Optimization and practical implementation of ultrafast 2D NMR experiments

Detalhes bibliográficos
Autor(a) principal: Queiroz Júnior,Luiz H. K.
Data de Publicação: 2013
Outros Autores: Ferreira,Antonio G., Giraudeau,Patrick
Tipo de documento: Relatório
Idioma: eng
Título da fonte: Química Nova (Online)
Texto Completo: http://old.scielo.br/scielo.php?script=sci_arttext&pid=S0100-40422013000400016
Resumo: Ultrafast 2D NMR is a powerful methodology that allows recording of a 2D NMR spectrum in a fraction of second. However, due to the numerous non-conventional parameters involved in this methodology its implementation is no trivial task. Here, an optimized experimental protocol is carefully described to ensure efficient implementation of ultrafast NMR. The ultrafast spectra resulting from this implementation are presented based on the example of two widely used 2D NMR experiments, COSY and HSQC, obtained in 0.2 s and 41 s, respectively.
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spelling Optimization and practical implementation of ultrafast 2D NMR experimentsultrafast 2D NMRCOSYHSQCUltrafast 2D NMR is a powerful methodology that allows recording of a 2D NMR spectrum in a fraction of second. However, due to the numerous non-conventional parameters involved in this methodology its implementation is no trivial task. Here, an optimized experimental protocol is carefully described to ensure efficient implementation of ultrafast NMR. The ultrafast spectra resulting from this implementation are presented based on the example of two widely used 2D NMR experiments, COSY and HSQC, obtained in 0.2 s and 41 s, respectively.Sociedade Brasileira de Química2013-01-01info:eu-repo/semantics/reportinfo:eu-repo/semantics/publishedVersiontext/htmlhttp://old.scielo.br/scielo.php?script=sci_arttext&pid=S0100-40422013000400016Química Nova v.36 n.4 2013reponame:Química Nova (Online)instname:Sociedade Brasileira de Química (SBQ)instacron:SBQ10.1590/S0100-40422013000400016info:eu-repo/semantics/openAccessQueiroz Júnior,Luiz H. K.Ferreira,Antonio G.Giraudeau,Patrickeng2013-05-17T00:00:00Zoai:scielo:S0100-40422013000400016Revistahttps://www.scielo.br/j/qn/ONGhttps://old.scielo.br/oai/scielo-oai.phpquimicanova@sbq.org.br1678-70640100-4042opendoar:2013-05-17T00:00Química Nova (Online) - Sociedade Brasileira de Química (SBQ)false
dc.title.none.fl_str_mv Optimization and practical implementation of ultrafast 2D NMR experiments
title Optimization and practical implementation of ultrafast 2D NMR experiments
spellingShingle Optimization and practical implementation of ultrafast 2D NMR experiments
Queiroz Júnior,Luiz H. K.
ultrafast 2D NMR
COSY
HSQC
title_short Optimization and practical implementation of ultrafast 2D NMR experiments
title_full Optimization and practical implementation of ultrafast 2D NMR experiments
title_fullStr Optimization and practical implementation of ultrafast 2D NMR experiments
title_full_unstemmed Optimization and practical implementation of ultrafast 2D NMR experiments
title_sort Optimization and practical implementation of ultrafast 2D NMR experiments
author Queiroz Júnior,Luiz H. K.
author_facet Queiroz Júnior,Luiz H. K.
Ferreira,Antonio G.
Giraudeau,Patrick
author_role author
author2 Ferreira,Antonio G.
Giraudeau,Patrick
author2_role author
author
dc.contributor.author.fl_str_mv Queiroz Júnior,Luiz H. K.
Ferreira,Antonio G.
Giraudeau,Patrick
dc.subject.por.fl_str_mv ultrafast 2D NMR
COSY
HSQC
topic ultrafast 2D NMR
COSY
HSQC
description Ultrafast 2D NMR is a powerful methodology that allows recording of a 2D NMR spectrum in a fraction of second. However, due to the numerous non-conventional parameters involved in this methodology its implementation is no trivial task. Here, an optimized experimental protocol is carefully described to ensure efficient implementation of ultrafast NMR. The ultrafast spectra resulting from this implementation are presented based on the example of two widely used 2D NMR experiments, COSY and HSQC, obtained in 0.2 s and 41 s, respectively.
publishDate 2013
dc.date.none.fl_str_mv 2013-01-01
dc.type.driver.fl_str_mv info:eu-repo/semantics/report
dc.type.status.fl_str_mv info:eu-repo/semantics/publishedVersion
format report
status_str publishedVersion
dc.identifier.uri.fl_str_mv http://old.scielo.br/scielo.php?script=sci_arttext&pid=S0100-40422013000400016
url http://old.scielo.br/scielo.php?script=sci_arttext&pid=S0100-40422013000400016
dc.language.iso.fl_str_mv eng
language eng
dc.relation.none.fl_str_mv 10.1590/S0100-40422013000400016
dc.rights.driver.fl_str_mv info:eu-repo/semantics/openAccess
eu_rights_str_mv openAccess
dc.format.none.fl_str_mv text/html
dc.publisher.none.fl_str_mv Sociedade Brasileira de Química
publisher.none.fl_str_mv Sociedade Brasileira de Química
dc.source.none.fl_str_mv Química Nova v.36 n.4 2013
reponame:Química Nova (Online)
instname:Sociedade Brasileira de Química (SBQ)
instacron:SBQ
instname_str Sociedade Brasileira de Química (SBQ)
instacron_str SBQ
institution SBQ
reponame_str Química Nova (Online)
collection Química Nova (Online)
repository.name.fl_str_mv Química Nova (Online) - Sociedade Brasileira de Química (SBQ)
repository.mail.fl_str_mv quimicanova@sbq.org.br
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