Propriedades mecânicas das ligas Ti34Cu36Ni8Zr22 e (TiZr)80Co12Fe8
Autor(a) principal: | |
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Data de Publicação: | 2012 |
Tipo de documento: | Tese |
Idioma: | por |
Título da fonte: | Repositório Institucional da UFSCAR |
Texto Completo: | https://repositorio.ufscar.br/handle/ufscar/701 |
Resumo: | Bulk amorphous and nanocrystalline alloys have attracted great interest from the scientific community. Titanium based alloys have demonstrated potential for formation of amorphous. This study aimed at to evaluate the mechanical properties of the Ti34Cu36Ni8Zr22 and (TiZr)80Co12Fe8 alloys, at room temperature. Thereby, nanoindentation, compression and three points bending tests were performed. The methodology involved the following steps: (i) production of alloys by arc melting under argon atmosphere, (ii) production of amorphous ribbon by melt-spinning, (iii) heat treatment of the ribbons at different temperatures, (iv) production of test specimens through casting in copper chill followed by quenching (v) microstructural characterization via scanning electron microscopy (SEM) with energy dispersive spectroscopy (EDS), transmission electron microscopy (TEM), differential scanning calorimetry (DSC) and X-ray diffraction (XRD), (vi) mechanical characterization based on nanoindentation, compression and torsion tests. The results of nanoindentation showed an increase in hardness and reduced Young's modulus as the temperature of the heat treatment approachs the crystallization temperature. Results of compression and bending showed strong dependence on the preparation surface and internal defects of the specimens. The Young's modules and tensile strengths are below those reported in the literature, probably due to internal defects present in the samples such as pores. |
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Medeiros, Marcia MoreiraBolfarini, Claudemirohttp://lattes.cnpq.br/9231627080617037http://lattes.cnpq.br/82603911215439620a82e05a-244b-42e5-8bcc-06e0f048df422016-06-02T19:10:13Z2012-12-122016-06-02T19:10:13Z2012-03-23MEDEIROS, Marcia Moreira. Mechanical Properties of Ti34Cu36Ni8Zr22 and (TiZr)80Co12Fe8 Alloys. 2012. 98 f. Tese (Doutorado em Ciências Exatas e da Terra) - Universidade Federal de São Carlos, São Carlos, 2012.https://repositorio.ufscar.br/handle/ufscar/701Bulk amorphous and nanocrystalline alloys have attracted great interest from the scientific community. Titanium based alloys have demonstrated potential for formation of amorphous. This study aimed at to evaluate the mechanical properties of the Ti34Cu36Ni8Zr22 and (TiZr)80Co12Fe8 alloys, at room temperature. Thereby, nanoindentation, compression and three points bending tests were performed. The methodology involved the following steps: (i) production of alloys by arc melting under argon atmosphere, (ii) production of amorphous ribbon by melt-spinning, (iii) heat treatment of the ribbons at different temperatures, (iv) production of test specimens through casting in copper chill followed by quenching (v) microstructural characterization via scanning electron microscopy (SEM) with energy dispersive spectroscopy (EDS), transmission electron microscopy (TEM), differential scanning calorimetry (DSC) and X-ray diffraction (XRD), (vi) mechanical characterization based on nanoindentation, compression and torsion tests. The results of nanoindentation showed an increase in hardness and reduced Young's modulus as the temperature of the heat treatment approachs the crystallization temperature. Results of compression and bending showed strong dependence on the preparation surface and internal defects of the specimens. The Young's modules and tensile strengths are below those reported in the literature, probably due to internal defects present in the samples such as pores.Ligas amorfas e nanocristalinas de grande