Analysis of Cannabis sativa L. leaves by ambient mass spectrometry
Autor(a) principal: | |
---|---|
Data de Publicação: | 2023 |
Outros Autores: | , , |
Tipo de documento: | Artigo |
Idioma: | por |
Título da fonte: | Revista Eletrônica Debates em Educação Científica e Tecnológica |
Texto Completo: | https://ojs.ifes.edu.br/index.php/ric/article/view/2184 |
Resumo: | The Cannabis plant has had a very close relationship with society for many years, whether due to its cultural and/or medicinal use, as well as the use of its derivative products (such as marijuana and hashish) for recreational purposes. Regardless of the purpose of use, the fast and efficient identification of Cannabis must be achieved by the detection of compounds of its main class: the cannabinoids. In this sense, the present work presents an alternative of fast analysis and with a reduced matrix effect using Ambient Mass Spectrometry techniques: with paper spray (PS) and leaf spray ionization (LS) sources and comparing them with the Atmospheric Pressure Ionization technique (API): using electrospray ionization (ESI) source. All sources proved to be adequate in the ionization process of the target class: cannabinoids. However, the LS-MS technique exhibited greater relative intensity and a smaller ionic suppression effect, indicating it as a promising tool for the rapid detection of cannabinoids directly from plant tissue, eliminating the extraction and dilution steps required in the other presented sources.Keywords: cannabinoids; ambient mass spectrometry; leaf spray ionization. |
id |
IFES-1_8440a860bae8c59763aa3de2cf6763d3 |
---|---|
oai_identifier_str |
oai::article/2184 |
network_acronym_str |
IFES-1 |
network_name_str |
Revista Eletrônica Debates em Educação Científica e Tecnológica |
repository_id_str |
|
spelling |
Analysis of Cannabis sativa L. leaves by ambient mass spectrometryANÁLISE DE FOLHAS DE CANNABIS SATIVA L. POR ESPECTROMETRIA DE MASSAS AMBIENTEcanabinoidesespectrometria de massas ambienteleaf spray ionizationThe Cannabis plant has had a very close relationship with society for many years, whether due to its cultural and/or medicinal use, as well as the use of its derivative products (such as marijuana and hashish) for recreational purposes. Regardless of the purpose of use, the fast and efficient identification of Cannabis must be achieved by the detection of compounds of its main class: the cannabinoids. In this sense, the present work presents an alternative of fast analysis and with a reduced matrix effect using Ambient Mass Spectrometry techniques: with paper spray (PS) and leaf spray ionization (LS) sources and comparing them with the Atmospheric Pressure Ionization technique (API): using electrospray ionization (ESI) source. All sources proved to be adequate in the ionization process of the target class: cannabinoids. However, the LS-MS technique exhibited greater relative intensity and a smaller ionic suppression effect, indicating it as a promising tool for the rapid detection of cannabinoids directly from plant tissue, eliminating the extraction and dilution steps required in the other presented sources.Keywords: cannabinoids; ambient mass spectrometry; leaf spray ionization.A planta Cannabis possui uma relação muito próxima com a sociedade há vários anos, seja devido ao seu uso cultural e/ou medicinal, como no uso de seus produtos derivados (como maconha e haxixe) para fins recreativos. Independente da finalidade do uso, a rápida e eficiente identificação da Cannabis deve ser alcançada com, por exemplo, a detecção de compostos da sua principal classe; os canabinoides. Nesse sentido, o presente trabalho apresenta uma alternativa de análise rápida e com reduzido efeito de matriz utilizando técnicas Ambient Mass Spectrometry: com as fontes paper spray (PS) e leaf spray ionization (LS), e comparando-as com a técnica Atmospheric Pressure Ionization (API): utilizando a fonte electrospray (ESI). Todas as fontes mostraram-se hábeis no processo de ionização da classe alvo: canabinoides, no entanto, uma maior intensidade relativa, e menor efeito de supressão iônica foram observados com uso da técnica de LS-MS, indicando-a como uma ferramenta promissora para rápida detecção de canabinoides diretamente do tecido vegetal, extinguindo etapas de extração e diluição requeridas nas outras fontes apresentadas.Instituto Federal do Espírito Santo2023-10-01info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersionapplication/pdfhttps://ojs.ifes.edu.br/index.php/ric/article/view/218410.36524/ric.v9i3.2184Revista Ifes Ciência ; v. 9 n. 3 (2023): Edição Especial: Ciências Forenses ; 01-122359-479910.36524/ric.v9i3reponame:Revista Eletrônica Debates em Educação Científica e Tecnológicainstname:Instituto Federal de Educação, Ciência e Tecnologia do Espírito Santo (IFES)instacron:IFESporhttps://ojs.ifes.edu.br/index.php/ric/article/view/2184/1068Copyright (c) 2023 Revista Ifes Ciência https://creativecommons.org/licenses/by-nc-nd/4.0info:eu-repo/semantics/openAccessAraujo dos Santos, NayaraScorsatto Ortiz, Rafael Sander Fett, Mauro Romão, Wanderson 2024-03-25T14:39:22Zoai::article/2184Revistahttps://ojs.ifes.edu.br/index.php/indexPUBhttps://ojs.ifes.edu.br/index.php/index/oairevistadect@gmail.com||sidneiquezada@gmail.com2236-21502179-6955opendoar:2024-03-25T14:39:22Revista Eletrônica Debates em Educação Científica e Tecnológica - Instituto Federal de Educação, Ciência e Tecnologia do Espírito Santo (IFES)false |
