Comportamento mecânico em fadiga da liga de titânio beta metaestável Ti-5553

Detalhes bibliográficos
Autor(a) principal: Campanelli, Leonardo Contri
Data de Publicação: 2016
Tipo de documento: Tese
Idioma: por
Título da fonte: Repositório Institucional da UFSCAR
Texto Completo: https://repositorio.ufscar.br/handle/ufscar/8627
Resumo: The microstructure of metastable beta Ti alloys is a decisive factor that governs their properties and, therefore, the assessment of the relation between the microstructure and the fatigue response means an advance in the still incipient knowledge on these alloys. The purpose of this work was to study the fatigue behavior of Ti-5Al-5Mo-5V-3Cr (Ti-5553) alloy recently developed for landing gear applications, which was kindly supplied by Boeing for this work. The material was subjected to different heat treatments (BASCA and double aging) aiming at to comprehend the influence of the alpha phase precipitation over the beta matrix, as well as to understand the effect of hydrogen even in commercially acceptable contents. BASCA microstructure comprised large laths and fine needles of primary and secondary alpha phase respectively, with a film of approximately 2 μm of thickness at grain boundaries. A refined and aligned structure of alpha phase resulted from the double aging treatment, reducing to 0.2 μm the thickness of the grain boundary alpha film. The fatigue limit at 5x106 cycles raised by the standardized staircase method initially showed an improved result for the harder microstructure, which resulted from the double aging, for 100 ppm of hydrogen. The fatigue crack nucleation, whether at the surface or subsurface, was attributed to the thickness of the grain boundary alpha film. In spite of this film brittleness, crack propagation predominantly occurred through the grains and exhibited quasi-cleavage facets and dimples. For the structure arising from the BASCA treatment, the decrease of the hydrogen content for 25 ppm led to a significant increase of the fatigue resistance as a consequence of the absence of hydrides and the higher toughness, overcoming the effect of the coarse alpha phase particles in the beta phase matrix.
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spelling Campanelli, Leonardo ContriBolfarini, Claudemirohttp://lattes.cnpq.br/9231627080617037Silva, Paulo Sergio Carvalho Pereira dahttp://lattes.cnpq.br/4783514460488161http://lattes.cnpq.br/898325923682924832f7676b-0e12-49f1-8434-192f70ce25b52017-04-18T20:16:18Z2017-04-18T20:16:18Z2016-10-14CAMPANELLI, Leonardo Contri. Comportamento mecânico em fadiga da liga de titânio beta metaestável Ti-5553. 2016. Tese (Doutorado em Ciência e Engenharia de Materiais) – Universidade Federal de São Carlos, São Carlos, 2016. Disponível em: https://repositorio.ufscar.br/handle/ufscar/8627.https://repositorio.ufscar.br/handle/ufscar/8627The microstructure of metastable beta Ti alloys is a decisive factor that governs their properties and, therefore, the assessment of the relation between the microstructure and the fatigue response means an advance in the still incipient knowledge on these alloys. The purpose of this work was to study the fatigue behavior of Ti-5Al-5Mo-5V-3Cr (Ti-5553) alloy recently developed for landing gear applications, which was kindly supplied by Boeing for this work. The material was subjected to different heat treatments (BASCA and double aging) aiming at to comprehend the influence of the alpha phase precipitation over the beta matrix, as well as to understand the effect of hydrogen even in commercially acceptable contents. BASCA microstructure comprised large laths and fine needles of primary and secondary alpha phase respectively, with a film of approximately 2 μm of thickness at grain boundaries. A refined and aligned structure of alpha phase resulted from the double aging treatment, reducing to 0.2 μm the thickness of the grain boundary alpha film. The fatigue limit at 5x106 cycles raised by the standardized staircase method initially showed an improved result for the harder microstructure, which resulted from the double aging, for 100 ppm of hydrogen. The fatigue crack nucleation, whether at the surface or subsurface, was attributed to the thickness of the grain boundary alpha film. In spite of this film brittleness, crack propagation predominantly occurred through the grains and exhibited quasi-cleavage facets and dimples. For the structure arising from the BASCA treatment, the decrease of the hydrogen content for 25 ppm led to a significant increase of the fatigue resistance as a consequence of the absence of hydrides and the