Otimização das condições do processo de secagem do extrato de café em leito de espuma e aplicação em mistura para cappuccino

Detalhes bibliográficos
Autor(a) principal: Maciel, Kátia Silva
Data de Publicação: 2017
Tipo de documento: Dissertação
Idioma: por
Título da fonte: Repositório Institucional da Universidade Federal do Espírito Santo (riUfes)
Texto Completo: http://repositorio.ufes.br/handle/10/8100
Resumo: As a result of consumers' preference for quality of products and time of preparation, there is an increasing demand related to soluble coffee, both for consumption and as an ingredient in various coffee products, such as cappuccino. In the processing of soluble coffee there are transformations and aromatic losses, that can negatively alter the flavor and aroma of the coffee. Facing such problems, the foam mat is an alternative technology for soluble coffee production. This process is low cost, low temperatures and drying time; in addition, the use of foaming agents allows the formation of a stable foam throughout the drying process, increasing the area exposed to hot air, which the evaporation is facilitated through the spaces filled with air, allowing a greater retention of aromas and compounds, as well as obtaining a porous product with easy rehydration. In this context, the objective of this study was to optimize the conditions of the soluble coffee production process by the foam mat drying method. The experiment was divided into two phases. Initially, the influence of different levels of maltodextrin and whey proteins on the foam production of the coffee extract obtained through the Rotational Central Compound Design were investigated. In the second phase, the effect of different drying air temperatures on the production of dehydrated coffee, was to evaluate, in which the ideal concentration of agents obtained in the previous phase was used. The desirability function was used to define the optimal conditions of the process to obtain powders with the most desirable characteristics in both phases. For this, the following response variables were evaluated: a) related to the coffee extract foam: density and coalescence index; b) related to foam mat drying: drying time; c) related to the powders obtained (dehydrated coffee): solubility, antioxidant activity (DPPH and ABTS), wettability and moisture; d) related to the sensorial analysis of cappuccino: sensorial acceptance. The physicochemical characterization of the obtained powders was performed in relation to water activity, color, pH and acidity. In addition, the study of the drying kinetics of foams was also assessed. Results revealed that the combination of 1.32% maltodextrin and 2.64% whey proteins obtained greater overall desirability (0.6503), since the most desirable characteristics (maximization of flavor acceptance, aroma, the overall impression and antioxidant activity (ABTS and DPPH) and minimization of coalescence index, drying time, wettability and moisture were obtained with this combination. The foam density and solubility of the powders had no influence. In the second phase, the maximum desirability obtained was 0.726 at the drying temperature of 61.77 ºC. The variable sensory acceptance (flavor) was maximized and the variables drying, wettability and moisture were minimized. The different drying temperatures did not influence the variables antioxidant activity (ABTS and DPPH) and solubility. In the physical-chemical characterization of the powders, obtained with different concentrations of agents, there was an influence on the variables color, pH, acidity and water activity. In the powders obtained at different temperatures, a significant difference occurred only in the water activity response variable. It is concluded that the foam formation with 1.32% maltodextrin and 2.64% whey proteins, using the temperature of 61.77 oC for drying, are the optimal conditions for the drying process of the extract coffee in foam mat.
