Evaluation of the analytical methodology for the determination of arsenic, cadmium and lead in coffee samples, according to Codex Alimentarius acceptance criteria: Vigil Sanit Debate, Rio de Janeiro, 2024, v.12: e02192 | Published on: 15/03/2024
Autor(a) principal: | |
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Data de Publicação: | 2024 |
Outros Autores: | , , , , |
Tipo de documento: | Artigo |
Idioma: | por |
Título da fonte: | Vigilância Sanitária em Debate |
Texto Completo: | https://visaemdebate.incqs.fiocruz.br/index.php/visaemdebate/article/view/2192 |
Resumo: | Introduction: The Codex Alimentarius establishes international standards in the food segments to protect the health of consumers and ensure legal trade practices between countries. INMETRO, on the other hand, provides guidance documents that help laboratories carry out the validation of analytical methodology. These documents are used as a criteria to validate and verify conformity of the methods applied to determine contamination and residues in different products. Objective: To evaluate the validatedanalytical methodology used to determine arsenic, cadmium and lead in samples of roasted coffee powder according to the acceptance criteria recommended in the Codex Alimentarius 27th edition procedure manual. Method: This is an observational study of the descriptive exploratory qualitative type using secondary data base. Results: With the reading of the Codex Alimentarius, the parameters used were established, namely, the minimum application range, the detection limit, the quantification limit, precision and accuracy. Thus, the evaluation of the validated methodology was carried out and it was verified that it is applicable for the analysis of As, Cd and Pb in samples of roasted coffee powder. Conclusions: Current Brazilian legislation aimed at controlling the presence of contaminants in food establishes the maximum tolerated limits for As, Cd and Pb, but does not define which methodologies should be used to verify the presence and concentration of these elements. Therefore, the methodology presented in this study is adequate to control the quality of roasted coffee powder regarding the presence of these inorganic contaminants, thus contributing to the protection and safety of the population. |
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Evaluation of the analytical methodology for the determination of arsenic, cadmium and lead in coffee samples, according to Codex Alimentarius acceptance criteria: Vigil Sanit Debate, Rio de Janeiro, 2024, v.12: e02192 | Published on: 15/03/2024Avaliação da metodologia analítica para determinação de arsênio, cádmio e chumbo em amostras de café, segundo os critérios de aceitação do Codex Alimentarius: Vigil Sanit Debate, Rio de Janeiro, 2024, v.12: e02192| Publicado em: 15/03/2024Codex AlimentariusInmetroParâmetros de ValidaçãoCafé Torrado em PóCodex AlimentariusInmetroValidation ParametersRoasted Coffee PowderIntroduction: The Codex Alimentarius establishes international standards in the food segments to protect the health of consumers and ensure legal trade practices between countries. INMETRO, on the other hand, provides guidance documents that help laboratories carry out the validation of analytical methodology. These documents are used as a criteria to validate and verify conformity of the methods applied to determine contamination and residues in different products. Objective: To evaluate the validatedanalytical methodology used to determine arsenic, cadmium and lead in samples of roasted coffee powder according to the acceptance criteria recommended in the Codex Alimentarius 27th edition procedure manual. Method: This is an observational study of the descriptive exploratory qualitative type using secondary data base. Results: With the reading