Spectrophotometric and inductively coupled plasma atomic emission spectrometric determination of titanium in ilmenites after rapid dissolution with phosphoric acid

Detalhes bibliográficos
Autor(a) principal: Andrade, Jailson Bittencourt de
Data de Publicação: 1997
Outros Autores: Nunes, Genebaldo S., Veiga, Merilio P., Costa, Antonio Celso Spinola, Ferreira, Sergio Luis Costa, Amorim, Adelaide Maria Mendonça, Reis, Selma T.
Tipo de documento: Artigo
Idioma: eng
Título da fonte: Repositório Institucional da UFBA
Texto Completo: http://www.repositorio.ufba.br/ri/handle/ri/8339
Resumo: Texto completo: acesso restrito. p.165-168
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spelling Andrade, Jailson Bittencourt deNunes, Genebaldo S.Veiga, Merilio P.Costa, Antonio Celso SpinolaFerreira, Sergio Luis CostaAmorim, Adelaide Maria MendonçaReis, Selma T.Andrade, Jailson Bittencourt deNunes, Genebaldo S.Veiga, Merilio P.Costa, Antonio Celso SpinolaFerreira, Sergio Luis CostaAmorim, Adelaide Maria MendonçaReis, Selma T.2013-02-04T15:18:56Z19970039-9140http://www.repositorio.ufba.br/ri/handle/ri/8339v. 44, n. 2Texto completo: acesso restrito. p.165-168The use of 85% phosphoric acid in borosilicate conical flasks for the dissolution of ilmenites at 230 ± 10°C is reported. The samples were quantitatively dissolved in less than 13 min. Titanium was determined by both spectrophotometry and inductively coupled plasma atomic emission spectrometry ICP-AES. Vanadium and iron were determined by ICP-AES. In several samples of ilmenites analyzed, the TiO2 concentration was in the range 10.6–57.5% and those of FeO and V2O5 were in the ranges 31.6–51.4% and 0.39–1.32%, respectively. In the spectrophotometric method, vanadium interference occurs only when the View the MathML source concentration ratio is <4. In all samples analyzed this ratio was around 12, resulting in no interferences due to vanadium. Hence the ilmenite dissolution procedure using phosphoric acid was compatible with titanium quantification by both spectrophotometry and ICP-AES.Submitted by Suelen Reis (suelen_suzane@hotmail.com) on 2013-02-04T15:18:56Z No. of bitstreams: 1 Andrade.pdf: 257256 bytes, checksum: 4716d640c581bb68a486dc1895e0a52e (MD5)Made available in DSpace on 2013-02-04T15:18:56Z (GMT). No. of bitstreams: 1 Andrade.pdf: 257256 bytes, checksum: 4716d640c581bb68a486dc1895e0a52e (MD5) Previous issue date: 1997http://dx.doi.org/10.1016/S0039-9140(96)02026-7reponame:Repositório Institucional da UFBAinstname:Universidade Federal da Bahia (UFBA)instacron:UFBAInductively coupled plasma atomic emission spectrometryllmenitesPhosphoric acid dissolutionSpectrophotometryTitaniumSpectrophotometric and inductively coupled plasma atomic emission spectrometric determination of titanium in ilmenites after rapid dissolution with phosphoric acidTalantainfo:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/article10000-01-01enginfo:eu-repo/semantics/openAccessORIGINALAndrade.pdfAndrade.pdfapplication/pdf257256https://repositorio.ufba.br/bitstream/ri/8339/1/Andrade.pdf4716d640c581bb68a486dc1895e0a52eMD51LICENSElicense.txtlicense.txttext/plain1762https://repositorio.ufba.br/bitstream/ri/8339/2/license.txt1b89a9a0548218172d7c829f87a0eab9MD52TEXTAndrade.pdf.txtAndrade.pdf.txtExtracted texttext/plain11486https://repositorio.ufba.br/bitstream/ri/8339/3/Andrade.pdf.txt0f4aa399025c566525cbb8e4914dac69MD53ri/83392022-08-08 13:17:28.293oai:repositorio.ufba.br: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Repositório InstitucionalPUBhttp://192.188.11.11:8080/oai/requestopendoar:19322022-08-08T16:17:28Repositório Institucional da UFBA - Universidade Federal da Bahia (UFBA)false
