Complete ¹H- and 13C- Resonance Assignment of Methyl 2alpha, 3beta, 24-Tri-O-acetylurs-12-en-28-oate and Methyl 2alpha, 3beta, 24-Tri-O-acetylolean-12-en-28-oate by NMR Spectroscopy
Autor(a) principal: | |
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Data de Publicação: | 1998 |
Outros Autores: | |
Tipo de documento: | Artigo |
Idioma: | eng |
Título da fonte: | Journal of the Brazilian Chemical Society (Online) |
Texto Completo: | http://old.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50531998000100005 |
Resumo: | The complete ¹H and 13C chemical shift assignments of extended hydrogen spin systems in triterpenoid derivatives (methyl 2alpha, 3beta, 24-tri-O-acetylurs-12-en-28-oate and methyl 2alpha, 3beta, 24-tri-O-acetylolean-12-en-28-oate) was accomplished making use of one and two dimensional NMR techniques (HMBC, HMQC, COSY and NOESY). |
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Journal of the Brazilian Chemical Society (Online) |
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Complete ¹H- and 13C- Resonance Assignment of Methyl 2alpha, 3beta, 24-Tri-O-acetylurs-12-en-28-oate and Methyl 2alpha, 3beta, 24-Tri-O-acetylolean-12-en-28-oate by NMR Spectroscopytriterpenoidscomplete ¹H and 13C-NMR signal assignments1D NMR; 2D NMR (¹H x 13C-HMBC, ¹H x 13C -HMQC, ¹H x ¹H-COSY, ¹H x ¹H-NOESY)The complete ¹H and 13C chemical shift assignments of extended hydrogen spin systems in triterpenoid derivatives (methyl 2alpha, 3beta, 24-tri-O-acetylurs-12-en-28-oate and methyl 2alpha, 3beta, 24-tri-O-acetylolean-12-en-28-oate) was accomplished making use of one and two dimensional NMR techniques (HMBC, HMQC, COSY and NOESY).Sociedade Brasileira de Química1998-02-01info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersiontext/htmlhttp://old.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50531998000100005Journal of the Brazilian Chemical Society v.9 n.1 1998reponame:Journal of the Brazilian Chemical Society (Online)instname:Sociedade Brasileira de Química (SBQ)instacron:SBQ10.1590/S0103-50531998000100005info:eu-repo/semantics/openAccessMonte,F.J.Q.Kintzinger,J.P.eng2008-03-17T00:00:00Zoai:scielo:S0103-50531998000100005Revistahttp://jbcs.sbq.org.brONGhttps://old.scielo.br/oai/scielo-oai.php||office@jbcs.sbq.org.br1678-47900103-5053opendoar:2008-03-17T00:00Journal of the Brazilian Chemical Society (Online) - Sociedade Brasileira de Química (SBQ)false |
dc.title.none.fl_str_mv |
Complete ¹H- and 13C- Resonance Assignment of Methyl 2alpha, 3beta, 24-Tri-O-acetylurs-12-en-28-oate and Methyl 2alpha, 3beta, 24-Tri-O-acetylolean-12-en-28-oate by NMR Spectroscopy |
title |
Complete ¹H- and 13C- Resonance Assignment of Methyl 2alpha, 3beta, 24-Tri-O-acetylurs-12-en-28-oate and Methyl 2alpha, 3beta, 24-Tri-O-acetylolean-12-en-28-oate by NMR Spectroscopy |
spellingShingle |
Complete ¹H- and 13C- Resonance Assignment of Methyl 2alpha, 3beta, 24-Tri-O-acetylurs-12-en-28-oate and Methyl 2alpha, 3beta, 24-Tri-O-acetylolean-12-en-28-oate by NMR Spectroscopy Monte,F.J.Q. triterpenoids complete ¹H and 13C-NMR signal assignments 1D NMR; 2D NMR (¹H x 13C-HMBC, ¹H x 13C -HMQC, ¹H x ¹H-COSY, ¹H x ¹H-NOESY) |
title_short |
