Estudo da resistência à fadiga da liga Ti-6Al-4V com superfície modificada por tratamento químico

Detalhes bibliográficos
Autor(a) principal: Claros, Cesar Adolfo Escobar
Data de Publicação: 2016
Tipo de documento: Dissertação
Idioma: por
Título da fonte: Repositório Institucional da UFSCAR
Texto Completo: https://repositorio.ufscar.br/handle/ufscar/8016
Resumo: Chemical surface treatments (CST) in cementless and endosseous implants are used to increase the implant-bone contact area, reducing the period of osseointegration and favouring bonding ability between implants and bone. However, surface modifications can affect the fatigue strength of these materials, especially the fatigue crack nucleation. For these reasons, this work evaluated the influence of the surface modification using acid etching, combined with alkaline treatment on the fatigue strength of Ti-6Al-4V ELI alloy. The topography developed by chemical surface treatments was examined by scanning electron microscopy (SEM) and confocal laser scanning microscopy (CLSM). Increased roughness and the effective surface area were investigated and compared with the Ti-6Al-4V samples without modification. Surface composition was analyzed by energy dispersive X-ray spectroscopy (EDS). Axial fatigue resistances of polished and modified surfaces were determined by stepwise load increase tests and staircase test method. Finally, SEM was employed to examine the fracture surface of the tested specimens. According to the results, it was observed a similar fatigue behavior of the chemically treated Ti-6Al-4V alloy compared to the samples without treatment.
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spelling Claros, Cesar Adolfo EscobarBolfarini, Claudemirohttp://lattes.cnpq.br/9231627080617037Oliveira, Diego Pedreira dehttp://lattes.cnpq.br/8388790875028551http://lattes.cnpq.br/68781561718172088da62d5b-2435-4b80-b12e-b3fb50e16ae92016-10-20T18:49:14Z2016-10-20T18:49:14Z2016-03-22CLAROS, Cesar Adolfo Escobar. Estudo da resistência à fadiga da liga Ti-6Al-4V com superfície modificada por tratamento químico. 2016. Dissertação (Mestrado em Ciência e Engenharia de Materiais) – Universidade Federal de São Carlos, São Carlos, 2016. Disponível em: https://repositorio.ufscar.br/handle/ufscar/8016.https://repositorio.ufscar.br/handle/ufscar/8016Chemical surface treatments (CST) in cementless and endosseous implants are used to increase the implant-bone contact area, reducing the period of osseointegration and favouring bonding ability between implants and bone. However, surface modifications can affect the fatigue strength of these materials, especially the fatigue crack nucleation. For these reasons, this work evaluated the influence of the surface modification using acid etching, combined with alkaline treatment on the fatigue strength of Ti-6Al-4V ELI alloy. The topography developed by chemical surface treatments was examined by scanning electron microscopy (SEM) and confocal laser scanning microscopy (CLSM). Increased roughness and the effective surface area were investigated and compared with the Ti-6Al-4V samples without modification. Surface composition was analyzed by energy dispersive X-ray spectroscopy (EDS). Axial fatigue resistances of polished and modified surfaces were determined by stepwise load increase tests and staircase test method. Finally, SEM was employed to examine the fracture surface of the tested specimens. According to the results, it was observed a similar fatigue behavior of the chemically treated Ti-6Al-4V alloy compared to the samples without treatment.Tratamentos químicos sobre a superfície dos implantes intra-ósseos são usados para aumentar a área de contato do par implante-osso, diminuindo o período de osseointegração e favorecendo a capacidade de ligação entre o implante e o osso. No entanto, modificações de superfície