Desenvolvimento de extrato hidrossolúvel à base de castanha-do-brasil (bertholletia excelsa) e macadâmia (Macadamia integrifolia)

Detalhes bibliográficos
Autor(a) principal: Machado, André Luiz Borges
Data de Publicação: 2017
Tipo de documento: Dissertação
Idioma: por
Título da fonte: Repositório Institucional da UFG
dARK ID: ark:/38995/00130000048gm
Texto Completo: http://repositorio.bc.ufg.br/tede/handle/tede/7066
Resumo: Brazil nut (Bertholletia excelsa) and Macadamia (Macadamia integrifolia) are rich feeds with excellent nutrients with higher quality. The main form of consumption of these nuts and almonds are in natura, but there are products which can be elaborated using these raw materials with high nutritional value and pleasant flavor. Water-soluble extracts are an alternative to consume them, which consist of fluid food of plant origin, that can be produced by nuts, oleaginous and even some grasses and they have great commercial appeal since they are free of animal’s fats, “lac free” (free of lactose) and have high rate of minerals. Thus, this research aimed to determine the best formulation, to accompany physical and microbiological stability, proximal composition, to estimate the shelf life and to determine the rheological behavior of a water-soluble extract made of Brazil nut and Macadamia. For the construction of mathematical models, with the purpose of knowing the effect of the variation of water, Brazil nut and Macadamia concentrations, basic components in the elaboration of the product on the proximal composition and physical aspects such as pH, titratable acidity and colorimetry, a simplex centroid design for mixtures was used and provided quadratic and cubic models showing excellent adjustment of experimental data. The Global Acceptance and Purchase Intention tests were performed for each experiment proposed by simplex centroid design and the Tukey test was used in order to determine the best proportion among the components of the ternary mixture. The formulation of water-soluble extract composed of 70% (w/w) water, 15% (w / w) Brazilian nut and 15% (w/w) Macadamia was considered to be the most preferred by tasters submitted to the sensory evaluations. In order to improve the product’s flavor, 10% (w/v) of sugar, expressed as sucrose, was added and the concentration of preservatives citric acid, potassium sorbate and sodium benzoate was reduced. The product was processed technologically under hygienic conditions and filled in 220 ml transparent glass bottles, hermetically sealed with metal crown cork, pasteurized at 80 °C/25 min, stored under refrigeration at 4 ° C and had its stability evaluated during 28 days. Growth of Thermotolerant Coliforms, Positive Coagulase Staphylococci, Salmonella sp, Molds and Yeasts during the evaluation period was not detected. There was a significant variation (p < 0.05) in pH in the first two weeks of storage, and remained without significant variation (p > 0.05) for the other weeks analyzed. The acidity remained constant throughout the lifetime. The product showed a yellowish-white color throughout the study, determined by the coordinates of the colorimetry. Sensory analysis scores for odor, color, taste and global impression averaged around 6, thus, concluding that the product has a 28 days of shelf life. The rheological profile of the beverage was evaluated at three different temperatures, at 25 °C (room temperature), at 45 °C (temperature of the disintegration stage of Brazil nut and Macadamia with water in blender), and at 80 °C, (pasteurization temperature). The Ostwald-de-Waele model was considered the best to describe the beverage flow and since the calculated flow rate of the model, was less than 1 at the temperatures studied, it had concluded that the beverage behaved as a fluid Non-Newtonian pseudoplastic. The apparent viscosity curves of the mixed drink were plotted and showed that the apparent viscosity decreased significantly (p < 0.05) with the increasing of temperature.
