Sorption isothermes and physicochemical characterization of dried milk products
Autor(a) principal: | |
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Data de Publicação: | 2013 |
Outros Autores: | , , , |
Tipo de documento: | Artigo |
Idioma: | por |
Título da fonte: | Revista do Instituto de Laticínios Cândido Tostes |
Texto Completo: | https://www.revistadoilct.com.br/rilct/article/view/48 |
Resumo: | The aim of this study was to determine the composition, establish the isotherms at 25 º C and apply the BET model for instant whole milk powder (LPI), instant skim milk powder (SMP), half skim milk powder (LPSD), pre-crystallized whole whey by primary nucleation (SPNP), pre-crystallized whole whey by adding 0.05% w / w of lactose (SP0, 05) and pre-crystallized whole whey by adding 0.1% w / w lactose (SP0,1). The Brunauer, Emmett and Teller (BET) model was utilized for analysis of the experimental data. Isotherms of the dried milk products evaluated were fitted to the BET model and the moisture contents were higher than those calculated for the monolayer. Water mass in the monolayer calculated by the BET model presented a statistically significant negative correlation (p=0.026) with the fat concentrations. The difference between enthalpy of adsorption in the monolayer and enthalpy of water condensation between water molecules in the monolayer and in the pure solvent presented statistically significant positive correlations with the concentrations of lactose (p=0.001) and negative correlations with moisture content (p=0.005). |
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Sorption isothermes and physicochemical characterization of dried milk productsIsotermas de sorção e caracterização físico-química de lácteos desidratadoslactose; crystallization; BET.lactose; cristalização; BET.The aim of this study was to determine the composition, establish the isotherms at 25 º C and apply the BET model for instant whole milk powder (LPI), instant skim milk powder (SMP), half skim milk powder (LPSD), pre-crystallized whole whey by primary nucleation (SPNP), pre-crystallized whole whey by adding 0.05% w / w of lactose (SP0, 05) and pre-crystallized whole whey by adding 0.1% w / w lactose (SP0,1). The Brunauer, Emmett and Teller (BET) model was utilized for analysis of the experimental data. Isotherms of the dried milk products evaluated were fitted to the BET model and the moisture contents were higher than those calculated for the monolayer. Water mass in the monolayer calculated by the BET model presented a statistically significant negative correlation (p=0.026) with the fat concentrations. The difference between enthalpy of adsorption in the monolayer and enthalpy of water condensation between water molecules in the monolayer and in the pure solvent presented statistically significant positive correlations with the concentrations of lactose (p=0.001) and negative correlations with moisture content (p=0.005).O objetivo deste trabalho foi determinar a composição centesimal, construir as isotermas a 25 ºC e aplicar o modelo de BET para leite em pó instantâneo integral (LPI), leite em pó instantâneo desnatado (LPD), leite em pó semidesnatado (LPSD), soro em pó integral pré-cristalizado por nucleação primária (SPNP), soro em pó integral pré-cristalizado por adição de 0,05 % m/m de lactose (SP0,05) e soro em pó pré cristalizado por adição de 0,1 % m/m de lactose (SP0,1). As isotermas dos lácteos desidratados estudados se ajustaram ao modelo de BET e os teores de umidade estão acima dos calculados para a monocamada. A massa de água na monocamada calculada pelo modelo de BET apresenta correlação negativa (p=0,026) estaticamente significativa com os teores de gordura dos pós. A diferença de entalpia de adsorção entre as moléculas de água na monocamada e no solvente puro apresentou correlação positiva estatisticamente significativa com os teores de lactose (p=0,001) e correlação negativa com os teores de umidade dos pós (p=0,005). ILCTPerrone, Ítalo TulerRenhe, Isis Rodrigues ToledoPereira, Danielle Braga CheliniSilva, Paulo Henrique Fonseca daCarvalho, Antônio Fernandes de2013-12-18info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersionapplication/pdfhttps://www.revistadoilct.com.br/rilct/article/view/4810.5935/2238-6416.20130046Journal of Candido Tostes Dairy Institute; v. 68, n. 395 (2013); 33-38Revista do Instituto de Laticínios Cândido Tostes; v. 68, n. 395 (2013); 33-382238-64160100-3674reponame:Revista do Instituto de Laticínios Cândido Tostesinstname:Empresa de Pesquisa Agropecuária de Minas Gerais (EPAMIG)instacron:EPAMIGporhttps://www.revistadoilct.com.br/rilct/article/view/48/54Direitos autorais 2014 Revista do Instituto de Laticínios Cândido Tostesinfo:eu-repo/semantics/openAccess2014-02-27T10:17:49Zoai:oai.rilct.emnuvens.com.br:article/48Revistahttp://www.revistadoilct.com.br/ONGhttps://www.revistadoilct.com.br/rilct/oai||revistadoilct@epamig.br|| revistadoilct@oi.com.br2238-64160100-3674opendoar:2014-02-27T10:17:49Revista do Instituto de Laticínios Cândido Tostes - Empresa de Pesquisa Agropecuária de Minas Gerais (EPAMIG)false |
