Analysis of Cannabis sativa L. leaves by ambient mass spectrometry

Detalhes bibliográficos
Autor(a) principal: Araujo dos Santos, Nayara
Data de Publicação: 2023
Outros Autores: Scorsatto Ortiz, Rafael, Sander Fett, Mauro, Romão, Wanderson
Tipo de documento: Artigo
Idioma: por
Título da fonte: Revista Eletrônica Debates em Educação Científica e Tecnológica
Texto Completo: https://ojs.ifes.edu.br/index.php/ric/article/view/2184
Resumo: The Cannabis plant has had a very close relationship with society for many years, whether due to its cultural and/or medicinal use, as well as the use of its derivative products (such as marijuana and hashish) for recreational purposes. Regardless of the purpose of use, the fast and efficient identification of Cannabis must be achieved by the detection of compounds of its main class: the cannabinoids. In this sense, the present work presents an alternative of fast analysis and with a reduced matrix effect using Ambient Mass Spectrometry techniques: with paper spray (PS) and leaf spray ionization (LS) sources and comparing them with the Atmospheric Pressure Ionization technique (API): using electrospray ionization (ESI) source. All sources proved to be adequate in the ionization process of the target class: cannabinoids. However, the LS-MS technique exhibited greater relative intensity and a smaller ionic suppression effect, indicating it as a promising tool for the rapid detection of cannabinoids directly from plant tissue, eliminating the extraction and dilution steps required in the other presented sources.Keywords: cannabinoids; ambient mass spectrometry; leaf spray ionization.
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spelling Analysis of Cannabis sativa L. leaves by ambient mass spectrometryANÁLISE DE FOLHAS DE CANNABIS SATIVA L. POR ESPECTROMETRIA DE MASSAS AMBIENTEcanabinoidesespectrometria de massas ambienteleaf spray ionizationThe Cannabis plant has had a very close relationship with society for many years, whether due to its cultural and/or medicinal use, as well as the use of its derivative products (such as marijuana and hashish) for recreational purposes. Regardless of the purpose of use, the fast and efficient identification of Cannabis must be achieved by the detection of compounds of its main class: the cannabinoids. In this sense, the present work presents an alternative of fast analysis and with a reduced matrix effect using Ambient Mass Spectrometry techniques: with paper spray (PS) and leaf spray ionization (LS) sources and comparing them with the Atmospheric Pressure Ionization technique (API): using electrospray ionization (ESI) source. All sources proved to be adequate in the ionization process of the target class: cannabinoids. However, the LS-MS technique exhibited greater relative intensity and a smaller ionic suppression effect, indicating it as a promising tool for the rapid detection of cannabinoids directly from plant tissue, eliminating the extraction and dilution steps required in the other presented sources.Keywords: cannabinoids; ambient mass spectrometry; leaf spray ionization.A planta Cannabis possui uma relação muito próxima com a sociedade há vários anos, seja devido ao seu uso cultural e/ou medicinal, como no uso de seus produtos derivados (como maconha e haxixe) para fins recreativos. Independente da finalidade do uso, a rápida e eficiente identificação da Cannabis deve ser alcançada com, por exemplo, a detecção de compostos da sua principal classe; os canabinoides. Nesse sentido, o presente trabalho apresenta uma alternativa de análise rápida e com reduzido efeito de matriz utilizando técnicas Ambient Mass Spectrometry: com as fontes paper spray (PS) e leaf spray ionization (LS), e comparando-as com a técnica Atmospheric Pressure Ionization (API): utilizando a fonte electrospray (ESI). Todas as fontes mostraram-se hábeis no processo de ionização da classe alvo: canabinoides, no entanto, uma maior intensidade relativa, e menor efeito de supressão iônica foram observados com uso da técnica de LS-MS, indicando-a como uma ferramenta promissora para rápida detecção de canabinoides diretamente do tecido vegetal, extinguindo etapas de extração e diluição requeridas nas outras fontes apresentadas.Instituto Federal do Espírito Santo2023-10-01info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersionapplication/pdfhttps://ojs.ifes.edu.br/index.php/ric/article/view/218410.36524/ric.v9i3.2184Revista Ifes Ciência ; v. 9 n. 3 (2023): Edição Especial: Ciências Forenses ; 01-122359-479910.36524/ric.v9i3reponame:Revista Eletrônica Debates em Educação Científica e Tecnológicainstname:Instituto Federal de Educação, Ciência e Tecnologia do Espírito Santo (IFES)instacron:IFESporhttps://ojs.ifes.edu.br/index.php/ric/article/view/2184/1068Copyright (c) 2023 Revista Ifes Ciência https://creativecommons.org/licenses/by-nc-nd/4.0info:eu-repo/semantics/openAccessAraujo dos Santos, NayaraScorsatto Ortiz, Rafael Sander Fett, Mauro Romão, Wanderson 2024-03-25T14:39:22Zoai::article/2184Revistahttps://ojs.ifes.edu.br/index.php/indexPUBhttps://ojs.ifes.edu.br/index.php/index/oairevistadect@gmail.com||sidneiquezada@gmail.com2236-21502179-6955opendoar:2024-03-25T14:39:22Revista Eletrônica Debates em Educação Científica e Tecnológica - Instituto Federal de Educação, Ciência e Tecnologia do Espírito Santo (IFES)false
