Evaluation of residues of β-lactam, sulfonamide, tetracycline, quinolone, fluoroquinolone e pyrimidine in raw milk
Autor(a) principal: | |
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Data de Publicação: | 2021 |
Outros Autores: | , , , , , |
Tipo de documento: | Artigo |
Idioma: | eng |
Título da fonte: | Food Science and Technology (Campinas) |
Texto Completo: | http://old.scielo.br/scielo.php?script=sci_arttext&pid=S0101-20612021000300603 |
Resumo: | Abstract Food quality and safety have been a concern of the world population, especially in relation to the chemical and microbiological hazards present in food. The presence of antimicrobial residues at levels above the maximum residue limit makes milk unsuitable for human consumption. In this context, the objective of this study was to analyze 184 raw milk samples from the dairy region of Pernambuco state, in order to evaluate the presence of 31 antimicrobial residues from six different groups (β-lactam, sulfonamide, tetracycline, quinolone, fluoroquinolone and pyrimidine). The samples were collected from producers who supply the dairys with and no inspection service and the analyses were performed by liquid chromatography coupled to mass spectrometry. In the qualitative analysis of multiresidues, no sample presented violation for the antimicrobials analyzed. In the quantitative analysis of β-lactams, only one sample of producers who supply milk to dairys with state inspection service presented a result above the maximum residue limit for cloxacillin (464 μg.L-1). It is concluded that raw milk produced in the dairy region of the state of Pernambuco has a low rate of violation of the values established by the current legislation for antimicrobial residues. |
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Evaluation of residues of β-lactam, sulfonamide, tetracycline, quinolone, fluoroquinolone e pyrimidine in raw milkmastitismaximum residue limitinspection serviceantimicrobial residueLC-MS/MSAbstract Food quality and safety have been a concern of the world population, especially in relation to the chemical and microbiological hazards present in food. The presence of antimicrobial residues at levels above the maximum residue limit makes milk unsuitable for human consumption. In this context, the objective of this study was to analyze 184 raw milk samples from the dairy region of Pernambuco state, in order to evaluate the presence of 31 antimicrobial residues from six different groups (β-lactam, sulfonamide, tetracycline, quinolone, fluoroquinolone and pyrimidine). The samples were collected from producers who supply the dairys with and no inspection service and the analyses were performed by liquid chromatography coupled to mass spectrometry. In the qualitative analysis of multiresidues, no sample presented violation for the antimicrobials analyzed. In the quantitative analysis of β-lactams, only one sample of producers who supply milk to dairys with state inspection service presented a result above the maximum residue limit for cloxacillin (464 μg.L-1). It is concluded that raw milk produced in the dairy region of the state of Pernambuco has a low rate of violation of the values established by the current legislation for antimicrobial residues.Sociedade Brasileira de Ciência e Tecnologia de Alimentos2021-09-01info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersiontext/htmlhttp://old.scielo.br/scielo.php?script=sci_arttext&pid=S0101-20612021000300603Food Science and Technology v.41 n.3 2021reponame:Food Science and Technology (Campinas)instname:Sociedade Brasileira de Ciência e Tecnologia de Alimentos (SBCTA)instacron:SBCTA10.1590/fst.23520info:eu-repo/semantics/openAccessVALENÇA,Luciana MartinsPAIVA,José do Egito deBARBOSA,Severino Benone PaesPINHEIRO,Irapuan OliveiraBATISTA,Ângela Maria VieiraSILVA,Marcelo José Ferreira Batista daMEDEIROS,Elizabeth Sampaio deeng2021-07-23T00:00:00Zoai:scielo:S0101-20612021000300603Revistahttp://www.scielo.br/ctaONGhttps://old.scielo.br/oai/scielo-oai.php||revista@sbcta.org.br1678-457X0101-2061opendoar:2021-07-23T00:00Food Science and Technology (Campinas) - Sociedade Brasileira de Ciência e Tecnologia de Alimentos (SBCTA)false |
dc.title.none.fl_str_mv |
Evaluation of residues of β-lactam, sulfonamide, tetracycline, quinolone, fluoroquinolone e pyrimidine in raw milk |
title |
Evaluation of residues of β-lactam, sulfonamide, tetracycline, quinolone, fluoroquinolone e pyrimidine in raw milk |
spellingShingle |