podem afetar a resistência à fadiga destes materiais, especialmente quanto a nucleação de trinca por fadiga. Por estas razões, este trabalho avaliou e analisou a influência na resistência à fadiga das ligas de Ti-6Al-4V ELI com modificações na superfície, geradas por tratamentos ácidos e um posterior tratamento alcalino. A mudança na topografia promovida pelos tratamentos químicos foi examinada com microscopia eletrônica de varredura (MEV) e microscopia confocal de varredura a LASER (CLSM). O aumento da rugosidade e da área efetiva de contato foram estudadas e comparadas com as amostras de Ti-6Al-4V sem modificação. A composição química da superfície foi analisada por espectroscopia com energia dispersiva de raios-X (EDS). A resistência axial à fadiga dos corpos-de-prova polidos e modificados foi determinada pelo método escalonado de tensões e o método “staircase”. Finalmente, Imagens por MEV foram usadas para examinar a superfície de fratura dos espécimenes fraturados após serem testados à fadiga. De acordo com os resultados obtidos, observou-se um comportamento semelhante no desempenho à fadiga do material com a superfície tratada quimicamente com H3PO4 ou HCl e posteriormente com NaOH, em comparação com o sem tratamento.Não recebi financiamentoporUniversidade Federal de São CarlosCâmpus São CarlosPrograma de Pós-Graduação em Ciência e Engenharia de Materiais - PPGCEMUFSCarTitânioFadigaTratamento químicoTratamento da superfícieBiomateriaisENGENHARIAS::ENGENHARIA DE MATERIAIS E METALURGICAEstudo da resistência à fadiga da liga Ti-6Al-4V com superfície modificada por tratamento químicoFatigue behavior of Ti-6Al-4v alloy with surface modified by chemical treatmentinfo:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/masterThesisOnline600600ea2697dd-8d22-4c7a-8bdd-487c739e04c7info:eu-repo/semantics/openAccessreponame:Repositório Institucional da UFSCARinstname:Universidade Federal de São Carlos (UFSCAR)instacron:UFSCARORIGINALDissCAEC.pdfDissCAEC.pdfapplication/pdf4586918https://repositorio.ufscar.br/bitstream/ufscar/8016/1/DissCAEC.pdf8999e545d069d3ff24ef2b22f83a3b31MD51LICENSElicense.txtlicense.txttext/plain; charset=utf-81957https://repositorio.ufscar.br/bitstream/ufscar/8016/2/license.txtae0398b6f8b235e40ad82cba6c50031dMD52TEXTDissCAEC.pdf.txtDissCAEC.pdf.txtExtracted texttext/plain126907https://repositorio.ufscar.br/bitstream/ufscar/8016/3/DissCAEC.pdf.txtdd9e4bfe891bdbb0d330ba59cb6a6d8eMD53THUMBNAILDissCAEC.pdf.jpgDissCAEC.pdf.jpgIM Thumbnailimage/jpeg6434https://repositorio.ufscar.br/bitstream/ufscar/8016/4/DissCAEC.pdf.jpg8b1e05ca1ff105183811865bbd1f9b8dMD54ufscar/80162023-09-18 18:31:48.671oai:repositorio.ufscar.br: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Repositório InstitucionalPUBhttps://repositorio.ufscar.br/oai/requestopendoar:43222023-09-18T18:31:48Repositório Institucional da UFSCAR - Universidade Federal de São Carlos (UFSCAR)false
dc.title.por.fl_str_mv Estudo da resistência à fadiga da liga Ti-6Al-4V com superfície modificada por tratamento químico
dc.title.alternative.eng.fl_str_mv Fatigue behavior of Ti-6Al-4v alloy with surface modified by chemical treatment
title Estudo da resistência à fadiga da liga Ti-6Al-4V com superfície modificada por tratamento químico
spellingShingle Estudo da resistência à fadiga da liga Ti-6Al-4V com superfície modificada por tratamento químico
Claros, Cesar Adolfo Escobar
Titânio
Fadiga
Tratamento químico
Tratamento da superfície
Biomateriais
ENGENHARIAS::ENGENHARIA DE MATERIAIS E METALURGICA
title_short Estudo da resistência à fadiga da liga Ti-6Al-4V com superfície modificada por tratamento químico
title_full Estudo da resistência à fadiga da liga Ti-6Al-4V com superfície modificada por tratamento químico
title_fullStr Estudo da resistência à fadiga da liga Ti-6Al-4V com superfície modificada por tratamento químico
