Grinding and Milling: Two Efficient Methodologies in the Solvent-Free Phosphomolybdic Acid-Catalyzed and Mechanochemical Synthesis of cis-4-Amido-N-yl-2-methyl-tetrahydroquinolines

Detalhes bibliográficos
Autor(a) principal: Kouznetsov,Vladimir V.
Data de Publicação: 2016
Outros Autores: Merchán-Arenas,Diego R., Martínez-Bonilla,Carlos A., Macías,Mario A., Roussel,Pascal, Gauthier,Gilles H.
Tipo de documento: Artigo
Idioma: eng
Título da fonte: Journal of the Brazilian Chemical Society (Online)
Texto Completo: http://old.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50532016001202246
Resumo: The ball-milling process of ABB' Povarov reaction through mechano-chemical activation with phosphomolybdic acid (PMA) as heteropolyacid (HPA) catalyst, was first time explored. The developed high speed vibratory ball milling (HSVBM) green method offers simple and efficient diastereoselective synthesis of cis-2,4-disubstituted tetrahydroquinolines in good to excellent yields (56-76%).
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spelling Grinding and Milling: Two Efficient Methodologies in the Solvent-Free Phosphomolybdic Acid-Catalyzed and Mechanochemical Synthesis of cis-4-Amido-N-yl-2-methyl-tetrahydroquinolinesmechano-chemical millingABB' Povarov type reactionphosphomolybdic acid catalystsolvent-free Povarov reactionThe ball-milling process of ABB' Povarov reaction through mechano-chemical activation with phosphomolybdic acid (PMA) as heteropolyacid (HPA) catalyst, was first time explored. The developed high speed vibratory ball milling (HSVBM) green method offers simple and efficient diastereoselective synthesis of cis-2,4-disubstituted tetrahydroquinolines in good to excellent yields (56-76%).Sociedade Brasileira de Química2016-12-01info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersiontext/htmlhttp://old.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50532016001202246Journal of the Brazilian Chemical Society v.27 n.12 2016reponame:Journal of the Brazilian Chemical Society (Online)instname:Sociedade Brasileira de Química (SBQ)instacron:SBQ10.5935/0103-5053.20160117info:eu-repo/semantics/openAccessKouznetsov,Vladimir V.Merchán-Arenas,Diego R.Martínez-Bonilla,Carlos A.Macías,Mario A.Roussel,PascalGauthier,Gilles H.eng2016-12-01T00:00:00Zoai:scielo:S0103-50532016001202246Revistahttp://jbcs.sbq.org.brONGhttps://old.scielo.br/oai/scielo-oai.php||office@jbcs.sbq.org.br1678-47900103-5053opendoar:2016-12-01T00:00Journal of the Brazilian Chemical Society (Online) - Sociedade Brasileira de Química (SBQ)false
dc.title.none.fl_str_mv Grinding and Milling: Two Efficient Methodologies in the Solvent-Free Phosphomolybdic Acid-Catalyzed and Mechanochemical Synthesis of cis-4-Amido-N-yl-2-methyl-tetrahydroquinolines
title Grinding and Milling: Two Efficient Methodologies in the Solvent-Free Phosphomolybdic Acid-Catalyzed and Mechanochemical Synthesis of cis-4-Amido-N-yl-2-methyl-tetrahydroquinolines
spellingShingle Grinding and Milling: Two Efficient Methodologies in the Solvent-Free Phosphomolybdic Acid-Catalyzed and Mechanochemical Synthesis of cis-4-Amido-N-yl-2-methyl-tetrahydroquinolines
Kouznetsov,Vladimir V.
