Spectrophotometric and inductively coupled plasma atomic emission spectrometric determination of titanium in ilmenites after rapid dissolution with phosphoric acid
Autor(a) principal: | |
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Data de Publicação: | 1997 |
Outros Autores: | , , , , , |
Tipo de documento: | Artigo |
Idioma: | eng |
Título da fonte: | Repositório Institucional da UFBA |
Texto Completo: | http://www.repositorio.ufba.br/ri/handle/ri/8339 |
Resumo: | Texto completo: acesso restrito. p.165-168 |
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Andrade, Jailson Bittencourt deNunes, Genebaldo S.Veiga, Merilio P.Costa, Antonio Celso SpinolaFerreira, Sergio Luis CostaAmorim, Adelaide Maria MendonçaReis, Selma T.Andrade, Jailson Bittencourt deNunes, Genebaldo S.Veiga, Merilio P.Costa, Antonio Celso SpinolaFerreira, Sergio Luis CostaAmorim, Adelaide Maria MendonçaReis, Selma T.2013-02-04T15:18:56Z19970039-9140http://www.repositorio.ufba.br/ri/handle/ri/8339v. 44, n. 2Texto completo: acesso restrito. p.165-168The use of 85% phosphoric acid in borosilicate conical flasks for the dissolution of ilmenites at 230 ± 10°C is reported. The samples were quantitatively dissolved in less than 13 min. Titanium was determined by both spectrophotometry and inductively coupled plasma atomic emission spectrometry ICP-AES. Vanadium and iron were determined by ICP-AES. In several samples of ilmenites analyzed, the TiO2 concentration was in the range 10.6–57.5% and those of FeO and V2O5 were in the ranges 31.6–51.4% and 0.39–1.32%, respectively. In the spectrophotometric method, vanadium interference occurs only when the View the MathML source concentration ratio is <4. In all samples analyzed this ratio was around 12, resulting in no interferences due to vanadium. Hence the ilmenite dissolution procedure using phosphoric acid was compatible with titanium quantification by both spectrophotometry and ICP-AES.Submitted by Suelen Reis (suelen_suzane@hotmail.com) on 2013-02-04T15:18:56Z No. of bitstreams: 1 Andrade.pdf: 257256 bytes, checksum: 4716d640c581bb68a486dc1895e0a52e (MD5)Made available in DSpace on 2013-02-04T15:18:56Z (GMT). No. of bitstreams: 1 Andrade.pdf: 257256 bytes, checksum: 4716d640c581bb68a486dc1895e0a52e (MD5) Previous issue date: 1997http://dx.doi.org/10.1016/S0039-9140(96)02026-7reponame:Repositório Institucional da UFBAinstname:Universidade Federal da Bahia (UFBA)instacron:UFBAInductively coupled plasma atomic emission spectrometryllmenitesPhosphoric acid dissolutionSpectrophotometryTitaniumSpectrophotometric and inductively coupled plasma atomic emission spectrometric determination of titanium in ilmenites after rapid dissolution with phosphoric acidTalantainfo:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/article10000-01-01enginfo:eu-repo/semantics/openAccessORIGINALAndrade.pdfAndrade.pdfapplication/pdf257256https://repositorio.ufba.br/bitstream/ri/8339/1/Andrade.pdf4716d640c581bb68a486dc1895e0a52eMD51LICENSElicense.txtlicense.txttext/plain1762https://repositorio.ufba.br/bitstream/ri/8339/2/license.txt1b89a9a0548218172d7c829f87a0eab9MD52TEXTAndrade.pdf.txtAndrade.pdf.txtExtracted texttext/plain11486https://repositorio.ufba.br/bitstream/ri/8339/3/Andrade.pdf.txt0f4aa399025c566525cbb8e4914dac69MD53ri/83392022-08-08 13:17:28.293oai:repositorio.ufba.br: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Repositório InstitucionalPUBhttp://192.188.11.11:8080/oai/requestopendoar:19322022-08-08T16:17:28Repositório Institucional da UFBA - Universidade Federal da Bahia (UFBA)false |
dc.title.pt_BR.fl_str_mv |
Spectrophotometric and inductively coupled plasma atomic emission spectrometric determination of titanium in ilmenites after rapid dissolution with phosphoric acid |
dc.title.alternative.pt_BR.fl_str_mv |
Talanta |
title |
