Characterization of aroma compounds in portuguese extra virgin olive oils from Galega vulgar and Cobrançosa cultivars using GC-O and GC x GC-ToFMS
Autor(a) principal: | |
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Data de Publicação: | 2013 |
Outros Autores: | , , , , |
Tipo de documento: | Artigo |
Idioma: | eng |
Título da fonte: | Repositório Científico de Acesso Aberto de Portugal (Repositórios Cientìficos) |
Texto Completo: | http://hdl.handle.net/10400.5/15820 |
Resumo: | Aroma compounds of virgin olive oils extracted from two olive cultivars – Galega Vulgar and Cobrançosa – grown in Beira Baixa region in central Portugal were investigated. Gas chromatography–olfactometry (GC–O) was carried out to select the important odorants for subsequent comprehensive gas chromatography/time of flightmass spectrometry (GC × GC–ToFMS) analysis. By GC–O fifteen odorants were identified. For the quantification of volatile compounds, headspace solid phasemicroextraction (SPME) technique was optimized. Under optimized conditions, 22 volatile compounds were quantified in all samples. Trans-2-hexenal was the most abundant compound. A discriminant analysis (DA) was used to discriminate among olive oil samples obtained from olives of the two cultivars with different harvest time/ripening stages. Concerning the harvesting time and cultivar, nine volatiles showed to have discriminant power among samples, namely heptanal, trans-2-hexenal, 1-octen-1-ol, nonanal, 2,3-butanedione, ethyl-2-methylbutyrate, hexanal, cis-3-hexenylacetate and 3-methylbuthylacetate |
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Characterization of aroma compounds in portuguese extra virgin olive oils from Galega vulgar and Cobrançosa cultivars using GC-O and GC x GC-ToFMSharvest dateolive cultivarolive oilvolatile compoundsAroma compounds of virgin olive oils extracted from two olive cultivars – Galega Vulgar and Cobrançosa – grown in Beira Baixa region in central Portugal were investigated. Gas chromatography–olfactometry (GC–O) was carried out to select the important odorants for subsequent comprehensive gas chromatography/time of flightmass spectrometry (GC × GC–ToFMS) analysis. By GC–O fifteen odorants were identified. For the quantification of volatile compounds, headspace solid phasemicroextraction (SPME) technique was optimized. Under optimized conditions, 22 volatile compounds were quantified in all samples. Trans-2-hexenal was the most abundant compound. A discriminant analysis (DA) was used to discriminate among olive oil samples obtained from olives of the two cultivars with different harvest time/ripening stages. Concerning the harvesting time and cultivar, nine volatiles showed to have discriminant power among samples, namely heptanal, trans-2-hexenal, 1-octen-1-ol, nonanal, 2,3-butanedione, ethyl-2-methylbutyrate, hexanal, cis-3-hexenylacetate and 3-methylbuthylacetateElsevierRepositório da Universidade de LisboaPeres, F.Jelén, H.H.Majcher, M.M.Arraias, M.Louro Martins, LuisaFerreira-Dias, Suzana2018-07-17T13:14:53Z20132013-01-01T00:00:00Zinfo:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/articleapplication/pdfhttp://hdl.handle.net/10400.5/15820engFood Research International 54 (2013) 1979–1986http://dx.doi.org/10.1016/j.foodres.2013.06.015info:eu-repo/semantics/openAccessreponame:Repositório Científico de Acesso Aberto de Portugal (Repositórios Cientìficos)instname:Agência para a Sociedade do Conhecimento (UMIC) - FCT - Sociedade da Informaçãoinstacron:RCAAP2023-03-06T14:45:43Zoai:www.repository.utl.pt:10400.5/15820Portal AgregadorONGhttps://www.rcaap.pt/oai/openaireopendoar:71602024-03-19T17:01:23.095175Repositório Científico de Acesso Aberto de Portugal (Repositórios Cientìficos) - Agência para a Sociedade do Conhecimento (UMIC) - FCT - Sociedade da Informaçãofalse |
dc.title.none.fl_str_mv |
Characterization of aroma compounds in portuguese extra virgin olive oils from Galega vulgar and Cobrançosa cultivars using GC-O and GC x GC-ToFMS |
title |
Characterization of aroma compounds in portuguese extra virgin olive oils from Galega vulgar and Cobrançosa cultivars using GC-O and GC x GC-ToFMS |
spellingShingle |
Characterization of aroma compounds in portuguese extra virgin olive oils from Galega vulgar and Cobrançosa cultivars using GC-O and GC x GC-ToFMS Peres, F. harvest date olive cultivar olive oil volatile compounds |
