; BET.
topic lactose; crystallization; BET.
lactose; cristalização; BET.
description The aim of this study was to determine the composition, establish the isotherms at 25 º C and apply the BET model for instant whole milk powder (LPI), instant skim milk powder (SMP), half skim milk powder (LPSD), pre-crystallized whole whey by primary nucleation (SPNP), pre-crystallized whole whey by adding 0.05% w / w of lactose (SP0, 05) and pre-crystallized whole whey by adding 0.1% w / w lactose (SP0,1). The Brunauer, Emmett and Teller (BET) model was utilized for analysis of the experimental data. Isotherms of the dried milk products evaluated were fitted to the BET model and the moisture contents were higher than those calculated for the monolayer. Water mass in the monolayer calculated by the BET model presented a statistically significant negative correlation (p=0.026) with the fat concentrations. The difference between enthalpy of adsorption in the monolayer and enthalpy of water condensation between water molecules in the monolayer and in the pure solvent presented statistically significant positive correlations with the concentrations of lactose (p=0.001) and negative correlations with moisture content (p=0.005).
publishDate 2013
dc.date.none.fl_str_mv 2013-12-18
dc.type.none.fl_str_mv


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10.5935/2238-6416.20130046
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identifier_str_mv 10.5935/2238-6416.20130046
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dc.relation.none.fl_str_mv https://www.revistadoilct.com.br/rilct/article/view/48/54
dc.rights.driver.fl_str_mv Direitos autorais 2014 Revista do Instituto de Laticínios Cândido Tostes
info:eu-repo/semantics/openAccess
rights_invalid_str_mv Direitos autorais 2014 Revista do Instituto de Laticínios Cândido Tostes
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dc.publisher.none.fl_str_mv ILCT
publisher.none.fl_str_mv ILCT
dc.source.none.fl_str_mv Journal of Candido Tostes Dairy Institute; v. 68, n. 395 (2013); 33-38
Revista do Instituto de Laticínios Cândido Tostes; v. 68, n. 395 (2013); 33-38
2238-6416
0100-3674
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