Análise da presença do glicerol no comportamento fluidodinâmico de leitos fluidizados e vibrofluidizado.

Detalhes bibliográficos
Autor(a) principal: Daleffe, Roger Valeri
Data de Publicação: 2002
Tipo de documento: Dissertação
Idioma: por
Título da fonte: Repositório Institucional da UFSCAR
Texto Completo: https://repositorio.ufscar.br/handle/ufscar/4067
Resumo: Vibrofluidized beds with inert particles are often used for drying pastes in a laboratory scale. Aiming to contribute to the study of paste drying in such beds, the main purpose of this work is to analyze fluid dynamic behavior of fluidized and vibrofluidized beds as a function of parameters such as the inert particle diameter, the bed temperature, the vibrational parameter and the liquid saturation rate in the bed (defined as the quotient volume of liquid/volume of particles). Curves of pressure drop fluctuations as a function of time were obtained for the tri-phase system and the effect of those parameters on the mixture minimum velocity (as proposed by Gupta and Mujumdar, 1980a) were also analyzed. As liquid phase was employed glycerol, which have been fed into the bed in a batch mode. Glycerol was chosen because it suffers practically no evaporation at the experimental conditions. As inert particles were employed glass spheres in group D of Geldart´s classification. The vibrofluidized bed was of galvanized steel, with square-cross section of 0.20x1.10 m and height of 0.20 m. Pressure drop data and superficial air velocity data were collected by pressure transducers connected to an acquisition data system. The data were collected for vibrational ranges from 0.00 to 1.50; mean particle diameters of 1.095x10-3, 1.545x10-3 e 1,850x10-3 m; bed temperatures of 40, 50 and 60 oC and saturation rates from 0.0000 to 0.0040. The results indicate that the bed temperature does not affect significantly the pressure drop curves behavior. The vibrational parameter also shows little influence on pressure drop versus air velocity curves, excepting in the transition between fluidized and vibrofluidized beds. On the other hand, the pressure drop curves behavior is strongly affected by the increasing of the liquid saturation rate and by variation of particle diameter. Analysis of standard deviation of pressure drop fluctuations shows that for conditions which are typical of a fixed bed, the standard deviations are very small and almost independent on every parameter investigated. At fluidized bed conditions, these standard deviations are significant, particularly at the greatest air velocities. It was observed that they increase a lot in the presence of vibration, even at fixed bed conditions. Besides providing additional information on the bed fluid dynamic behavior, the curves of standard deviation of pressure drop fluctuations are also useful to identify the beginning of particle displacement into the bed due to vibration. It was observed that the methodology applied to identify the minimum fluidization velocity did not provide good results, but it worked well to identify the mixture minimum velocity as defined by Gupta and Mujundar (1980a). For the conditions investigated, the mixture minimum velocity is strongly affected by the liquid saturation rate and by the particle diameter, while both the bed temperature and the vibrational parameter show little influence on it.
id SCAR_43fc0ff77e6b068882b8cac439a92030
oai_identifier_str oai:repositorio.ufscar.br:ufscar/4067
network_acronym_str SCAR
network_name_str Repositório Institucional da UFSCAR
repository_id_str 4322
spelling Daleffe, Roger ValeriFreire, José Teixeirahttp://lattes.cnpq.br/2270677706718167http://genos.cnpq.br:12010/dwlattes/owa/prc_imp_cv_int?f_cod=K4707955U9b65db7af-569b-4289-b34c-4229660c2a7d2016-06-02T19:56:42Z2005-01-042016-06-02T19:56:42Z2002-04-18DALEFFE, Roger Valeri. Análise da presença do glicerol no comportamento fluidodinâmico de leitos fluidizados e vibrofluidizado.. 2002. 236 f. Dissertação (Mestrado em Ciências Exatas e da Terra) - Universidade Federal de São Carlos, São Carlos, 2002.https://repositorio.ufscar.br/handle/ufscar/4067Vibrofluidized beds with inert particles are often used for drying pastes in a laboratory scale. Aiming to contribute to the study of paste drying in such beds, the main purpose of this work is to analyze fluid dynamic behavior of fluidized and vibrofluidized beds as a function of parameters such as the inert particle diameter, the bed temperature, the vibrational parameter and the liquid saturation rate in the bed (defined as the quotient volume of liquid/volume of particles). Curves of pressure drop fluctuations as a function of time were obtained for the tri-phase system and the effect of those parameters on the