Study of modern Chinese cloisonné by means of small-spot energy dispersive X-ray fluorescence spectrometry and Raman spectroscopy

Detalhes bibliográficos
Autor(a) principal: Queralt, I.
Data de Publicação: 2023
Outros Autores: Pessanha, S., Carvalho, M. L., Manso, M.
Tipo de documento: Artigo
Idioma: eng
Título da fonte: Repositório Científico de Acesso Aberto de Portugal (Repositórios Cientìficos)
Texto Completo: http://hdl.handle.net/10362/154665
Resumo: Funding Information: I.Queralt acknowledges a Sabbatical grant from the Ministry of Education of the Spanish Government (Ref. PRX16/00159). Funding Information: IDAEA-CSIC is a Centre of Excellence Severo Ochoa (Spanish Ministry of Science and Innovation, Project CEX2018-000794-S). Publisher Copyright: © 2022 The Authors
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spelling Study of modern Chinese cloisonné by means of small-spot energy dispersive X-ray fluorescence spectrometry and Raman spectroscopyCloisonnéEDXRFEnamelMetal coatingsRaman spectroscopyAnalytical ChemistryAtomic and Molecular Physics, and OpticsInstrumentationSpectroscopyFunding Information: I.Queralt acknowledges a Sabbatical grant from the Ministry of Education of the Spanish Government (Ref. PRX16/00159). Funding Information: IDAEA-CSIC is a Centre of Excellence Severo Ochoa (Spanish Ministry of Science and Innovation, Project CEX2018-000794-S). Publisher Copyright: © 2022 The AuthorsIn this work, we studied the features of a modern Chinese cloisonné vase by means of small-spot energy dispersive X-ray fluorescence (EDXRF) and micro-Raman spectroscopy. Quantitative elemental results of enamel have been obtained after calibration of EDXRF instrumentation with certified reference materials. Up to eleven different coloured enamels have been recognized and analysed (black, pink, red, white, yellow and three shades of both blue and green). Enamel paste is mainly formed by the main identified elemental colouring agents - chromium, manganese, iron, cobalt, copper, antimony and cadmium– in a lead alkali silicate matrix. The body of the vase is made by copper with minor amounts of zinc and tin. Analysis of metallic decorations at the surface of the vase reveal the presence of metal coatings applied for the embellishment of the artwork. Thickness of layered metal structures have been obtained by XRF fundamental parameters assisted with data from pure metal spectra, thus revealing the gilded coatings consist of a thick layer made by silver-doped nickel.DF – Departamento de FísicaLIBPhys-UNLVICARTE - Vidro e Cerâmica para as ArtesDCR - Departamento de Conservação e RestauroRUNQueralt, I.Pessanha, S.Carvalho, M. L.Manso, M.2023-06-30T22:15:41Z2023-022023-02-01T00:00:00Zinfo:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/article6application/pdfhttp://hdl.handle.net/10362/154665eng0584-8547PURE: 64999583https://doi.org/10.1016/j.sab.2022.106594info:eu-repo/semantics/openAccessreponame:Repositório Científico de Acesso Aberto de Portugal (Repositórios Cientìficos)instname:Agência para a Sociedade do Conhecimento (UMIC) - FCT - Sociedade da Informaçãoinstacron:RCAAP2024-03-11T05:37:08Zoai:run.unl.pt:10362/154665Portal AgregadorONGhttps://www.rcaap.pt/oai/openaireopendoar:71602024-03-20T03:55:43.054373Repositório Científico de Acesso Aberto de Portugal (Repositórios Cientìficos) - Agência para a Sociedade do Conhecimento (UMIC) - FCT - Sociedade da Informaçãofalse
dc.title.none.fl_str_mv Study of modern Chinese cloisonné by means of small-spot energy dispersive X-ray fluorescence spectrometry and Raman spectroscopy
title Study of modern Chinese cloisonné by means of small-spot energy dispersive X-ray fluorescence spectrometry and Raman spectroscopy
spellingShingle Study of modern Chinese cloisonné by means of small-spot energy dispersive X-ray fluorescence spectrometry and Raman spectroscopy
Queralt, I.