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spelling Teixeira, Luciano José QuintãoDella Lucia, Suzana MariaSaraiva, Sérgio HenriquesMaciel, Kátia SilvaLima Filho, Tarcísio2018-08-01T23:19:04Z2018-08-012018-08-01T23:19:04Z2017-02-21As a result of consumers' preference for quality of products and time of preparation, there is an increasing demand related to soluble coffee, both for consumption and as an ingredient in various coffee products, such as cappuccino. In the processing of soluble coffee there are transformations and aromatic losses, that can negatively alter the flavor and aroma of the coffee. Facing such problems, the foam mat is an alternative technology for soluble coffee production. This process is low cost, low temperatures and drying time; in addition, the use of foaming agents allows the formation of a stable foam throughout the drying process, increasing the area exposed to hot air, which the evaporation is facilitated through the spaces filled with air, allowing a greater retention of aromas and compounds, as well as obtaining a porous product with easy rehydration. In this context, the objective of this study was to optimize the conditions of the soluble coffee production process by the foam mat drying method. The experiment was divided into two phases. Initially, the influence of different levels of maltodextrin and whey proteins on the foam production of the coffee extract obtained through the Rotational Central Compound Design were investigated. In the second phase, the effect of different drying air temperatures on the production of dehydrated coffee, was to evaluate, in which the ideal concentration of agents obtained in the previous phase was used. The desirability function was used to define the optimal conditions of the process to obtain powders with the most desirable characteristics in both phases. For this, the following response variables were evaluated: a) related to the coffee extract foam: density and coalescence index; b) related to foam mat drying: drying time; c) related to the powders obtained (dehydrated coffee): solubility, antioxidant activity (DPPH and ABTS), wettability and moisture; d) related to the sensorial analysis of cappuccino: sensorial acceptance. The physicochemical characterization of the obtained powders was performed in relation to water activity, color, pH and acidity. In addition, the study of the drying kinetics of foams was also assessed. Results revealed that the combination of 1.32% maltodextrin and 2.64% whey proteins obtained greater overall desirability (0.6503), since the most desirable characteristics (maximization of flavor acceptance, aroma, the overall impression and antioxidant activity (ABTS and DPPH) and minimization of coalescence index, drying time, wettability and moisture were obtained with this combination. The foam density and solubility of the powders had no influence. In the second phase, the maximum desirability obtained was 0.726 at the drying temperature of 61.77 ºC. The variable sensory acceptance (flavor) was maximized and the variables drying, wettability and moisture were minimized. The different drying temperatures did not influence the variables antioxidant activity (ABTS and DPPH) and solubility. In the physical-chemical characterization of the powders, obtained with different concentrations of agents, there was an influence on the variables color, pH, acidity and water activity. In the powders obtained at different temperatures, a significant difference occurred only in the water activity response variable. It is concluded that the foam formation with 1.32% maltodextrin and 2.64% whey proteins, using the temperature of 61.77 oC for drying, are the optimal conditions for the drying process of the extract coffee in foam mat.Em decorrência da preferência dos consumidores por produtos de qualidade e de preparo rápido, há um aumento na demanda de café solúvel, tanto para consumo como também em forma de ingrediente em vários produtos a base de café, como o cappuccino. No processamento de café solúvel ocorrem transformações e perdas aromáticas que alteram de forma negativa o sabor e o aroma do café. Diante de tais problemas, o leito de espuma é uma tecnologia alternativa para a sua produção. Este processo é de baixo custo, utilizam-se baixas temperaturas e tempo de secagem; além disso, a utilização de agentes possibilita a formação de uma espuma estável durante todo o processo de secagem, aumentando a área exposta ao ar quente, o que facilita a saída de água pelos espaços preenchidos de ar, permitindo maior retenção de aromas e compostos, bem como a obtenção de um produto poroso e de fácil reidratação. Diante deste contexto, o objetivo desse trabalho foi otimizar as condições do processo de produção de café solúvel pelo método de secagem em leito de espuma. O experimento foi dividido em duas fases. Inicialmente, foi investigada a influência de diferentes teores de maltodextrina e de proteínas do soro de leite, obtidos por meio do Delineamento Composto Central Rotacional, na produção da espuma do extrato de café. O estudo da segunda fase foi avaliar o efeito de diferentes temperaturas do ar de secagem