volume vêm despertando grande interesse da comunidade científica. Ligas à base de titânio têm demonstrado potencial para formação de amorfo. O presente estudo objetivou avaliar as propriedades mecânicas, em temperatura ambiente, das ligas Ti34Cu36Ni8Zr22 e (TiZr)80Co12Fe8. Para tanto, foram realizados ensaios de nanoindentação, compressão e flexão em três pontos. A metodologia empregada envolveu as seguintes etapas: (i) produção das ligas via fusão a arco sob atmosfera de argônio; (ii) produção de fitas amorfas via melt-spinning, (iii) tratamento térmico das fitas em diferentes temperaturas, (iv) produção de corpos de prova através do vazamento em coquilha de cobre seguido de resfriamento rápido; (v) caracterização microestrutural através de microscopia eletrônica de varredura (MEV) com espectroscopia por dispersão de energia (EDS), microscopia eletrônica de transmissão (MET), calorimetria exploratória de varredura (DSC) e difratometria de raios-X (DRX); (vi) caracterização mecânica baseada em ensaios de nanoindentação, compressão e flexão em três pontos. Os resultados de nanoindentação mostraram um aumento nos valores de dureza e módulo de Young reduzido conforme o tratamento térmico se aproxima da liga cristalina. Resultados de compressão e flexão mostraram forte dependência em relação a preparação superficial e defeitos internos dos corpos de prova. Os módulos de Young e tensão de ruptura estão abaixo dos relatados pela literatura, provavelmente devido a defeitos internos presentes nas amostras, como poros.Financiadora de Estudos e Projetosapplication/pdfporUniversidade Federal de São CarlosPrograma de Pós-Graduação em Ciência e Engenharia de Materiais - PPGCEMUFSCarBRPropriedades mecânicasLigas de titânioMetal amorfoENGENHARIAS::ENGENHARIA DE MATERIAIS E METALURGICAPropriedades mecânicas das ligas Ti34Cu36Ni8Zr22 e (TiZr)80Co12Fe8Mechanical Properties of Ti34Cu36Ni8Zr22 and (TiZr)80Co12Fe8 Alloysinfo:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/doctoralThesis-1-1ea2697dd-8d22-4c7a-8bdd-487c739e04c7info:eu-repo/semantics/openAccessreponame:Repositório Institucional da UFSCARinstname:Universidade Federal de São Carlos (UFSCAR)instacron:UFSCARORIGINAL4739.pdfapplication/pdf8852417https://repositorio.ufscar.br/bitstream/ufscar/701/1/4739.pdf54d6a4b01ec455b6d6fc320e63d6dc26MD51TEXT4739.pdf.txt4739.pdf.txtExtracted texttext/plain0https://repositorio.ufscar.br/bitstream/ufscar/701/2/4739.pdf.txtd41d8cd98f00b204e9800998ecf8427eMD52THUMBNAIL4739.pdf.jpg4739.pdf.jpgIM Thumbnailimage/jpeg5770https://repositorio.ufscar.br/bitstream/ufscar/701/3/4739.pdf.jpg1651e55ca996d95ccf13433c5a65fbe4MD53ufscar/7012023-09-18 18:31:27.746oai:repositorio.ufscar.br:ufscar/701Repositório InstitucionalPUBhttps://repositorio.ufscar.br/oai/requestopendoar:43222023-09-18T18:31:27Repositório Institucional da UFSCAR - Universidade Federal de São Carlos (UFSCAR)false |
dc.title.por.fl_str_mv |
Propriedades mecânicas das ligas Ti34Cu36Ni8Zr22 e (TiZr)80Co12Fe8 |
dc.title.alternative.eng.fl_str_mv |
Mechanical Properties of Ti34Cu36Ni8Zr22 and (TiZr)80Co12Fe8 Alloys |
title |
Propriedades mecânicas das ligas Ti34Cu36Ni8Zr22 e (TiZr)80Co12Fe8 |
spellingShingle |
Propriedades mecânicas das ligas Ti34Cu36Ni8Zr22 e (TiZr)80Co12Fe8 Medeiros, Marcia Moreira Propriedades mecânicas Ligas de titânio Metal amorfo ENGENHARIAS::ENGENHARIA DE MATERIAIS E METALURGICA |
title_short |
Propriedades mecânicas das ligas Ti34Cu36Ni8Zr22 e (TiZr)80Co12Fe8 |
title_full |
Propriedades mecânicas das ligas Ti34Cu36Ni8Zr22 e (TiZr)80Co12Fe8 |
title_fullStr |
Propriedades mecânicas das ligas Ti34Cu36Ni8Zr22 e (TiZr)80Co12Fe8 |
title_full_unstemmed |
Propriedades mecânicas das ligas Ti34Cu36Ni8Zr22 e (TiZr)80Co12Fe8 |
title_sort |
Propriedades mecânicas das ligas Ti34Cu36Ni8Zr22 e (TiZr)80Co12Fe8 |
author |
Medeiros, Marcia Moreira |
author_facet |
Medeiros, Marcia Moreira |