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spelling Cardoso, Cláudio Fernandeshttp://lattes.cnpq.br/5163369332806586Silva, Flávio Alves dahttp://lattes.cnpq.br/1713250447051507Cardoso, Cláudio FernandesSilva, Flávio Alves daFreitas, Fernanda FerreiraLima, Mayra Conceição Peixoto Martinshttp://lattes.cnpq.br/4278774730558540Machado, André Luiz Borges2017-04-04T10:15:52Z2017-02-23MACHADO, A. L. B. Desenvolvimento de extrato hidrossolúvel à base de castanha-do-brasil (bertholletia excelsa) e macadâmia (Macadamia integrifolia). 2017. 108 f. Dissertação (Mestrado em Engenharia Química) - Universidade Federal de Goiás, 2017.http://repositorio.bc.ufg.br/tede/handle/tede/7066ark:/38995/00130000048gmBrazil nut (Bertholletia excelsa) and Macadamia (Macadamia integrifolia) are rich feeds with excellent nutrients with higher quality. The main form of consumption of these nuts and almonds are in natura, but there are products which can be elaborated using these raw materials with high nutritional value and pleasant flavor. Water-soluble extracts are an alternative to consume them, which consist of fluid food of plant origin, that can be produced by nuts, oleaginous and even some grasses and they have great commercial appeal since they are free of animal’s fats, “lac free” (free of lactose) and have high rate of minerals. Thus, this research aimed to determine the best formulation, to accompany physical and microbiological stability, proximal composition, to estimate the shelf life and to determine the rheological behavior of a water-soluble extract made of Brazil nut and Macadamia. For the construction of mathematical models, with the purpose of knowing the effect of the variation of water, Brazil nut and Macadamia concentrations, basic components in the elaboration of the product on the proximal composition and physical aspects such as pH, titratable acidity and colorimetry, a simplex centroid design for mixtures was used and provided quadratic and cubic models showing excellent adjustment of experimental data. The Global Acceptance and Purchase Intention tests were performed for each experiment proposed by simplex centroid design and the Tukey test was used in order to determine the best proportion among the components of the ternary mixture. The formulation of water-soluble extract composed of 70% (w/w) water, 15% (w / w) Brazilian nut and 15% (w/w) Macadamia was considered to be the most preferred by tasters submitted to the sensory evaluations. In order to improve the product’s flavor, 10% (w/v) of sugar, expressed as sucrose, was added and the concentration of preservatives citric acid, potassium sorbate and sodium benzoate was reduced. The product was processed technologically under hygienic conditions and filled in 220 ml transparent glass bottles, hermetically sealed with metal crown cork, pasteurized at 80 °C/25 min, stored under refrigeration at 4 ° C and had its stability evaluated during 28 days. Growth of Thermotolerant Coliforms, Positive Coagulase Staphylococci, Salmonella sp, Molds and Yeasts during the evaluation period was not detected. There was a significant variation (p < 0.05) in pH in the first two weeks of storage, and remained without significant variation (p > 0.05) for the other weeks analyzed. The acidity remained constant throughout the lifetime. The product showed a yellowish-white color throughout the study, determined by the coordinates of the colorimetry. Sensory analysis scores for odor, color, taste and global impression averaged around 6, thus, concluding that the product has a 28 days of shelf life. The rheological profile of the beverage was evaluated at three different temperatures, at 25 °C (room temperature), at 45 °C (temperature of the disintegration stage of Brazil nut and Macadamia with water in blender), and at 80 °C, (pasteurization temperature). The Ostwald-de-Waele model was considered the best to describe the beverage flow and since the calculated flow rate of the model, was less than 1 at the temperatures studied, it had concluded that the beverage behaved as a fluid Non-Newtonian pseudoplastic. The apparent viscosity curves of the mixed drink were plotted and showed that the apparent viscosity decreased significantly (p < 0.05) with the increasing of temperature.A Castanha-do-Brasil (Bertholletia excelsa) e a Macadâmia (Macadamia integrifolia) são alimentos ricos em nutrientes de excelente qualidade. A principal forma de consumo de nozes e amêndoas é in natura, porém existem produtos que podem ser elaborados a partir destas