mixture minimum velocity (as proposed by Gupta and Mujumdar, 1980a) were also analyzed. As liquid phase was employed glycerol, which have been fed into the bed in a batch mode. Glycerol was chosen because it suffers practically no evaporation at the experimental conditions. As inert particles were employed glass spheres in group D of Geldart´s classification. The vibrofluidized bed was of galvanized steel, with square-cross section of 0.20x1.10 m and height of 0.20 m. Pressure drop data and superficial air velocity data were collected by pressure transducers connected to an acquisition data system. The data were collected for vibrational ranges from 0.00 to 1.50; mean particle diameters of 1.095x10-3, 1.545x10-3 e 1,850x10-3 m; bed temperatures of 40, 50 and 60 oC and saturation rates from 0.0000 to 0.0040. The results indicate that the bed temperature does not affect significantly the pressure drop curves behavior. The vibrational parameter also shows little influence on pressure drop versus air velocity curves, excepting in the transition between fluidized and vibrofluidized beds. On the other hand, the pressure drop curves behavior is strongly affected by the increasing of the liquid saturation rate and by variation of particle diameter. Analysis of standard deviation of pressure drop fluctuations shows that for conditions which are typical of a fixed bed, the standard deviations are very small and almost independent on every parameter investigated. At fluidized bed conditions, these standard deviations are significant, particularly at the greatest air velocities. It was observed that they increase a lot in the presence of vibration, even at fixed bed conditions. Besides providing additional information on the bed fluid dynamic behavior, the curves of standard deviation of pressure drop fluctuations are also useful to identify the beginning of particle displacement into the bed due to vibration. It was observed that the methodology applied to identify the minimum fluidization velocity did not provide good results, but it worked well to identify the mixture minimum velocity as defined by Gupta and Mujundar (1980a). For the conditions investigated, the mixture minimum velocity is strongly affected by the liquid saturation rate and by the particle diameter, while both the bed temperature and the vibrational parameter show little influence on it.Os leitos vibrofluidizados vêm sendo utilizados em escala de laboratório para a secagem de pastas utilizando partículas inertes como meio para fluidização. A fim de contribuir para essa aplicação, o objetivo principal deste trabalho é analisar o comportamento fluidodinâmico dos leitos vibrofluidizado e fluidizado em função do diâmetro das partículas inertes, da temperatura no leito, do parâmetro vibracional e do grau de saturação de líquido (volume de líquido/volume de partículas). De forma complementar, objetiva-se também o estudo das curvas de desvio padrão da queda de pressão para o sistema trifásico e a análise da influência dos parâmetros sobre a velocidade mínima de mistura na forma proposta por Gupta e Mujumdar (1980a). Como líquido utilizou-se o glicerol por este praticamente não evaporar nas condições de trabalho, o qual foi alimentado em batelada, e como inertes foram utilizadas partículas de vidro classificadas no grupo D de Geldart. O equipamento utilizado foi um leito vibrofluidizado de seção retangular com 0,20 m de comprimento, 0,10 m de largura e 0,30 m de altura, construído em aço carbono galvanizado. Os dados de queda de pressão e de velocidade superficial de ar foram obtidos através de transdutores de pressão ligados em um sistema computadorizado de aquisição de dados. As análises foram feitas para intervalo de parâmetro vibracional entre 0,00 e 1,50; diâmetros médios de partículas de 1,095x10-3, 1,545x10-3 e 1,850x10-3 m, temperaturas de 40, 50 e 60 ºC e intervalo de saturação de glicerol entre 0,0000 e 0,0040. Na análise da fluidodinâmica, verificou-se que a temperatura praticamente não influenciou o comportamento da queda de pressão e com exceção da transição entre o leito fluidizado e o vibrofluidizado, a intensidade de vibração também não tornou significativa as variações da queda de pressão. Já o aumento do grau de saturação de líquido, tanto quanto a variação do diâmetro das partículas, tiveram grande influência sobre o comportamento das curvas características principalmente em relação à queda de pressão no leito. Na análise do desvio padrão da queda de pressão verificou-se que, quando o leito está na região de leito fixo ou totalmente aglomerado, o desvio padrão apresentado foi muito pequeno e praticamente independe dos parâmetros de ensaio. Quando o leito está na região de leito fluidizado o desvio padrão