mechano-chemical milling
ABB' Povarov type reaction
phosphomolybdic acid catalyst
solvent-free Povarov reaction
title_short Grinding and Milling: Two Efficient Methodologies in the Solvent-Free Phosphomolybdic Acid-Catalyzed and Mechanochemical Synthesis of cis-4-Amido-N-yl-2-methyl-tetrahydroquinolines
title_full Grinding and Milling: Two Efficient Methodologies in the Solvent-Free Phosphomolybdic Acid-Catalyzed and Mechanochemical Synthesis of cis-4-Amido-N-yl-2-methyl-tetrahydroquinolines
title_fullStr Grinding and Milling: Two Efficient Methodologies in the Solvent-Free Phosphomolybdic Acid-Catalyzed and Mechanochemical Synthesis of cis-4-Amido-N-yl-2-methyl-tetrahydroquinolines
title_full_unstemmed Grinding and Milling: Two Efficient Methodologies in the Solvent-Free Phosphomolybdic Acid-Catalyzed and Mechanochemical Synthesis of cis-4-Amido-N-yl-2-methyl-tetrahydroquinolines
title_sort Grinding and Milling: Two Efficient Methodologies in the Solvent-Free Phosphomolybdic Acid-Catalyzed and Mechanochemical Synthesis of cis-4-Amido-N-yl-2-methyl-tetrahydroquinolines
author Kouznetsov,Vladimir V.
author_facet Kouznetsov,Vladimir V.
Merchán-Arenas,Diego R.
Martínez-Bonilla,Carlos A.
Macías,Mario A.
Roussel,Pascal
Gauthier,Gilles H.
author_role author
author2 Merchán-Arenas,Diego R.
Martínez-Bonilla,Carlos A.
Macías,Mario A.
Roussel,Pascal
Gauthier,Gilles H.
author2_role author
author
author
author
author
dc.contributor.author.fl_str_mv Kouznetsov,Vladimir V.
Merchán-Arenas,Diego R.
Martínez-Bonilla,Carlos A.
Macías,Mario A.
Roussel,Pascal
Gauthier,Gilles H.
dc.subject.por.fl_str_mv mechano-chemical milling
ABB' Povarov type reaction
phosphomolybdic acid catalyst
solvent-free Povarov reaction
topic mechano-chemical milling
ABB' Povarov type reaction
phosphomolybdic acid catalyst
solvent-free Povarov reaction
description The ball-milling process of ABB' Povarov reaction through mechano-chemical activation with phosphomolybdic acid (PMA) as heteropolyacid (HPA) catalyst, was first time explored. The developed high speed vibratory ball milling (HSVBM) green method offers simple and efficient diastereoselective synthesis of cis-2,4-disubstituted tetrahydroquinolines in good to excellent yields (56-76%).
publishDate 2016
dc.date.none.fl_str_mv 2016-12-01
dc.type.driver.fl_str_mv info:eu-repo/semantics/article
dc.type.status.fl_str_mv info:eu-repo/semantics/publishedVersion
format article
status_str publishedVersion
dc.identifier.uri.fl_str_mv http://old.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50532016001202246
url http://old.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50532016001202246
dc.language.iso.fl_str_mv eng
language eng
dc.relation.none.fl_str_mv 10.5935/0103-5053.20160117
dc.rights.driver.fl_str_mv info:eu-repo/semantics/openAccess
eu_rights_str_mv openAccess
dc.format.none.fl_str_mv text/html
dc.publisher.none.fl_str_mv Sociedade Brasileira de Química
publisher.none.fl_str_mv Sociedade Brasileira de Química
dc.source.none.fl_str_mv Journal of the Brazilian Chemical Society v.27 n.12 2016
reponame:Journal of the Brazilian Chemical Society (Online)
instname:Sociedade Brasileira de Química (SBQ)
instacron:SBQ
instname_str Sociedade Brasileira de Química (SBQ)
instacron_str SBQ
institution SBQ
reponame_str Journal of the Brazilian Chemical Society (Online)
collection Journal of the Brazilian Chemical Society (Online)
repository.name.fl_str_mv Journal of the Brazilian Chemical Society (Online) - Sociedade Brasileira de Química (SBQ)
repository.mail.fl_str_mv ||office@jbcs.sbq.org.br
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