Complete ¹H- and 13C- Resonance Assignment of Methyl 2alpha, 3beta, 24-Tri-O-acetylurs-12-en-28-oate and Methyl 2alpha, 3beta, 24-Tri-O-acetylolean-12-en-28-oate by NMR Spectroscopy |
title_full |
Complete ¹H- and 13C- Resonance Assignment of Methyl 2alpha, 3beta, 24-Tri-O-acetylurs-12-en-28-oate and Methyl 2alpha, 3beta, 24-Tri-O-acetylolean-12-en-28-oate by NMR Spectroscopy |
title_fullStr |
Complete ¹H- and 13C- Resonance Assignment of Methyl 2alpha, 3beta, 24-Tri-O-acetylurs-12-en-28-oate and Methyl 2alpha, 3beta, 24-Tri-O-acetylolean-12-en-28-oate by NMR Spectroscopy |
title_full_unstemmed |
Complete ¹H- and 13C- Resonance Assignment of Methyl 2alpha, 3beta, 24-Tri-O-acetylurs-12-en-28-oate and Methyl 2alpha, 3beta, 24-Tri-O-acetylolean-12-en-28-oate by NMR Spectroscopy |
title_sort |
Complete ¹H- and 13C- Resonance Assignment of Methyl 2alpha, 3beta, 24-Tri-O-acetylurs-12-en-28-oate and Methyl 2alpha, 3beta, 24-Tri-O-acetylolean-12-en-28-oate by NMR Spectroscopy |
author |
Monte,F.J.Q. |
author_facet |
Monte,F.J.Q. Kintzinger,J.P. |
author_role |
author |
author2 |
Kintzinger,J.P. |
author2_role |
author |
dc.contributor.author.fl_str_mv |
Monte,F.J.Q. Kintzinger,J.P. |
dc.subject.por.fl_str_mv |
triterpenoids complete ¹H and 13C-NMR signal assignments 1D NMR; 2D NMR (¹H x 13C-HMBC, ¹H x 13C -HMQC, ¹H x ¹H-COSY, ¹H x ¹H-NOESY) |
topic |
triterpenoids complete ¹H and 13C-NMR signal assignments 1D NMR; 2D NMR (¹H x 13C-HMBC, ¹H x 13C -HMQC, ¹H x ¹H-COSY, ¹H x ¹H-NOESY) |
description |
The complete ¹H and 13C chemical shift assignments of extended hydrogen spin systems in triterpenoid derivatives (methyl 2alpha, 3beta, 24-tri-O-acetylurs-12-en-28-oate and methyl 2alpha, 3beta, 24-tri-O-acetylolean-12-en-28-oate) was accomplished making use of one and two dimensional NMR techniques (HMBC, HMQC, COSY and NOESY). |
publishDate |
1998 |
dc.date.none.fl_str_mv |
1998-02-01 |
dc.type.driver.fl_str_mv |
info:eu-repo/semantics/article |
dc.type.status.fl_str_mv |
info:eu-repo/semantics/publishedVersion |
format |
article |
status_str |
publishedVersion |
dc.identifier.uri.fl_str_mv |
http://old.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50531998000100005 |
url |
http://old.scielo.br/scielo.php?script=sci_arttext&pid=S0103-50531998000100005 |
dc.language.iso.fl_str_mv |
eng |
language |
eng |
dc.relation.none.fl_str_mv |
10.1590/S0103-50531998000100005 |
dc.rights.driver.fl_str_mv |
info:eu-repo/semantics/openAccess |
eu_rights_str_mv |
openAccess |
dc.format.none.fl_str_mv |
text/html |
dc.publisher.none.fl_str_mv |
Sociedade Brasileira de Química |
publisher.none.fl_str_mv |
Sociedade Brasileira de Química |
dc.source.none.fl_str_mv |
Journal of the Brazilian Chemical Society v.9 n.1 1998 reponame:Journal of the Brazilian Chemical Society (Online) instname:Sociedade Brasileira de Química (SBQ) instacron:SBQ |
instname_str |
Sociedade Brasileira de Química (SBQ) |
instacron_str |
SBQ |
institution |
SBQ |
reponame_str |
Journal of the Brazilian Chemical Society (Online) |
collection |
Journal of the Brazilian Chemical Society (Online) |
repository.name.fl_str_mv |
Journal of the Brazilian Chemical Society (Online) - Sociedade Brasileira de Química (SBQ) |
repository.mail.fl_str_mv |
||office@jbcs.sbq.org.br |
_version_ |
1750318163359170560 |