author_role |
author |
dc.contributor.authorlattes.por.fl_str_mv |
http://lattes.cnpq.br/8260391121543962 |
dc.contributor.author.fl_str_mv |
Medeiros, Marcia Moreira |
dc.contributor.advisor1.fl_str_mv |
Bolfarini, Claudemiro |
dc.contributor.advisor1Lattes.fl_str_mv |
http://lattes.cnpq.br/9231627080617037 |
dc.contributor.authorID.fl_str_mv |
0a82e05a-244b-42e5-8bcc-06e0f048df42 |
contributor_str_mv |
Bolfarini, Claudemiro |
dc.subject.por.fl_str_mv |
Propriedades mecânicas Ligas de titânio Metal amorfo |
topic |
Propriedades mecânicas Ligas de titânio Metal amorfo ENGENHARIAS::ENGENHARIA DE MATERIAIS E METALURGICA |
dc.subject.cnpq.fl_str_mv |
ENGENHARIAS::ENGENHARIA DE MATERIAIS E METALURGICA |
description |
Bulk amorphous and nanocrystalline alloys have attracted great interest from the scientific community. Titanium based alloys have demonstrated potential for formation of amorphous. This study aimed at to evaluate the mechanical properties of the Ti34Cu36Ni8Zr22 and (TiZr)80Co12Fe8 alloys, at room temperature. Thereby, nanoindentation, compression and three points bending tests were performed. The methodology involved the following steps: (i) production of alloys by arc melting under argon atmosphere, (ii) production of amorphous ribbon by melt-spinning, (iii) heat treatment of the ribbons at different temperatures, (iv) production of test specimens through casting in copper chill followed by quenching (v) microstructural characterization via scanning electron microscopy (SEM) with energy dispersive spectroscopy (EDS), transmission electron microscopy (TEM), differential scanning calorimetry (DSC) and X-ray diffraction (XRD), (vi) mechanical characterization based on nanoindentation, compression and torsion tests. The results of nanoindentation showed an increase in hardness and reduced Young's modulus as the temperature of the heat treatment approachs the crystallization temperature. Results of compression and bending showed strong dependence on the preparation surface and internal defects of the specimens. The Young's modules and tensile strengths are below those reported in the literature, probably due to internal defects present in the samples such as pores. |
publishDate |
2012 |
dc.date.available.fl_str_mv |
2012-12-12 2016-06-02T19:10:13Z |
dc.date.issued.fl_str_mv |
2012-03-23 |
dc.date.accessioned.fl_str_mv |
2016-06-02T19:10:13Z |
dc.type.status.fl_str_mv |
info:eu-repo/semantics/publishedVersion |
dc.type.driver.fl_str_mv |
info:eu-repo/semantics/doctoralThesis |
format |
doctoralThesis |
status_str |
publishedVersion |
dc.identifier.citation.fl_str_mv |
MEDEIROS, Marcia Moreira. Mechanical Properties of Ti34Cu36Ni8Zr22 and (TiZr)80Co12Fe8 Alloys. 2012. 98 f. Tese (Doutorado em Ciências Exatas e da Terra) - Universidade Federal de São Carlos, São Carlos, 2012. |
dc.identifier.uri.fl_str_mv |
https://repositorio.ufscar.br/handle/ufscar/701 |
identifier_str_mv |
MEDEIROS, Marcia Moreira. Mechanical Properties of Ti34Cu36Ni8Zr22 and (TiZr)80Co12Fe8 Alloys. 2012. 98 f. Tese (Doutorado em Ciências Exatas e da Terra) - Universidade Federal de São Carlos, São Carlos, 2012. |
url |
https://repositorio.ufscar.br/handle/ufscar/701 |
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info:eu-repo/semantics/openAccess |
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openAccess |
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application/pdf |
dc.publisher.none.fl_str_mv |
Universidade Federal de São Carlos |
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Programa de Pós-Graduação em Ciência e Engenharia de Materiais - PPGCEM |
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UFSCar |
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BR |
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Universidade Federal de São Carlos |
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