foi significativo, principalmente a altas velocidades de ar e foi bastante intensificado em presença de vibração, inclusive na região de leito fixo. As curvas obtidas de desvio padrão, além de fornecer informações adicionais sobre o comportamento fluidodinâmico do leito, também pode auxiliar na determinação do momento em que se inicia a movimentação das partículas no leito. Verificou-se que a metodologia utilizada para a obtenção da velocidade mínima de fluidização não apresentou resultados coerentes fisicamente, situação que foi satisfeita pela velocidade mínima de mistura da forma como foi definida por Gupta e Mujumdar (1980a). Pôde-se verificar que a temperatura praticamente não influenciou a velocidade mínima de mistura e a intensidade de vibração teve pouca influência sobre este parâmetro nas condições deste trabalho. Já o efeito da quantidade de líquido adicionado no leito e o tamanho das partículas tiveram influência considerável sobre este parâmetro.application/pdfporUniversidade Federal de São CarlosPrograma de Pós-Graduação em Engenharia Química - PPGEQUFSCarBRFluidizaçãoLeito vibrofluidizadoFluidodinâmicaGlicerolSecagem de pastasVelocidade mínima de fluidizaçãoENGENHARIAS::ENGENHARIA QUIMICAAnálise da presença do glicerol no comportamento fluidodinâmico de leitos fluidizados e vibrofluidizado.info:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/masterThesis-1-12e542afc-9fec-43b4-b11a-1eb2ed3a1f3dinfo:eu-repo/semantics/openAccessreponame:Repositório Institucional da UFSCARinstname:Universidade Federal de São Carlos (UFSCAR)instacron:UFSCARORIGINALDissRVD.pdfapplication/pdf1325863https://repositorio.ufscar.br/bitstream/ufscar/4067/1/DissRVD.pdf91591a72315d2aaffd6fb3ececca45d4MD51THUMBNAILDissRVD.pdf.jpgDissRVD.pdf.jpgIM Thumbnailimage/jpeg9960https://repositorio.ufscar.br/bitstream/ufscar/4067/2/DissRVD.pdf.jpg93edb82f2b7e01742b3badea0e70d2b5MD52ufscar/40672023-09-18 18:30:59.551oai:repositorio.ufscar.br:ufscar/4067Repositório InstitucionalPUBhttps://repositorio.ufscar.br/oai/requestopendoar:43222023-09-18T18:30:59Repositório Institucional da UFSCAR - Universidade Federal de São Carlos (UFSCAR)false
dc.title.por.fl_str_mv Análise da presença do glicerol no comportamento fluidodinâmico de leitos fluidizados e vibrofluidizado.
title Análise da presença do glicerol no comportamento fluidodinâmico de leitos fluidizados e vibrofluidizado.
spellingShingle Análise da presença do glicerol no comportamento fluidodinâmico de leitos fluidizados e vibrofluidizado.
Daleffe, Roger Valeri
Fluidização
Leito vibrofluidizado
Fluidodinâmica
Glicerol
Secagem de pastas
Velocidade mínima de fluidização
ENGENHARIAS::ENGENHARIA QUIMICA
title_short Análise da presença do glicerol no comportamento fluidodinâmico de leitos fluidizados e vibrofluidizado.
title_full Análise da presença do glicerol no comportamento fluidodinâmico de leitos fluidizados e vibrofluidizado.
title_fullStr Análise da presença do glicerol no comportamento fluidodinâmico de leitos fluidizados e vibrofluidizado.
title_full_unstemmed Análise da presença do glicerol no comportamento fluidodinâmico de leitos fluidizados e vibrofluidizado.
title_sort Análise da presença do glicerol no comportamento fluidodinâmico de leitos fluidizados e vibrofluidizado.
author Daleffe, Roger Valeri
author_facet Daleffe, Roger Valeri
author_role author
dc.contributor.authorlattes.por.fl_str_mv http://genos.cnpq.br:12010/dwlattes/owa/prc_imp_cv_int?f_cod=K4707955U9
dc.contributor.author.fl_str_mv Daleffe, Roger Valeri
dc.contributor.advisor1.fl_str_mv Freire, José Teixeira
dc.contributor.advisor1Lattes.fl_str_mv http://lattes.cnpq.br/2270677706718167
dc.contributor.authorID.fl_str_mv b65db7af-569b-4289-b34c-4229660c2a7d
contributor_str_mv Freire, José Teixeira
dc.subject.por.fl_str_mv Fluidização
Leito vibrofluidizado
Fluidodinâmica
Glicerol
Secagem de pastas
Velocidade mínima de fluidização
topic Fluidização
Leito vibrofluidizado
Fluidodinâmica
Glicerol
Secagem de pastas
Velocidade mínima de fluidização
ENGENHARIAS::ENGENHARIA QUIMICA
dc.subject.cnpq.fl_str_mv ENGENHARIAS::ENGENHARIA QUIMICA