Evaluation of residues of β-lactam, sulfonamide, tetracycline, quinolone, fluoroquinolone e pyrimidine in raw milk VALENÇA,Luciana Martins mastitis maximum residue limit inspection service antimicrobial residue LC-MS/MS |
title_short |
Evaluation of residues of β-lactam, sulfonamide, tetracycline, quinolone, fluoroquinolone e pyrimidine in raw milk |
title_full |
Evaluation of residues of β-lactam, sulfonamide, tetracycline, quinolone, fluoroquinolone e pyrimidine in raw milk |
title_fullStr |
Evaluation of residues of β-lactam, sulfonamide, tetracycline, quinolone, fluoroquinolone e pyrimidine in raw milk |
title_full_unstemmed |
Evaluation of residues of β-lactam, sulfonamide, tetracycline, quinolone, fluoroquinolone e pyrimidine in raw milk |
title_sort |
Evaluation of residues of β-lactam, sulfonamide, tetracycline, quinolone, fluoroquinolone e pyrimidine in raw milk |
author |
VALENÇA,Luciana Martins |
author_facet |
VALENÇA,Luciana Martins PAIVA,José do Egito de BARBOSA,Severino Benone Paes PINHEIRO,Irapuan Oliveira BATISTA,Ângela Maria Vieira SILVA,Marcelo José Ferreira Batista da MEDEIROS,Elizabeth Sampaio de |
author_role |
author |
author2 |
PAIVA,José do Egito de BARBOSA,Severino Benone Paes PINHEIRO,Irapuan Oliveira BATISTA,Ângela Maria Vieira SILVA,Marcelo José Ferreira Batista da MEDEIROS,Elizabeth Sampaio de |
author2_role |
author author author author author author |
dc.contributor.author.fl_str_mv |
VALENÇA,Luciana Martins PAIVA,José do Egito de BARBOSA,Severino Benone Paes PINHEIRO,Irapuan Oliveira BATISTA,Ângela Maria Vieira SILVA,Marcelo José Ferreira Batista da MEDEIROS,Elizabeth Sampaio de |
dc.subject.por.fl_str_mv |
mastitis maximum residue limit inspection service antimicrobial residue LC-MS/MS |
topic |
mastitis maximum residue limit inspection service antimicrobial residue LC-MS/MS |
description |
Abstract Food quality and safety have been a concern of the world population, especially in relation to the chemical and microbiological hazards present in food. The presence of antimicrobial residues at levels above the maximum residue limit makes milk unsuitable for human consumption. In this context, the objective of this study was to analyze 184 raw milk samples from the dairy region of Pernambuco state, in order to evaluate the presence of 31 antimicrobial residues from six different groups (β-lactam, sulfonamide, tetracycline, quinolone, fluoroquinolone and pyrimidine). The samples were collected from producers who supply the dairys with and no inspection service and the analyses were performed by liquid chromatography coupled to mass spectrometry. In the qualitative analysis of multiresidues, no sample presented violation for the antimicrobials analyzed. In the quantitative analysis of β-lactams, only one sample of producers who supply milk to dairys with state inspection service presented a result above the maximum residue limit for cloxacillin (464 μg.L-1). It is concluded that raw milk produced in the dairy region of the state of Pernambuco has a low rate of violation of the values established by the current legislation for antimicrobial residues. |
publishDate |
2021 |
dc.date.none.fl_str_mv |
2021-09-01 |
dc.type.driver.fl_str_mv |
info:eu-repo/semantics/article |
dc.type.status.fl_str_mv |
info:eu-repo/semantics/publishedVersion |
format |
article |
status_str |
publishedVersion |
dc.identifier.uri.fl_str_mv |
http://old.scielo.br/scielo.php?script=sci_arttext&pid=S0101-20612021000300603 |
url |
http://old.scielo.br/scielo.php?script=sci_arttext&pid=S0101-20612021000300603 |
dc.language.iso.fl_str_mv |
eng |
language |
eng |
dc.relation.none.fl_str_mv |
10.1590/fst.23520 |
dc.rights.driver.fl_str_mv |
info:eu-repo/semantics/openAccess |
eu_rights_str_mv |
openAccess |
dc.format.none.fl_str_mv |
text/html |
dc.publisher.none.fl_str_mv |
Sociedade Brasileira de Ciência e Tecnologia de Alimentos |
publisher.none.fl_str_mv |
Sociedade Brasileira de Ciência e Tecnologia de Alimentos |
dc.source.none.fl_str_mv |
Food Science and Technology v.41 n.3 2021 reponame:Food Science and Technology (Campinas) instname:Sociedade Brasileira de Ciência e Tecnologia de Alimentos (SBCTA) instacron:SBCTA |
instname_str |
Sociedade Brasileira de Ciência e Tecnologia de Alimentos (SBCTA) |
instacron_str |
SBCTA |
institution |
SBCTA |
reponame_str |
Food Science and Technology (Campinas) |
collection |
Food Science and Technology (Campinas) |
repository.name.fl_str_mv |
Food Science and Technology (Campinas) - Sociedade Brasileira de Ciência e Tecnologia de Alimentos (SBCTA) |
repository.mail.fl_str_mv |
||revista@sbcta.org.br |
_version_ |
1752126328200495104 |