dc.title.none.fl_str_mv |
Sorption isothermes and physicochemical characterization of dried milk products Isotermas de sorção e caracterização físico-química de lácteos desidratados |
title |
Sorption isothermes and physicochemical characterization of dried milk products |
spellingShingle |
Sorption isothermes and physicochemical characterization of dried milk products Perrone, Ítalo Tuler lactose; crystallization; BET. lactose; cristalização; BET. |
title_short |
Sorption isothermes and physicochemical characterization of dried milk products |
title_full |
Sorption isothermes and physicochemical characterization of dried milk products |
title_fullStr |
Sorption isothermes and physicochemical characterization of dried milk products |
title_full_unstemmed |
Sorption isothermes and physicochemical characterization of dried milk products |
title_sort |
Sorption isothermes and physicochemical characterization of dried milk products |
author |
Perrone, Ítalo Tuler |
author_facet |
Perrone, Ítalo Tuler Renhe, Isis Rodrigues Toledo Pereira, Danielle Braga Chelini Silva, Paulo Henrique Fonseca da Carvalho, Antônio Fernandes de |
author_role |
author |
author2 |
Renhe, Isis Rodrigues Toledo Pereira, Danielle Braga Chelini Silva, Paulo Henrique Fonseca da Carvalho, Antônio Fernandes de |
author2_role |
author author author author |
dc.contributor.none.fl_str_mv |
|
dc.contributor.author.fl_str_mv |
Perrone, Ítalo Tuler Renhe, Isis Rodrigues Toledo Pereira, Danielle Braga Chelini Silva, Paulo Henrique Fonseca da Carvalho, Antônio Fernandes de |
dc.subject.none.fl_str_mv |
|
dc.subject.por.fl_str_mv |
lactose; crystallization; BET. lactose; cristalização; BET. |
topic |
lactose; crystallization; BET. lactose; cristalização; BET. |
description |
The aim of this study was to determine the composition, establish the isotherms at 25 º C and apply the BET model for instant whole milk powder (LPI), instant skim milk powder (SMP), half skim milk powder (LPSD), pre-crystallized whole whey by primary nucleation (SPNP), pre-crystallized whole whey by adding 0.05% w / w of lactose (SP0, 05) and pre-crystallized whole whey by adding 0.1% w / w lactose (SP0,1). The Brunauer, Emmett and Teller (BET) model was utilized for analysis of the experimental data. Isotherms of the dried milk products evaluated were fitted to the BET model and the moisture contents were higher than those calculated for the monolayer. Water mass in the monolayer calculated by the BET model presented a statistically significant negative correlation (p=0.026) with the fat concentrations. The difference between enthalpy of adsorption in the monolayer and enthalpy of water condensation between water molecules in the monolayer and in the pure solvent presented statistically significant positive correlations with the concentrations of lactose (p=0.001) and negative correlations with moisture content (p=0.005). |
publishDate |
2013 |
dc.date.none.fl_str_mv |
2013-12-18 |
dc.type.none.fl_str_mv |
|
dc.type.driver.fl_str_mv |
info:eu-repo/semantics/article info:eu-repo/semantics/publishedVersion |
format |
article |
status_str |
publishedVersion |
dc.identifier.uri.fl_str_mv |
https://www.revistadoilct.com.br/rilct/article/view/48 10.5935/2238-6416.20130046 |
url |
https://www.revistadoilct.com.br/rilct/article/view/48 |
identifier_str_mv |
10.5935/2238-6416.20130046 |
dc.language.iso.fl_str_mv |
por |
language |
por |
dc.relation.none.fl_str_mv |
https://www.revistadoilct.com.br/rilct/article/view/48/54 |
dc.rights.driver.fl_str_mv |
Direitos autorais 2014 Revista do Instituto de Laticínios Cândido Tostes info:eu-repo/semantics/openAccess |
rights_invalid_str_mv |
Direitos autorais 2014 Revista do Instituto de Laticínios Cândido Tostes |
eu_rights_str_mv |
openAccess |
dc.format.none.fl_str_mv |
application/pdf |
dc.publisher.none.fl_str_mv |
ILCT |
publisher.none.fl_str_mv |
ILCT |
dc.source.none.fl_str_mv |
Journal of Candido Tostes Dairy Institute; v. 68, n. 395 (2013); 33-38 Revista do Instituto de Laticínios Cândido Tostes; v. 68, n. 395 (2013); 33-38 2238-6416 0100-3674 reponame:Revista do Instituto de Laticínios Cândido Tostes instname:Empresa de Pesquisa Agropecuária de Minas Gerais (EPAMIG) instacron:EPAMIG |
instname_str |
Empresa de Pesquisa Agropecuária de Minas Gerais (EPAMIG) |
instacron_str |
EPAMIG |
institution |
EPAMIG |
reponame_str |
Revista do Instituto de Laticínios Cândido Tostes |
collection |
Revista do Instituto de Laticínios Cândido Tostes |
repository.name.fl_str_mv |
Revista do Instituto de Laticínios Cândido Tostes - Empresa de Pesquisa Agropecuária de Minas Gerais (EPAMIG) |
repository.mail.fl_str_mv |
||revistadoilct@epamig.br|| revistadoilct@oi.com.br |
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1809738129026842624 |