na produção de café desidratado, sendo que, para esse estudo, foi utilizada a concentração ideal de agentes obtida na fase anterior. Em ambas as fases, utilizou-se a função desejabilidade para definir as condições ótimas do processo para obtenção dos pós com características mais desejáveis. Para isso, foram avaliadas as seguintes variáveis resposta: a) relacionadas à espuma do extrato de café: densidade e índice de coalescência; b) relacionada à secagem em leito de espuma: tempo de secagem; c) relacionadas aos pós obtidos (café desidratado): solubilidade, atividade antioxidante (DPPH e ABTS), molhabilidade e umidade; d) relacionada à análise sensorial dos cappuccinos: aceitação sensorial. Foi feita a caracterização físico-química dos pós obtidos, quanto à atividade de água, cor, pH e acidez. Além disso, foi realizado o estudo da cinética de secagem das espumas. Constatou-se que a combinação dos agentes de 1,32% de maltodextrina e 2,64% de proteínas do soro de leite obteve maior desejabilidade global (0,6503), por apresentarem as características mais desejáveis (maximização da aceitação do sabor, do aroma, da impressão global e da atividade antioxidante (ABTS e DPPH) e minimização do índice de coalescência, do tempo de secagem, da molhabilidade e da umidade). A densidade da espuma e solubilidade dos pós não foram influenciadas nesse estudo. Na segunda fase, a desejabilidade máxima encontrada foi igual a 0,726, obtida na temperatura de secagem de 61,77 oC, na qual se maximizou a variável aceitação sensorial (sabor) e se minimizou as variáveis tempo de secagem, molhabilidade e umidade. As diferentes temperaturas de secagem não influenciaram nas variáveis atividade antioxidante (ABTS e DPPH) e solubilidade. Na caracterização físico-química dos pós obtidos com diferentes concentrações de agentes houve influência nas variáveis cor, pH, acidez e atividade de água. Já nos pós obtidos em diferentes temperaturas ocorreu diferença significativa somente na variável resposta atividade de água. Conclui-se que a formação de espuma com 1,32% de maltodextrina e 2,64% de proteínas do soro de leite, utilizando a temperatura de 61,77 oC para a secagem, são as condições ótimas para o processo de secagem do extrato de café em leito de espuma.Texthttp://repositorio.ufes.br/handle/10/8100porUniversidade Federal do Espírito SantoMestrado em Ciência e Tecnologia de AlimentosPrograma de Pós-Graduação em Ciência e Tecnologia de AlimentosUFESBRCentro de Ciências Agrárias e EngenhariasSecagem em leito de espumaCafé desidratadoAgentesTemperaturaDesejabilidadeDehydrated coffeeAgentsTemperatureDesirabilityCafé solúvelCafé - DesidrataçãoCafé - QualidadeTemperaturaCiência e Tecnologia de Alimentos664Otimização das condições do processo de secagem do extrato de café em leito de espuma e aplicação em mistura para cappuccinoOptimization of the conditions of the drying process of coffee extract in foam mat and application in cappuccino mixinfo:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/masterThesisinfo:eu-repo/semantics/openAccessreponame:Repositório Institucional da Universidade Federal do Espírito Santo (riUfes)instname:Universidade Federal do Espírito Santo (UFES)instacron:UFESORIGINALtese_9492_Resumo Final de Dissertação - Kátia Silva Maciel PDF.pdfapplication/pdf93189http://repositorio.ufes.br/bitstreams/b52dd2f7-6c65-47a9-ac6c-498e20a8cce2/download2778171158be3f5c98491c860c0d899fMD5110/81002024-06-21 16:56:11.822oai:repositorio.ufes.br:10/8100http://repositorio.ufes.brRepositório InstitucionalPUBhttp://repositorio.ufes.br/oai/requestopendoar:21082024-07-11T14:30:54.198194Repositório Institucional da Universidade Federal do Espírito Santo (riUfes) - Universidade Federal do Espírito Santo (UFES)false
dc.title.none.fl_str_mv Otimização das condições do processo de secagem do extrato de café em leito de espuma e aplicação em mistura para cappuccino
dc.title.alternative.none.fl_str_mv Optimization of the conditions of the drying process of coffee extract in foam mat and application in cappuccino mix
title Otimização das condições do processo de secagem do extrato de café em leito de espuma e aplicação em mistura para cappuccino
spellingShingle Otimização das condições do processo de secagem do extrato de café em leito de espuma e aplicação em mistura para cappuccino
Maciel, Kátia Silva
Secagem em leito de espuma
Café desidratado
Agentes
Temperatura
Desejabilidade
Dehydrated coffee
Agents
Temperature
Desirability
Ciência e Tecnologia de Alimentos
Café solúvel
Café - Desidratação
Café - Qualidade
Temperatura
664
title_short Otimização das condições do processo de secagem do extrato de café em leito de espuma e aplicação em mistura para cappuccino
title_full Otimização das condições do processo de secagem do extrato de café em leito de espuma e aplicação em mistura para cappuccino
title_fullStr Otimização das condições do processo de secagem do extrato de café em leito de espuma e aplicação em mistura para cappuccino
title_full_unstemmed Otimização das condições do processo de secagem do extrato de café em leito de espuma e aplicação em mistura para cappuccino