description Vibrofluidized beds with inert particles are often used for drying pastes in a laboratory scale. Aiming to contribute to the study of paste drying in such beds, the main purpose of this work is to analyze fluid dynamic behavior of fluidized and vibrofluidized beds as a function of parameters such as the inert particle diameter, the bed temperature, the vibrational parameter and the liquid saturation rate in the bed (defined as the quotient volume of liquid/volume of particles). Curves of pressure drop fluctuations as a function of time were obtained for the tri-phase system and the effect of those parameters on the mixture minimum velocity (as proposed by Gupta and Mujumdar, 1980a) were also analyzed. As liquid phase was employed glycerol, which have been fed into the bed in a batch mode. Glycerol was chosen because it suffers practically no evaporation at the experimental conditions. As inert particles were employed glass spheres in group D of Geldart´s classification. The vibrofluidized bed was of galvanized steel, with square-cross section of 0.20x1.10 m and height of 0.20 m. Pressure drop data and superficial air velocity data were collected by pressure transducers connected to an acquisition data system. The data were collected for vibrational ranges from 0.00 to 1.50; mean particle diameters of 1.095x10-3, 1.545x10-3 e 1,850x10-3 m; bed temperatures of 40, 50 and 60 oC and saturation rates from 0.0000 to 0.0040. The results indicate that the bed temperature does not affect significantly the pressure drop curves behavior. The vibrational parameter also shows little influence on pressure drop versus air velocity curves, excepting in the transition between fluidized and vibrofluidized beds. On the other hand, the pressure drop curves behavior is strongly affected by the increasing of the liquid saturation rate and by variation of particle diameter. Analysis of standard deviation of pressure drop fluctuations shows that for conditions which are typical of a fixed bed, the standard deviations are very small and almost independent on every parameter investigated. At fluidized bed conditions, these standard deviations are significant, particularly at the greatest air velocities. It was observed that they increase a lot in the presence of vibration, even at fixed bed conditions. Besides providing additional information on the bed fluid dynamic behavior, the curves of standard deviation of pressure drop fluctuations are also useful to identify the beginning of particle displacement into the bed due to vibration. It was observed that the methodology applied to identify the minimum fluidization velocity did not provide good results, but it worked well to identify the mixture minimum velocity as defined by Gupta and Mujundar (1980a). For the conditions investigated, the mixture minimum velocity is strongly affected by the liquid saturation rate and by the particle diameter, while both the bed temperature and the vibrational parameter show little influence on it.
publishDate 2002
dc.date.issued.fl_str_mv 2002-04-18
dc.date.available.fl_str_mv 2005-01-04
2016-06-02T19:56:42Z
dc.date.accessioned.fl_str_mv 2016-06-02T19:56:42Z
dc.type.status.fl_str_mv info:eu-repo/semantics/publishedVersion
dc.type.driver.fl_str_mv info:eu-repo/semantics/masterThesis
format masterThesis
status_str publishedVersion
dc.identifier.citation.fl_str_mv DALEFFE, Roger Valeri. Análise da presença do glicerol no comportamento fluidodinâmico de leitos fluidizados e vibrofluidizado.. 2002. 236 f. Dissertação (Mestrado em Ciências Exatas e da Terra) - Universidade Federal de São Carlos, São Carlos, 2002.
dc.identifier.uri.fl_str_mv https://repositorio.ufscar.br/handle/ufscar/4067
identifier_str_mv DALEFFE, Roger Valeri. Análise da presença do glicerol no comportamento fluidodinâmico de leitos fluidizados e vibrofluidizado.. 2002. 236 f. Dissertação (Mestrado em Ciências Exatas e da Terra) - Universidade Federal de São Carlos, São Carlos, 2002.
url https://repositorio.ufscar.br/handle/ufscar/4067
dc.language.iso.fl_str_mv por
language por
dc.relation.confidence.fl_str_mv -1
-1
dc.relation.authority.fl_str_mv 2e542afc-9fec-43b4-b11a-1eb2ed3a1f3d
dc.rights.driver.fl_str_mv info:eu-repo/semantics/openAccess
eu_rights_str_mv openAccess
dc.format.none.fl_str_mv application/pdf
dc.publisher.none.fl_str_mv Universidade Federal de São Carlos
dc.publisher.program.fl_str_mv Programa de Pós-Graduação em Engenharia Química - PPGEQ
dc.publisher.initials.fl_str_mv UFSCar
dc.publisher.country.fl_str_mv BR
publisher.none.fl_str_mv Universidade Federal de São Carlos
dc.source.none.fl_str_mv reponame:Repositório Institucional da UFSCAR
instname:Universidade Federal de São Carlos (UFSCAR)
instacron:UFSCAR
instname_str Universidade Federal de São Carlos (UFSCAR)
instacron_str UFSCAR
institution UFSCAR
reponame_str Repositório Institucional da UFSCAR
collection Repositório Institucional da UFSCAR
bitstream.url.fl_str_mv https://repositorio.ufscar.br/bitstream/ufscar/4067/1/DissRVD.pdf
https://repositorio.ufscar.br/bitstream/ufscar/4067/2/DissRVD.pdf.jpg
bitstream.checksum.fl_str_mv 91591a72315d2aaffd6fb3ececca45d4
93edb82f2b7e01742b3badea0e70d2b5
bitstream.checksumAlgorithm.fl_str_mv MD5
MD5
repository.name.fl_str_mv Repositório Institucional da UFSCAR - Universidade Federal de São Carlos (UFSCAR)
repository.mail.fl_str_mv
_version_ 1802136272121102336