Spectrophotometric and inductively coupled plasma atomic emission spectrometric determination of titanium in ilmenites after rapid dissolution with phosphoric acid |
spellingShingle |
Spectrophotometric and inductively coupled plasma atomic emission spectrometric determination of titanium in ilmenites after rapid dissolution with phosphoric acid Andrade, Jailson Bittencourt de Inductively coupled plasma atomic emission spectrometry llmenites Phosphoric acid dissolution Spectrophotometry Titanium |
title_short |
Spectrophotometric and inductively coupled plasma atomic emission spectrometric determination of titanium in ilmenites after rapid dissolution with phosphoric acid |
title_full |
Spectrophotometric and inductively coupled plasma atomic emission spectrometric determination of titanium in ilmenites after rapid dissolution with phosphoric acid |
title_fullStr |
Spectrophotometric and inductively coupled plasma atomic emission spectrometric determination of titanium in ilmenites after rapid dissolution with phosphoric acid |
title_full_unstemmed |
Spectrophotometric and inductively coupled plasma atomic emission spectrometric determination of titanium in ilmenites after rapid dissolution with phosphoric acid |
title_sort |
Spectrophotometric and inductively coupled plasma atomic emission spectrometric determination of titanium in ilmenites after rapid dissolution with phosphoric acid |
author |
Andrade, Jailson Bittencourt de |
author_facet |
Andrade, Jailson Bittencourt de Nunes, Genebaldo S. Veiga, Merilio P. Costa, Antonio Celso Spinola Ferreira, Sergio Luis Costa Amorim, Adelaide Maria Mendonça Reis, Selma T. |
author_role |
author |
author2 |
Nunes, Genebaldo S. Veiga, Merilio P. Costa, Antonio Celso Spinola Ferreira, Sergio Luis Costa Amorim, Adelaide Maria Mendonça Reis, Selma T. |
author2_role |
author author author author author author |
dc.contributor.author.fl_str_mv |
Andrade, Jailson Bittencourt de Nunes, Genebaldo S. Veiga, Merilio P. Costa, Antonio Celso Spinola Ferreira, Sergio Luis Costa Amorim, Adelaide Maria Mendonça Reis, Selma T. Andrade, Jailson Bittencourt de Nunes, Genebaldo S. Veiga, Merilio P. Costa, Antonio Celso Spinola Ferreira, Sergio Luis Costa Amorim, Adelaide Maria Mendonça Reis, Selma T. |
dc.subject.por.fl_str_mv |
Inductively coupled plasma atomic emission spectrometry llmenites Phosphoric acid dissolution Spectrophotometry Titanium |
topic |
Inductively coupled plasma atomic emission spectrometry llmenites Phosphoric acid dissolution Spectrophotometry Titanium |
description |
Texto completo: acesso restrito. p.165-168 |
publishDate |
1997 |
dc.date.issued.fl_str_mv |
1997 |
dc.date.accessioned.fl_str_mv |
2013-02-04T15:18:56Z |
dc.type.status.fl_str_mv |
info:eu-repo/semantics/publishedVersion |
dc.type.driver.fl_str_mv |
info:eu-repo/semantics/article |
format |
article |
status_str |
publishedVersion |
dc.identifier.uri.fl_str_mv |
http://www.repositorio.ufba.br/ri/handle/ri/8339 |
dc.identifier.issn.none.fl_str_mv |
0039-9140 |
dc.identifier.number.pt_BR.fl_str_mv |
v. 44, n. 2 |
identifier_str_mv |
0039-9140 v. 44, n. 2 |
url |
http://www.repositorio.ufba.br/ri/handle/ri/8339 |
dc.language.iso.fl_str_mv |
eng |
language |
eng |
dc.rights.driver.fl_str_mv |
info:eu-repo/semantics/openAccess |
eu_rights_str_mv |
openAccess |
dc.source.pt_BR.fl_str_mv |
http://dx.doi.org/10.1016/S0039-9140(96)02026-7 |
dc.source.none.fl_str_mv |
reponame:Repositório Institucional da UFBA instname:Universidade Federal da Bahia (UFBA) instacron:UFBA |
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Universidade Federal da Bahia (UFBA) |
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UFBA |
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UFBA |
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Repositório Institucional da UFBA |
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Repositório Institucional da UFBA |
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