dc.title.none.fl_str_mv Analysis of Cannabis sativa L. leaves by ambient mass spectrometry
ANÁLISE DE FOLHAS DE CANNABIS SATIVA L. POR ESPECTROMETRIA DE MASSAS AMBIENTE
title Analysis of Cannabis sativa L. leaves by ambient mass spectrometry
spellingShingle Analysis of Cannabis sativa L. leaves by ambient mass spectrometry
Araujo dos Santos, Nayara
canabinoides
espectrometria de massas ambiente
leaf spray ionization
title_short Analysis of Cannabis sativa L. leaves by ambient mass spectrometry
title_full Analysis of Cannabis sativa L. leaves by ambient mass spectrometry
title_fullStr Analysis of Cannabis sativa L. leaves by ambient mass spectrometry
title_full_unstemmed Analysis of Cannabis sativa L. leaves by ambient mass spectrometry
title_sort Analysis of Cannabis sativa L. leaves by ambient mass spectrometry
author Araujo dos Santos, Nayara
author_facet Araujo dos Santos, Nayara
Scorsatto Ortiz, Rafael
Sander Fett, Mauro
Romão, Wanderson
author_role author
author2 Scorsatto Ortiz, Rafael
Sander Fett, Mauro
Romão, Wanderson
author2_role author
author
author
dc.contributor.author.fl_str_mv Araujo dos Santos, Nayara
Scorsatto Ortiz, Rafael
Sander Fett, Mauro
Romão, Wanderson
dc.subject.por.fl_str_mv canabinoides
espectrometria de massas ambiente
leaf spray ionization
topic canabinoides
espectrometria de massas ambiente
leaf spray ionization
description The Cannabis plant has had a very close relationship with society for many years, whether due to its cultural and/or medicinal use, as well as the use of its derivative products (such as marijuana and hashish) for recreational purposes. Regardless of the purpose of use, the fast and efficient identification of Cannabis must be achieved by the detection of compounds of its main class: the cannabinoids. In this sense, the present work presents an alternative of fast analysis and with a reduced matrix effect using Ambient Mass Spectrometry techniques: with paper spray (PS) and leaf spray ionization (LS) sources and comparing them with the Atmospheric Pressure Ionization technique (API): using electrospray ionization (ESI) source. All sources proved to be adequate in the ionization process of the target class: cannabinoids. However, the LS-MS technique exhibited greater relative intensity and a smaller ionic suppression effect, indicating it as a promising tool for the rapid detection of cannabinoids directly from plant tissue, eliminating the extraction and dilution steps required in the other presented sources.Keywords: cannabinoids; ambient mass spectrometry; leaf spray ionization.
publishDate 2023
dc.date.none.fl_str_mv 2023-10-01
dc.type.driver.fl_str_mv info:eu-repo/semantics/article
info:eu-repo/semantics/publishedVersion
format article
status_str publishedVersion
dc.identifier.uri.fl_str_mv https://ojs.ifes.edu.br/index.php/ric/article/view/2184
10.36524/ric.v9i3.2184
url https://ojs.ifes.edu.br/index.php/ric/article/view/2184
identifier_str_mv 10.36524/ric.v9i3.2184
dc.language.iso.fl_str_mv por
language por
dc.relation.none.fl_str_mv https://ojs.ifes.edu.br/index.php/ric/article/view/2184/1068
dc.rights.driver.fl_str_mv Copyright (c) 2023 Revista Ifes Ciência
https://creativecommons.org/licenses/by-nc-nd/4.0
info:eu-repo/semantics/openAccess
rights_invalid_str_mv Copyright (c) 2023 Revista Ifes Ciência
https://creativecommons.org/licenses/by-nc-nd/4.0
eu_rights_str_mv openAccess
dc.format.none.fl_str_mv application/pdf
dc.publisher.none.fl_str_mv Instituto Federal do Espírito Santo
publisher.none.fl_str_mv Instituto Federal do Espírito Santo
dc.source.none.fl_str_mv Revista Ifes Ciência ; v. 9 n. 3 (2023): Edição Especial: Ciências Forenses ; 01-12
2359-4799
10.36524/ric.v9i3
reponame:Revista Eletrônica Debates em Educação Científica e Tecnológica
instname:Instituto Federal de Educação, Ciência e Tecnologia do Espírito Santo (IFES)
instacron:IFES
instname_str Instituto Federal de Educação, Ciência e Tecnologia do Espírito Santo (IFES)
instacron_str IFES
institution IFES
reponame_str Revista Eletrônica Debates em Educação Científica e Tecnológica
collection Revista Eletrônica Debates em Educação Científica e Tecnológica
repository.name.fl_str_mv Revista Eletrônica Debates em Educação Científica e Tecnológica - Instituto Federal de Educação, Ciência e Tecnologia do Espírito Santo (IFES)
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