title_short |
Characterization of aroma compounds in portuguese extra virgin olive oils from Galega vulgar and Cobrançosa cultivars using GC-O and GC x GC-ToFMS |
title_full |
Characterization of aroma compounds in portuguese extra virgin olive oils from Galega vulgar and Cobrançosa cultivars using GC-O and GC x GC-ToFMS |
title_fullStr |
Characterization of aroma compounds in portuguese extra virgin olive oils from Galega vulgar and Cobrançosa cultivars using GC-O and GC x GC-ToFMS |
title_full_unstemmed |
Characterization of aroma compounds in portuguese extra virgin olive oils from Galega vulgar and Cobrançosa cultivars using GC-O and GC x GC-ToFMS |
title_sort |
Characterization of aroma compounds in portuguese extra virgin olive oils from Galega vulgar and Cobrançosa cultivars using GC-O and GC x GC-ToFMS |
author |
Peres, F. |
author_facet |
Peres, F. Jelén, H.H. Majcher, M.M. Arraias, M. Louro Martins, Luisa Ferreira-Dias, Suzana |
author_role |
author |
author2 |
Jelén, H.H. Majcher, M.M. Arraias, M. Louro Martins, Luisa Ferreira-Dias, Suzana |
author2_role |
author author author author author |
dc.contributor.none.fl_str_mv |
Repositório da Universidade de Lisboa |
dc.contributor.author.fl_str_mv |
Peres, F. Jelén, H.H. Majcher, M.M. Arraias, M. Louro Martins, Luisa Ferreira-Dias, Suzana |
dc.subject.por.fl_str_mv |
harvest date olive cultivar olive oil volatile compounds |
topic |
harvest date olive cultivar olive oil volatile compounds |
description |
Aroma compounds of virgin olive oils extracted from two olive cultivars – Galega Vulgar and Cobrançosa – grown in Beira Baixa region in central Portugal were investigated. Gas chromatography–olfactometry (GC–O) was carried out to select the important odorants for subsequent comprehensive gas chromatography/time of flightmass spectrometry (GC × GC–ToFMS) analysis. By GC–O fifteen odorants were identified. For the quantification of volatile compounds, headspace solid phasemicroextraction (SPME) technique was optimized. Under optimized conditions, 22 volatile compounds were quantified in all samples. Trans-2-hexenal was the most abundant compound. A discriminant analysis (DA) was used to discriminate among olive oil samples obtained from olives of the two cultivars with different harvest time/ripening stages. Concerning the harvesting time and cultivar, nine volatiles showed to have discriminant power among samples, namely heptanal, trans-2-hexenal, 1-octen-1-ol, nonanal, 2,3-butanedione, ethyl-2-methylbutyrate, hexanal, cis-3-hexenylacetate and 3-methylbuthylacetate |
publishDate |
2013 |
dc.date.none.fl_str_mv |
2013 2013-01-01T00:00:00Z 2018-07-17T13:14:53Z |
dc.type.status.fl_str_mv |
info:eu-repo/semantics/publishedVersion |
dc.type.driver.fl_str_mv |
info:eu-repo/semantics/article |
format |
article |
status_str |
publishedVersion |
dc.identifier.uri.fl_str_mv |
http://hdl.handle.net/10400.5/15820 |
url |
http://hdl.handle.net/10400.5/15820 |
dc.language.iso.fl_str_mv |
eng |
language |
eng |
dc.relation.none.fl_str_mv |
Food Research International 54 (2013) 1979–1986 http://dx.doi.org/10.1016/j.foodres.2013.06.015 |
dc.rights.driver.fl_str_mv |
info:eu-repo/semantics/openAccess |
eu_rights_str_mv |
openAccess |
dc.format.none.fl_str_mv |
application/pdf |
dc.publisher.none.fl_str_mv |
Elsevier |
publisher.none.fl_str_mv |
Elsevier |
dc.source.none.fl_str_mv |
reponame:Repositório Científico de Acesso Aberto de Portugal (Repositórios Cientìficos) instname:Agência para a Sociedade do Conhecimento (UMIC) - FCT - Sociedade da Informação instacron:RCAAP |
instname_str |
Agência para a Sociedade do Conhecimento (UMIC) - FCT - Sociedade da Informação |
instacron_str |
RCAAP |
institution |
RCAAP |
reponame_str |
Repositório Científico de Acesso Aberto de Portugal (Repositórios Cientìficos) |
collection |
Repositório Científico de Acesso Aberto de Portugal (Repositórios Cientìficos) |
repository.name.fl_str_mv |
Repositório Científico de Acesso Aberto de Portugal (Repositórios Cientìficos) - Agência para a Sociedade do Conhecimento (UMIC) - FCT - Sociedade da Informação |
repository.mail.fl_str_mv |
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1799131102244241408 |