higher toughness, overcoming the effect of the coarse alpha phase particles in the beta phase matrix.A microestrutura das ligas de Ti do tipo beta metaestável é fator determinante para as suas propriedades e, portanto, o estudo da relação entre a microestrutura e a resposta em fadiga representa um avanço do conhecimento, que ainda é incipiente acerca destas ligas. O presente trabalho teve como propósito estudar o comportamento em fadiga da liga Ti-5Al-5Mo- 5V-3Cr (Ti-5553) recém-desenvolvida para aplicação em trens de pouso, a qual foi gentilmente fornecida pela Boeing para este estudo. O material foi submetido a diferentes tratamentos térmicos (BASCA e duplo envelhecimento) com o intuito de compreender a influência da precipitação da fase alfa sobre a matriz beta, além de um entendimento sobre o efeito do hidrogênio mesmo em teores comercialmente admissíveis. A microestrutura BASCA constituiu-se de grandes lamelas e finas agulhas de fase alfa primária e secundária respectivamente, com um filme de aproximadamente 2 μm de espessura nos contornos de grão. Uma estrutura refinada e alinhada de fase alfa resultou do tratamento de duplo envelhecimento, reduzindo para 0,2 μm a espessura do filme nos contornos. O limite de fadiga para 5x106 ciclos determinado pelo método normatizado conhecido como staircase mostrou um resultado superior para a microestrutura com a matriz de maior resistência, no caso a obtida pelo duplo envelhecimento, para o teor de 100 ppm de hidrogênio. A nucleação da trinca de fadiga, seja superficial ou subsuperficial, foi atribuída à espessura do filme de fase alfa nos contornos de grão. Apesar da fragilidade deste filme, a propagação da trinca ocorreu predominantemente de modo transgranular e exibiu facetas de quasi-clivagem e alvéolos. Para a estrutura obtida pelo tratamento BASCA, a redução do teor de hidrogênio para 25 ppm promoveu um acréscimo significativo da resistência à fadiga como consequência da ausência de hidretos e da maior tenacidade, superando o efeito decorrente da presença de partículas grosseiras de fase alfa na matriz de fase beta.Conselho Nacional de Desenvolvimento Científico e Tecnológico (CNPq)Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)FAPESP: 2013/04423-3CNPq: 140520/2013-9porUniversidade Federal de São CarlosCâmpus São CarlosPrograma de Pós-Graduação em Ciência e Engenharia de Materiais - PPGCEMUFSCarLigas de titânioPropriedades mecânicasFadigaFraturaENGENHARIAS::ENGENHARIA DE MATERIAIS E METALURGICAComportamento mecânico em fadiga da liga de titânio beta metaestável Ti-5553Fatigue mechanical behavior of the Ti-5553 metastable beta titanium alloyinfo:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/doctoralThesisOnline600600ea2697dd-8d22-4c7a-8bdd-487c739e04c7info:eu-repo/semantics/openAccessreponame:Repositório Institucional da UFSCARinstname:Universidade Federal de São Carlos (UFSCAR)instacron:UFSCARORIGINALTeseLCC.pdfTeseLCC.pdfapplication/pdf7613727https://repositorio.ufscar.br/bitstream/ufscar/8627/1/TeseLCC.pdf65610fb91878f6307a10290b043d7673MD51LICENSElicense.txtlicense.txttext/plain; charset=utf-81957https://repositorio.ufscar.br/bitstream/ufscar/8627/2/license.txtae0398b6f8b235e40ad82cba6c50031dMD52TEXTTeseLCC.pdf.txtTeseLCC.pdf.txtExtracted texttext/plain165840https://repositorio.ufscar.br/bitstream/ufscar/8627/3/TeseLCC.pdf.txtf016e9f1cb45dc3b5e4549300da35c09MD53THUMBNAILTeseLCC.pdf.jpgTeseLCC.pdf.jpgIM Thumbnailimage/jpeg5997https://repositorio.ufscar.br/bitstream/ufscar/8627/4/TeseLCC.pdf.jpgda605661f567bd982502918fe4a9d01aMD54ufscar/86272023-09-18 18:31:09.588oai:repositorio.ufscar.br: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Repositório InstitucionalPUBhttps://repositorio.ufscar.br/oai/requestopendoar:43222023-09-18T18:31:09Repositório Institucional da UFSCAR - Universidade Federal de São Carlos (UFSCAR)false
dc.title.por.fl_str_mv Comportamento mecânico em fadiga da liga de titânio beta metaestável Ti-5553
dc.title.alternative.eng.fl_str_mv Fatigue mechanical behavior of the Ti-5553 metastable beta titanium alloy
title Comportamento mecânico em fadiga da liga de titânio beta metaestável Ti-5553
spellingShingle Comportamento mecânico em fadiga da liga de titânio beta metaestável Ti-5553
Campanelli, Leonardo Contri
Ligas de titânio
Propriedades mecânicas
Fadiga
Fratura
ENGENHARIAS::ENGENHARIA DE MATERIAIS E METALURGICA
title_short Comportamento mecânico em fadiga da liga de titânio beta metaestável Ti-5553
title_full Comportamento mecânico em fadiga da liga de titânio beta metaestável Ti-5553
title_fullStr Comportamento mecânico em fadiga da liga de titânio beta metaestável Ti-5553