of the Codex Alimentarius, the parameters used were established, namely, the minimum application range, the detection limit, the quantification limit, precision and accuracy. Thus, the evaluation of the validated methodology was carried out and it was verified that it is applicable for the analysis of As, Cd and Pb in samples of roasted coffee powder. Conclusions: Current Brazilian legislation aimed at controlling the presence of contaminants in food establishes the maximum tolerated limits for As, Cd and Pb, but does not define which methodologies should be used to verify the presence and concentration of these elements. Therefore, the methodology presented in this study is adequate to control the quality of roasted coffee powder regarding the presence of these inorganic contaminants, thus contributing to the protection and safety of the population.Introdução: O Codex Alimentarius estabelece normas internacionais na área de alimentos para proteger a saúde dos consumidores e garantir práticas legais de comércio entre os países. O Instituto Nacional de Metrologia, Qualidade e Tecnologia (Inmetro) disponibiliza documentos orientativos que auxiliam os laboratórios a realizarem a validação de metodologias analíticas. Estas são utilizadas para estabelecer critérios de validação e verificação de conformidade dos métodos aplicados na determinação dos níveis de contaminantes e resíduos em produtos de interesse sanitário. Objetivo: Avaliar a metodologia analítica validada utilizada para determinação de arsênio, cádmio e chumbo em amostras de café torrado em pó segundo os critérios de aceitação preconizados no Manual de Procedimentos do Codex Alimentarius 27ª edição. Método: Trata-se de um estudo observacional do tipo descritivo exploratório qualitativo utilizando base de dados secundários. Resultados: Com a leitura do Codex Alimentarius, foram estabelecidos os parâmetros utilizados, sendo eles, a faixa mínima de aplicação, o limite de detecção, o limite de quantificação, a precisão e a exatidão. Assim foi realizada a avaliação da metodologia validada e verificou-se que esta é aplicável para a análise de As, Cd e Pb em amostras de café torrado em pó. Conclusões: A legislação brasileira atual voltada para o controle da presença de contaminantes em alimentos estabelece os limites máximo tolerados para As, Cd e Pb, mas não define quais metodologias devem ser utilizadas para verificar a presença e concentração destes elementos. Sendo assim, a metodologia apresentada nesse estudo é adequada para controlar a qualidade do café torrado em pó quanto a presença destes contaminantes inorgânicos, contribuindo assim para a proteção e a segurança da população.Instituto Nacional de Controle de Qualidade em Saúde2024-03-15info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersion"Peer-reviewed article""Artículo revisado por pares""Artigo avaliado pelos pares"application/pdfhttps://visaemdebate.incqs.fiocruz.br/index.php/visaemdebate/article/view/219210.22239/2317-269x.02192Health Surveillance under Debate: Society, Science & Technology ; v. 12 (2024) | Continuous publication; 1-5Vigilancia en Salud en Debate: Sociedad, Ciencia y Tecnología; v. 12 (2024) | Publicación continua; 1-5Vigil Sanit Debate, Rio de Janeiro; v. 12 (2024) | Publicação contínua; 1-52317-269Xreponame:Vigilância Sanitária em Debateinstname:Fundação Oswaldo Cruz (FIOCRUZ)instacron:FIOCRUZporhttps://visaemdebate.incqs.fiocruz.br/index.php/visaemdebate/article/view/2192/1632Copyright (c) 2024 Cristiane Barata-Silva, Carolina Duque Magalhães, Renata Aparecida Pereira, Santos Alves Vicentini Neto, Silvana Couto Jacob, Lisia Maria Gobbo dos Santos (Autor)https://creativecommons.org/licenses/by/4.0info:eu-repo/semantics/openAccessBarata-Silva, CristianeDuque Magalhães, CarolinaAparecida Pereira, RenataAlves Vicentini Neto, SantosCouto Jacob, SilvanaGobbo dos Santos, Lisia Maria2024-03-15T19:23:32Zoai:ojs.visaemdebate.incqs.fiocruz.br:article/2192Revistahttps://visaemdebate.incqs.fiocruz.br/index.php/visaemdebatePUBhttps://visaemdebate.incqs.fiocruz.br/index.php/visaemdebate/oaiincqs.visaemdebate@fiocruz.br || gisele.neves@fiocruz.br2317-269X2317-269Xopendoar:2024-03-15T19:23:32Vigilância Sanitária em Debate - Fundação Oswaldo Cruz (FIOCRUZ)false |