title_full_unstemmed Estudo da resistência à fadiga da liga Ti-6Al-4V com superfície modificada por tratamento químico
title_sort Estudo da resistência à fadiga da liga Ti-6Al-4V com superfície modificada por tratamento químico
author Claros, Cesar Adolfo Escobar
author_facet Claros, Cesar Adolfo Escobar
author_role author
dc.contributor.authorlattes.por.fl_str_mv http://lattes.cnpq.br/6878156171817208
dc.contributor.author.fl_str_mv Claros, Cesar Adolfo Escobar
dc.contributor.advisor1.fl_str_mv Bolfarini, Claudemiro
dc.contributor.advisor1Lattes.fl_str_mv http://lattes.cnpq.br/9231627080617037
dc.contributor.advisor-co1.fl_str_mv Oliveira, Diego Pedreira de
dc.contributor.advisor-co1Lattes.fl_str_mv http://lattes.cnpq.br/8388790875028551
dc.contributor.authorID.fl_str_mv 8da62d5b-2435-4b80-b12e-b3fb50e16ae9
contributor_str_mv Bolfarini, Claudemiro
Oliveira, Diego Pedreira de
dc.subject.por.fl_str_mv Titânio
Fadiga
Tratamento químico
Tratamento da superfície
Biomateriais
topic Titânio
Fadiga
Tratamento químico
Tratamento da superfície
Biomateriais
ENGENHARIAS::ENGENHARIA DE MATERIAIS E METALURGICA
dc.subject.cnpq.fl_str_mv ENGENHARIAS::ENGENHARIA DE MATERIAIS E METALURGICA
description Chemical surface treatments (CST) in cementless and endosseous implants are used to increase the implant-bone contact area, reducing the period of osseointegration and favouring bonding ability between implants and bone. However, surface modifications can affect the fatigue strength of these materials, especially the fatigue crack nucleation. For these reasons, this work evaluated the influence of the surface modification using acid etching, combined with alkaline treatment on the fatigue strength of Ti-6Al-4V ELI alloy. The topography developed by chemical surface treatments was examined by scanning electron microscopy (SEM) and confocal laser scanning microscopy (CLSM). Increased roughness and the effective surface area were investigated and compared with the Ti-6Al-4V samples without modification. Surface composition was analyzed by energy dispersive X-ray spectroscopy (EDS). Axial fatigue resistances of polished and modified surfaces were determined by stepwise load increase tests and staircase test method. Finally, SEM was employed to examine the fracture surface of the tested specimens. According to the results, it was observed a similar fatigue behavior of the chemically treated Ti-6Al-4V alloy compared to the samples without treatment.
publishDate 2016
dc.date.accessioned.fl_str_mv 2016-10-20T18:49:14Z
dc.date.available.fl_str_mv 2016-10-20T18:49:14Z
dc.date.issued.fl_str_mv 2016-03-22
dc.type.status.fl_str_mv info:eu-repo/semantics/publishedVersion
dc.type.driver.fl_str_mv info:eu-repo/semantics/masterThesis
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status_str publishedVersion
dc.identifier.citation.fl_str_mv CLAROS, Cesar Adolfo Escobar. Estudo da resistência à fadiga da liga Ti-6Al-4V com superfície modificada por tratamento químico. 2016. Dissertação (Mestrado em Ciência e Engenharia de Materiais) – Universidade Federal de São Carlos, São Carlos, 2016. Disponível em: https://repositorio.ufscar.br/handle/ufscar/8016.
dc.identifier.uri.fl_str_mv https://repositorio.ufscar.br/handle/ufscar/8016
identifier_str_mv CLAROS, Cesar Adolfo Escobar. Estudo da resistência à fadiga da liga Ti-6Al-4V com superfície modificada por tratamento químico. 2016. Dissertação (Mestrado em Ciência e Engenharia de Materiais) – Universidade Federal de São Carlos, São Carlos, 2016. Disponível em: https://repositorio.ufscar.br/handle/ufscar/8016.
url https://repositorio.ufscar.br/handle/ufscar/8016
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Câmpus São Carlos
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publisher.none.fl_str_mv Universidade Federal de São Carlos
Câmpus São Carlos
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