title_sort Otimização das condições do processo de secagem do extrato de café em leito de espuma e aplicação em mistura para cappuccino
author Maciel, Kátia Silva
author_facet Maciel, Kátia Silva
author_role author
dc.contributor.advisor-co1.fl_str_mv Teixeira, Luciano José Quintão
dc.contributor.advisor-co2.fl_str_mv Della Lucia, Suzana Maria
dc.contributor.advisor1.fl_str_mv Saraiva, Sérgio Henriques
dc.contributor.author.fl_str_mv Maciel, Kátia Silva
dc.contributor.referee1.fl_str_mv Lima Filho, Tarcísio
contributor_str_mv Teixeira, Luciano José Quintão
Della Lucia, Suzana Maria
Saraiva, Sérgio Henriques
Lima Filho, Tarcísio
dc.subject.por.fl_str_mv Secagem em leito de espuma
Café desidratado
Agentes
Temperatura
Desejabilidade
topic Secagem em leito de espuma
Café desidratado
Agentes
Temperatura
Desejabilidade
Dehydrated coffee
Agents
Temperature
Desirability
Ciência e Tecnologia de Alimentos
Café solúvel
Café - Desidratação
Café - Qualidade
Temperatura
664
dc.subject.eng.fl_str_mv Dehydrated coffee
Agents
Temperature
Desirability
dc.subject.cnpq.fl_str_mv Ciência e Tecnologia de Alimentos
dc.subject.br-rjbn.none.fl_str_mv Café solúvel
Café - Desidratação
Café - Qualidade
Temperatura
dc.subject.udc.none.fl_str_mv 664
description As a result of consumers' preference for quality of products and time of preparation, there is an increasing demand related to soluble coffee, both for consumption and as an ingredient in various coffee products, such as cappuccino. In the processing of soluble coffee there are transformations and aromatic losses, that can negatively alter the flavor and aroma of the coffee. Facing such problems, the foam mat is an alternative technology for soluble coffee production. This process is low cost, low temperatures and drying time; in addition, the use of foaming agents allows the formation of a stable foam throughout the drying process, increasing the area exposed to hot air, which the evaporation is facilitated through the spaces filled with air, allowing a greater retention of aromas and compounds, as well as obtaining a porous product with easy rehydration. In this context, the objective of this study was to optimize the conditions of the soluble coffee production process by the foam mat drying method. The experiment was divided into two phases. Initially, the influence of different levels of maltodextrin and whey proteins on the foam production of the coffee extract obtained through the Rotational Central Compound Design were investigated. In the second phase, the effect of different drying air temperatures on the production of dehydrated coffee, was to evaluate, in which the ideal concentration of agents obtained in the previous phase was used. The desirability function was used to define the optimal conditions of the process to obtain powders with the most desirable characteristics in both phases. For this, the following response variables were evaluated: a) related to the coffee extract foam: density and coalescence index; b) related to foam mat drying: drying time; c) related to the powders obtained (dehydrated coffee): solubility, antioxidant activity (DPPH and ABTS), wettability and moisture; d) related to the sensorial analysis of cappuccino: sensorial acceptance. The physicochemical characterization of the obtained powders was performed in relation to water activity, color, pH and acidity. In addition, the study of the drying kinetics of foams was also assessed. Results revealed that the combination of 1.32% maltodextrin and 2.64% whey proteins obtained greater overall desirability (0.6503), since the most desirable characteristics (maximization of flavor acceptance, aroma, the overall impression and antioxidant activity (ABTS and DPPH) and minimization of coalescence index, drying time, wettability and moisture were obtained with this combination. The foam density and solubility of the powders had no influence. In the second phase, the maximum desirability obtained was 0.726 at the drying temperature of 61.77 ºC. The variable sensory acceptance (flavor) was maximized and the variables drying, wettability and moisture were minimized. The different drying temperatures did not influence the variables antioxidant activity (ABTS and DPPH) and solubility. In the physical-chemical characterization of the powders, obtained with different concentrations of agents, there was an influence on the variables color, pH, acidity and water activity. In the powders obtained at different temperatures, a significant difference occurred only in the water activity response variable. It is concluded that the foam formation with 1.32% maltodextrin and 2.64% whey proteins, using the temperature of 61.77 oC for drying, are the optimal conditions for the drying process of the extract coffee in foam mat.
publishDate 2017
dc.date.issued.fl_str_mv 2017-02-21
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2018-08-01T23:19:04Z
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Mestrado em Ciência e Tecnologia de Alimentos
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publisher.none.fl_str_mv Universidade Federal do Espírito Santo
Mestrado em Ciência e Tecnologia de Alimentos
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