dc.title.none.fl_str_mv |
Evaluation of the analytical methodology for the determination of arsenic, cadmium and lead in coffee samples, according to Codex Alimentarius acceptance criteria: Vigil Sanit Debate, Rio de Janeiro, 2024, v.12: e02192 | Published on: 15/03/2024 Avaliação da metodologia analítica para determinação de arsênio, cádmio e chumbo em amostras de café, segundo os critérios de aceitação do Codex Alimentarius: Vigil Sanit Debate, Rio de Janeiro, 2024, v.12: e02192| Publicado em: 15/03/2024 |
title |
Evaluation of the analytical methodology for the determination of arsenic, cadmium and lead in coffee samples, according to Codex Alimentarius acceptance criteria: Vigil Sanit Debate, Rio de Janeiro, 2024, v.12: e02192 | Published on: 15/03/2024 |
spellingShingle |
Evaluation of the analytical methodology for the determination of arsenic, cadmium and lead in coffee samples, according to Codex Alimentarius acceptance criteria: Vigil Sanit Debate, Rio de Janeiro, 2024, v.12: e02192 | Published on: 15/03/2024 Barata-Silva, Cristiane Codex Alimentarius Inmetro Parâmetros de Validação Café Torrado em Pó Codex Alimentarius Inmetro Validation Parameters Roasted Coffee Powder |
title_short |
Evaluation of the analytical methodology for the determination of arsenic, cadmium and lead in coffee samples, according to Codex Alimentarius acceptance criteria: Vigil Sanit Debate, Rio de Janeiro, 2024, v.12: e02192 | Published on: 15/03/2024 |
title_full |
Evaluation of the analytical methodology for the determination of arsenic, cadmium and lead in coffee samples, according to Codex Alimentarius acceptance criteria: Vigil Sanit Debate, Rio de Janeiro, 2024, v.12: e02192 | Published on: 15/03/2024 |
title_fullStr |
Evaluation of the analytical methodology for the determination of arsenic, cadmium and lead in coffee samples, according to Codex Alimentarius acceptance criteria: Vigil Sanit Debate, Rio de Janeiro, 2024, v.12: e02192 | Published on: 15/03/2024 |
title_full_unstemmed |
Evaluation of the analytical methodology for the determination of arsenic, cadmium and lead in coffee samples, according to Codex Alimentarius acceptance criteria: Vigil Sanit Debate, Rio de Janeiro, 2024, v.12: e02192 | Published on: 15/03/2024 |
title_sort |
Evaluation of the analytical methodology for the determination of arsenic, cadmium and lead in coffee samples, according to Codex Alimentarius acceptance criteria: Vigil Sanit Debate, Rio de Janeiro, 2024, v.12: e02192 | Published on: 15/03/2024 |
author |
Barata-Silva, Cristiane |
author_facet |
Barata-Silva, Cristiane Duque Magalhães, Carolina Aparecida Pereira, Renata Alves Vicentini Neto, Santos Couto Jacob, Silvana Gobbo dos Santos, Lisia Maria |
author_role |
author |
author2 |
Duque Magalhães, Carolina Aparecida Pereira, Renata Alves Vicentini Neto, Santos Couto Jacob, Silvana Gobbo dos Santos, Lisia Maria |
author2_role |
author author author author author |
dc.contributor.author.fl_str_mv |
Barata-Silva, Cristiane Duque Magalhães, Carolina Aparecida Pereira, Renata Alves Vicentini Neto, Santos Couto Jacob, Silvana Gobbo dos Santos, Lisia Maria |
dc.subject.por.fl_str_mv |
Codex Alimentarius Inmetro Parâmetros de Validação Café Torrado em Pó Codex Alimentarius Inmetro Validation Parameters Roasted Coffee Powder |
topic |
Codex Alimentarius Inmetro Parâmetros de Validação Café Torrado em Pó Codex Alimentarius Inmetro Validation Parameters Roasted Coffee Powder |