title_full_unstemmed Comportamento mecânico em fadiga da liga de titânio beta metaestável Ti-5553
title_sort Comportamento mecânico em fadiga da liga de titânio beta metaestável Ti-5553
author Campanelli, Leonardo Contri
author_facet Campanelli, Leonardo Contri
author_role author
dc.contributor.authorlattes.por.fl_str_mv http://lattes.cnpq.br/8983259236829248
dc.contributor.author.fl_str_mv Campanelli, Leonardo Contri
dc.contributor.advisor1.fl_str_mv Bolfarini, Claudemiro
dc.contributor.advisor1Lattes.fl_str_mv http://lattes.cnpq.br/9231627080617037
dc.contributor.advisor-co1.fl_str_mv Silva, Paulo Sergio Carvalho Pereira da
dc.contributor.advisor-co1Lattes.fl_str_mv http://lattes.cnpq.br/4783514460488161
dc.contributor.authorID.fl_str_mv 32f7676b-0e12-49f1-8434-192f70ce25b5
contributor_str_mv Bolfarini, Claudemiro
Silva, Paulo Sergio Carvalho Pereira da
dc.subject.por.fl_str_mv Ligas de titânio
Propriedades mecânicas
Fadiga
Fratura
topic Ligas de titânio
Propriedades mecânicas
Fadiga
Fratura
ENGENHARIAS::ENGENHARIA DE MATERIAIS E METALURGICA
dc.subject.cnpq.fl_str_mv ENGENHARIAS::ENGENHARIA DE MATERIAIS E METALURGICA
description The microstructure of metastable beta Ti alloys is a decisive factor that governs their properties and, therefore, the assessment of the relation between the microstructure and the fatigue response means an advance in the still incipient knowledge on these alloys. The purpose of this work was to study the fatigue behavior of Ti-5Al-5Mo-5V-3Cr (Ti-5553) alloy recently developed for landing gear applications, which was kindly supplied by Boeing for this work. The material was subjected to different heat treatments (BASCA and double aging) aiming at to comprehend the influence of the alpha phase precipitation over the beta matrix, as well as to understand the effect of hydrogen even in commercially acceptable contents. BASCA microstructure comprised large laths and fine needles of primary and secondary alpha phase respectively, with a film of approximately 2 μm of thickness at grain boundaries. A refined and aligned structure of alpha phase resulted from the double aging treatment, reducing to 0.2 μm the thickness of the grain boundary alpha film. The fatigue limit at 5x106 cycles raised by the standardized staircase method initially showed an improved result for the harder microstructure, which resulted from the double aging, for 100 ppm of hydrogen. The fatigue crack nucleation, whether at the surface or subsurface, was attributed to the thickness of the grain boundary alpha film. In spite of this film brittleness, crack propagation predominantly occurred through the grains and exhibited quasi-cleavage facets and dimples. For the structure arising from the BASCA treatment, the decrease of the hydrogen content for 25 ppm led to a significant increase of the fatigue resistance as a consequence of the absence of hydrides and the higher toughness, overcoming the effect of the coarse alpha phase particles in the beta phase matrix.
publishDate 2016
dc.date.issued.fl_str_mv 2016-10-14
dc.date.accessioned.fl_str_mv 2017-04-18T20:16:18Z
dc.date.available.fl_str_mv 2017-04-18T20:16:18Z
dc.type.status.fl_str_mv info:eu-repo/semantics/publishedVersion
dc.type.driver.fl_str_mv info:eu-repo/semantics/doctoralThesis
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dc.identifier.citation.fl_str_mv CAMPANELLI, Leonardo Contri. Comportamento mecânico em fadiga da liga de titânio beta metaestável Ti-5553. 2016. Tese (Doutorado em Ciência e Engenharia de Materiais) – Universidade Federal de São Carlos, São Carlos, 2016. Disponível em: https://repositorio.ufscar.br/handle/ufscar/8627.
dc.identifier.uri.fl_str_mv https://repositorio.ufscar.br/handle/ufscar/8627
identifier_str_mv CAMPANELLI, Leonardo Contri. Comportamento mecânico em fadiga da liga de titânio beta metaestável Ti-5553. 2016. Tese (Doutorado em Ciência e Engenharia de Materiais) – Universidade Federal de São Carlos, São Carlos, 2016. Disponível em: https://repositorio.ufscar.br/handle/ufscar/8627.
url https://repositorio.ufscar.br/handle/ufscar/8627
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language por
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600
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dc.publisher.none.fl_str_mv Universidade Federal de São Carlos
Câmpus São Carlos
dc.publisher.program.fl_str_mv Programa de Pós-Graduação em Ciência e Engenharia de Materiais - PPGCEM
dc.publisher.initials.fl_str_mv UFSCar
publisher.none.fl_str_mv Universidade Federal de São Carlos
Câmpus São Carlos
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