dc.title.pt_BR.fl_str_mv Spectrophotometric and inductively coupled plasma atomic emission spectrometric determination of titanium in ilmenites after rapid dissolution with phosphoric acid
dc.title.alternative.pt_BR.fl_str_mv Talanta
title Spectrophotometric and inductively coupled plasma atomic emission spectrometric determination of titanium in ilmenites after rapid dissolution with phosphoric acid
spellingShingle Spectrophotometric and inductively coupled plasma atomic emission spectrometric determination of titanium in ilmenites after rapid dissolution with phosphoric acid
Andrade, Jailson Bittencourt de
Inductively coupled plasma atomic emission spectrometry
llmenites
Phosphoric acid dissolution
Spectrophotometry
Titanium
title_short Spectrophotometric and inductively coupled plasma atomic emission spectrometric determination of titanium in ilmenites after rapid dissolution with phosphoric acid
title_full Spectrophotometric and inductively coupled plasma atomic emission spectrometric determination of titanium in ilmenites after rapid dissolution with phosphoric acid
title_fullStr Spectrophotometric and inductively coupled plasma atomic emission spectrometric determination of titanium in ilmenites after rapid dissolution with phosphoric acid
title_full_unstemmed Spectrophotometric and inductively coupled plasma atomic emission spectrometric determination of titanium in ilmenites after rapid dissolution with phosphoric acid
title_sort Spectrophotometric and inductively coupled plasma atomic emission spectrometric determination of titanium in ilmenites after rapid dissolution with phosphoric acid
author Andrade, Jailson Bittencourt de
author_facet Andrade, Jailson Bittencourt de
Nunes, Genebaldo S.
Veiga, Merilio P.
Costa, Antonio Celso Spinola
Ferreira, Sergio Luis Costa
Amorim, Adelaide Maria Mendonça
Reis, Selma T.
author_role author
author2 Nunes, Genebaldo S.
Veiga, Merilio P.
Costa, Antonio Celso Spinola
Ferreira, Sergio Luis Costa
Amorim, Adelaide Maria Mendonça
Reis, Selma T.
author2_role author
author
author
author
author
author
dc.contributor.author.fl_str_mv Andrade, Jailson Bittencourt de
Nunes, Genebaldo S.
Veiga, Merilio P.
Costa, Antonio Celso Spinola
Ferreira, Sergio Luis Costa
Amorim, Adelaide Maria Mendonça
Reis, Selma T.
Andrade, Jailson Bittencourt de
Nunes, Genebaldo S.
Veiga, Merilio P.
Costa, Antonio Celso Spinola
Ferreira, Sergio Luis Costa
Amorim, Adelaide Maria Mendonça
Reis, Selma T.
dc.subject.por.fl_str_mv Inductively coupled plasma atomic emission spectrometry
llmenites
Phosphoric acid dissolution
Spectrophotometry
Titanium
topic Inductively coupled plasma atomic emission spectrometry
llmenites
Phosphoric acid dissolution
Spectrophotometry
Titanium
description Texto completo: acesso restrito. p.165-168
publishDate 1997
dc.date.issued.fl_str_mv 1997
dc.date.accessioned.fl_str_mv 2013-02-04T15:18:56Z
dc.type.status.fl_str_mv info:eu-repo/semantics/publishedVersion
dc.type.driver.fl_str_mv info:eu-repo/semantics/article
format article
status_str publishedVersion
dc.identifier.uri.fl_str_mv http://www.repositorio.ufba.br/ri/handle/ri/8339
dc.identifier.issn.none.fl_str_mv 0039-9140
dc.identifier.number.pt_BR.fl_str_mv v. 44, n. 2
identifier_str_mv 0039-9140
v. 44, n. 2
url http://www.repositorio.ufba.br/ri/handle/ri/8339
dc.language.iso.fl_str_mv eng
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dc.rights.driver.fl_str_mv info:eu-repo/semantics/openAccess
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