description |
Introduction: The Codex Alimentarius establishes international standards in the food segments to protect the health of consumers and ensure legal trade practices between countries. INMETRO, on the other hand, provides guidance documents that help laboratories carry out the validation of analytical methodology. These documents are used as a criteria to validate and verify conformity of the methods applied to determine contamination and residues in different products. Objective: To evaluate the validatedanalytical methodology used to determine arsenic, cadmium and lead in samples of roasted coffee powder according to the acceptance criteria recommended in the Codex Alimentarius 27th edition procedure manual. Method: This is an observational study of the descriptive exploratory qualitative type using secondary data base. Results: With the reading of the Codex Alimentarius, the parameters used were established, namely, the minimum application range, the detection limit, the quantification limit, precision and accuracy. Thus, the evaluation of the validated methodology was carried out and it was verified that it is applicable for the analysis of As, Cd and Pb in samples of roasted coffee powder. Conclusions: Current Brazilian legislation aimed at controlling the presence of contaminants in food establishes the maximum tolerated limits for As, Cd and Pb, but does not define which methodologies should be used to verify the presence and concentration of these elements. Therefore, the methodology presented in this study is adequate to control the quality of roasted coffee powder regarding the presence of these inorganic contaminants, thus contributing to the protection and safety of the population. |
publishDate |
2024 |
dc.date.none.fl_str_mv |
2024-03-15 |
dc.type.driver.fl_str_mv |
info:eu-repo/semantics/article info:eu-repo/semantics/publishedVersion "Peer-reviewed article" "Artículo revisado por pares" "Artigo avaliado pelos pares" |
format |
article |
status_str |
publishedVersion |
dc.identifier.uri.fl_str_mv |
https://visaemdebate.incqs.fiocruz.br/index.php/visaemdebate/article/view/2192 10.22239/2317-269x.02192 |
url |
https://visaemdebate.incqs.fiocruz.br/index.php/visaemdebate/article/view/2192 |
identifier_str_mv |
10.22239/2317-269x.02192 |
dc.language.iso.fl_str_mv |
por |
language |
por |
dc.relation.none.fl_str_mv |
https://visaemdebate.incqs.fiocruz.br/index.php/visaemdebate/article/view/2192/1632 |
dc.rights.driver.fl_str_mv |
https://creativecommons.org/licenses/by/4.0 info:eu-repo/semantics/openAccess |
rights_invalid_str_mv |
https://creativecommons.org/licenses/by/4.0 |
eu_rights_str_mv |
openAccess |
dc.format.none.fl_str_mv |
application/pdf |
dc.publisher.none.fl_str_mv |
Instituto Nacional de Controle de Qualidade em Saúde |
publisher.none.fl_str_mv |
Instituto Nacional de Controle de Qualidade em Saúde |
dc.source.none.fl_str_mv |
Health Surveillance under Debate: Society, Science & Technology ; v. 12 (2024) | Continuous publication; 1-5 Vigilancia en Salud en Debate: Sociedad, Ciencia y Tecnología; v. 12 (2024) | Publicación continua; 1-5 Vigil Sanit Debate, Rio de Janeiro; v. 12 (2024) | Publicação contínua; 1-5 2317-269X reponame:Vigilância Sanitária em Debate instname:Fundação Oswaldo Cruz (FIOCRUZ) instacron:FIOCRUZ |
instname_str |
Fundação Oswaldo Cruz (FIOCRUZ) |
instacron_str |
FIOCRUZ |
institution |
FIOCRUZ |
reponame_str |
Vigilância Sanitária em Debate |
collection |
Vigilância Sanitária em Debate |
repository.name.fl_str_mv |
Vigilância Sanitária em Debate - Fundação Oswaldo Cruz (FIOCRUZ) |
repository.mail.fl_str_mv |
incqs.visaemdebate@fiocruz.br || gisele.neves@fiocruz.br |
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1797042047320850432 |