Cloisonné
EDXRF
Enamel
Metal coatings
Raman spectroscopy
Analytical Chemistry
Atomic and Molecular Physics, and Optics
Instrumentation
Spectroscopy
title_short Study of modern Chinese cloisonné by means of small-spot energy dispersive X-ray fluorescence spectrometry and Raman spectroscopy
title_full Study of modern Chinese cloisonné by means of small-spot energy dispersive X-ray fluorescence spectrometry and Raman spectroscopy
title_fullStr Study of modern Chinese cloisonné by means of small-spot energy dispersive X-ray fluorescence spectrometry and Raman spectroscopy
title_full_unstemmed Study of modern Chinese cloisonné by means of small-spot energy dispersive X-ray fluorescence spectrometry and Raman spectroscopy
title_sort Study of modern Chinese cloisonné by means of small-spot energy dispersive X-ray fluorescence spectrometry and Raman spectroscopy
author Queralt, I.
author_facet Queralt, I.
Pessanha, S.
Carvalho, M. L.
Manso, M.
author_role author
author2 Pessanha, S.
Carvalho, M. L.
Manso, M.
author2_role author
author
author
dc.contributor.none.fl_str_mv DF – Departamento de Física
LIBPhys-UNL
VICARTE - Vidro e Cerâmica para as Artes
DCR - Departamento de Conservação e Restauro
RUN
dc.contributor.author.fl_str_mv Queralt, I.
Pessanha, S.
Carvalho, M. L.
Manso, M.
dc.subject.por.fl_str_mv Cloisonné
EDXRF
Enamel
Metal coatings
Raman spectroscopy
Analytical Chemistry
Atomic and Molecular Physics, and Optics
Instrumentation
Spectroscopy
topic Cloisonné
EDXRF
Enamel
Metal coatings
Raman spectroscopy
Analytical Chemistry
Atomic and Molecular Physics, and Optics
Instrumentation
Spectroscopy
description Funding Information: I.Queralt acknowledges a Sabbatical grant from the Ministry of Education of the Spanish Government (Ref. PRX16/00159). Funding Information: IDAEA-CSIC is a Centre of Excellence Severo Ochoa (Spanish Ministry of Science and Innovation, Project CEX2018-000794-S). Publisher Copyright: © 2022 The Authors
publishDate 2023
dc.date.none.fl_str_mv 2023-06-30T22:15:41Z
2023-02
2023-02-01T00:00:00Z
dc.type.status.fl_str_mv info:eu-repo/semantics/publishedVersion
dc.type.driver.fl_str_mv info:eu-repo/semantics/article
format article
status_str publishedVersion
dc.identifier.uri.fl_str_mv http://hdl.handle.net/10362/154665
url http://hdl.handle.net/10362/154665
dc.language.iso.fl_str_mv eng
language eng
dc.relation.none.fl_str_mv 0584-8547
PURE: 64999583
https://doi.org/10.1016/j.sab.2022.106594
dc.rights.driver.fl_str_mv info:eu-repo/semantics/openAccess
eu_rights_str_mv openAccess
dc.format.none.fl_str_mv 6
application/pdf
dc.source.none.fl_str_mv reponame:Repositório Científico de Acesso Aberto de Portugal (Repositórios Cientìficos)
instname:Agência para a Sociedade do Conhecimento (UMIC) - FCT - Sociedade da Informação
instacron:RCAAP
instname_str Agência para a Sociedade do Conhecimento (UMIC) - FCT - Sociedade da Informação
instacron_str RCAAP
institution RCAAP
reponame_str Repositório Científico de Acesso Aberto de Portugal (Repositórios Cientìficos)
collection Repositório Científico de Acesso Aberto de Portugal (Repositórios Cientìficos)
repository.name.fl_str_mv Repositório Científico de Acesso Aberto de Portugal (Repositórios Cientìficos) - Agência para a Sociedade do Conhecimento (UMIC) - FCT - Sociedade da Informação
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