dc.title.none.fl_str_mv |
Analysis of Cannabis sativa L. leaves by ambient mass spectrometry ANÁLISE DE FOLHAS DE CANNABIS SATIVA L. POR ESPECTROMETRIA DE MASSAS AMBIENTE |
title |
Analysis of Cannabis sativa L. leaves by ambient mass spectrometry |
spellingShingle |
Analysis of Cannabis sativa L. leaves by ambient mass spectrometry Araujo dos Santos, Nayara canabinoides espectrometria de massas ambiente leaf spray ionization |
title_short |
Analysis of Cannabis sativa L. leaves by ambient mass spectrometry |
title_full |
Analysis of Cannabis sativa L. leaves by ambient mass spectrometry |
title_fullStr |
Analysis of Cannabis sativa L. leaves by ambient mass spectrometry |
title_full_unstemmed |
Analysis of Cannabis sativa L. leaves by ambient mass spectrometry |
title_sort |
Analysis of Cannabis sativa L. leaves by ambient mass spectrometry |
author |
Araujo dos Santos, Nayara |
author_facet |
Araujo dos Santos, Nayara Scorsatto Ortiz, Rafael Sander Fett, Mauro Romão, Wanderson |
author_role |
author |
author2 |
Scorsatto Ortiz, Rafael Sander Fett, Mauro Romão, Wanderson |
author2_role |
author author author |
dc.contributor.author.fl_str_mv |
Araujo dos Santos, Nayara Scorsatto Ortiz, Rafael Sander Fett, Mauro Romão, Wanderson |
dc.subject.por.fl_str_mv |
canabinoides espectrometria de massas ambiente leaf spray ionization |
topic |
canabinoides espectrometria de massas ambiente leaf spray ionization |
description |
The Cannabis plant has had a very close relationship with society for many years, whether due to its cultural and/or medicinal use, as well as the use of its derivative products (such as marijuana and hashish) for recreational purposes. Regardless of the purpose of use, the fast and efficient identification of Cannabis must be achieved by the detection of compounds of its main class: the cannabinoids. In this sense, the present work presents an alternative of fast analysis and with a reduced matrix effect using Ambient Mass Spectrometry techniques: with paper spray (PS) and leaf spray ionization (LS) sources and comparing them with the Atmospheric Pressure Ionization technique (API): using electrospray ionization (ESI) source. All sources proved to be adequate in the ionization process of the target class: cannabinoids. However, the LS-MS technique exhibited greater relative intensity and a smaller ionic suppression effect, indicating it as a promising tool for the rapid detection of cannabinoids directly from plant tissue, eliminating the extraction and dilution steps required in the other presented sources.Keywords: cannabinoids; ambient mass spectrometry; leaf spray ionization. |
publishDate |
2023 |
dc.date.none.fl_str_mv |
2023-10-01 |
dc.type.driver.fl_str_mv |
info:eu-repo/semantics/article info:eu-repo/semantics/publishedVersion |
format |
article |
status_str |
publishedVersion |
dc.identifier.uri.fl_str_mv |
https://ojs.ifes.edu.br/index.php/ric/article/view/2184 10.36524/ric.v9i3.2184 |
url |
https://ojs.ifes.edu.br/index.php/ric/article/view/2184 |
identifier_str_mv |
10.36524/ric.v9i3.2184 |
dc.language.iso.fl_str_mv |
por |
language |
por |
dc.relation.none.fl_str_mv |
https://ojs.ifes.edu.br/index.php/ric/article/view/2184/1068 |
dc.rights.driver.fl_str_mv |
Copyright (c) 2023 Revista Ifes Ciência https://creativecommons.org/licenses/by-nc-nd/4.0 info:eu-repo/semantics/openAccess |
rights_invalid_str_mv |
Copyright (c) 2023 Revista Ifes Ciência https://creativecommons.org/licenses/by-nc-nd/4.0 |
eu_rights_str_mv |
openAccess |
dc.format.none.fl_str_mv |
application/pdf |
dc.publisher.none.fl_str_mv |
Instituto Federal do Espírito Santo |
publisher.none.fl_str_mv |
Instituto Federal do Espírito Santo |
dc.source.none.fl_str_mv |
Revista Ifes Ciência ; v. 9 n. 3 (2023): Edição Especial: Ciências Forenses ; 01-12 2359-4799 10.36524/ric.v9i3 reponame:Revista Eletrônica Debates em Educação Científica e Tecnológica instname:Instituto Federal de Educação, Ciência e Tecnologia do Espírito Santo (IFES) instacron:IFES |
instname_str |
Instituto Federal de Educação, Ciência e Tecnologia do Espírito Santo (IFES) |
instacron_str |
IFES |
institution |
IFES |
reponame_str |
Revista Eletrônica Debates em Educação Científica e Tecnológica |
collection |
Revista Eletrônica Debates em Educação Científica e Tecnológica |
repository.name.fl_str_mv |
Revista Eletrônica Debates em Educação Científica e Tecnológica - Instituto Federal de Educação, Ciência e Tecnologia do Espírito Santo (IFES) |
repository.mail.fl_str_mv |
revistadect@gmail.com||sidneiquezada@gmail.com |
_version_ |
1798948024224841728 |