matérias-primas com alto valor nutricional e também de sabor agradável. Uma alternativa ao consumo desses alimentos são os extratos hidrossolúveis, que consistem em alimentos fluidos de origem vegetal que podem ser produzidos a partir de castanhas, oleaginosas e até mesmo algumas gramíneas e possuem grande apelo comercial, uma vez que são isentos de gorduras animais, não possuem lactose e apresentam alto teor de minerais. Sendo assim, esta pesquisa objetivou determinar a melhor formulação, acompanhar a estabilidade física e microbiológica, composição proximal, estimar a vida útil e determinar o comportamento reológico de um extrato hidrossolúvel a base de Castanha-do-Brasil e Macadâmia. Para a construção de modelos matemáticos, com a finalidade de se conhecer o efeito da variação das concentrações de água, Castanha-do-Brasil e Macadâmia, dos componentes básicos na elaboração do produto sobre a composição proximal e aspectos físicos como pH, acidez titulável e colorimetria, utilizou-se o planejamento experimental para misturas tipo simplex centroide que forneceu modelos quadráticos e cúbicos com excelente ajuste frente aos dados experimentais. Os Testes de Aceitação Global e Intenção de Compra foram realizados para cada experimento proposto pelo planejamento simplex centroide e o teste de Tukey foi utilizado a fim de determinar a melhor proporção entre os componentes da mistura ternária. A formulação de extrato hidrossolúvel composta por 70% (p/p) de água, 15% (p/p) de Castanha-do-Brasil e 15% (p/p) de Macadâmia, foi considerada como a mais preferida pelos provadores submetidos as avaliações sensoriais. Com a finalidade de melhorar o sabor do produto, adicionou-se 10% (p/v) de açúcar, expressos em sacarose, e reduziu-se a concentração dos conservantes ácido cítrico, sorbato de potássio e benzoato de sódio. O produto foi processado tecnologicamente sob condições higiênicas, sendo envasado em garrafas de vidro transparente de 220 mL, fechado hermeticamente com tampas metálicas do tipo coroa, pasteurizado a 80 °C/25 min, armazenado sob refrigeração a 4 °C e teve sua estabilidade avaliada por 28 dias. Não foi detectado o crescimento de Coliformes Termotolerantes, Estafilococos Coagulase Positiva, Salmonella sp, Bolores e Leveduras durante o período de avaliação. Houve variação significativa (p < 0,05) do pH nas duas primeiras semanas de estocagem, estabilizando-se para as demais semanas analisadas. A acidez se manteve constante durante todo o período de vida útil. O produto apresentou coloração branco-amarelada durante todo o estudo, determinada pelas coordenadas da colorimetria. As notas das análises sensoriais para Odor, Cor, Sabor e Impressão Global tiveram média em torno de 6, concluindo assim que o produto tem vida útil de, pelo menos, 28 dias. Foi avaliado o perfil reológico da bebida em três temperaturas distintas, a 25 ºC (temperatura ambiente), a 45 ºC, (temperatura da etapa de desintegração da Castanha-do-Brasil e Macadâmia com a água em liquidificador), e a 80 ºC, (temperatura de pasteurização). O modelo de Ostwald-de-Waele foi considerado o melhor para descrever o escoamento da bebida e uma vez que o índice de escoamento calculado do modelo foi menor que 1, nas temperaturas estudadas, conclui-se que a bebida comportou-se como um fluido não newtoniano pseudoplástico. As curvas de viscosidade aparente da bebida mista foram plotadas e mostram que a viscosidade aparente diminuiu significativamente (p < 0,05) com o aumento da temperatura.Submitted by Luciana Ferreira (lucgeral@gmail.com) on 2017-04-04T10:15:18Z No. of bitstreams: 2 Dissertação - André Luiz Borges Machado - 2017.pdf: 4018960 bytes, checksum: 0f752eee89eafe0cb8606742dc6901b7 (MD5) license_rdf: 0 bytes, checksum: d41d8cd98f00b204e9800998ecf8427e (MD5)Approved for entry into archive by Luciana Ferreira (lucgeral@gmail.com) on 2017-04-04T10:15:52Z (GMT) No. of bitstreams: 2 Dissertação - André Luiz Borges Machado - 2017.pdf: 4018960 bytes, checksum: 0f752eee89eafe0cb8606742dc6901b7 (MD5) license_rdf: 0 bytes, checksum: d41d8cd98f00b204e9800998ecf8427e (MD5)Made available in DSpace on 2017-04-04T10:15:52Z (GMT). No. of bitstreams: 2 Dissertação - André Luiz Borges Machado - 2017.pdf: 4018960 bytes, checksum: 0f752eee89eafe0cb8606742dc6901b7 (MD5) license_rdf: 0 bytes, checksum: d41d8cd98f00b204e9800998ecf8427e (MD5) Previous issue date: 2017-02-23Coordenação de Aperfeiçoamento de Pessoal de Nível Superior - CAPESapplication/pdfporUniversidade Federal de GoiásPrograma de Pós-graduação em Engenharia Química (IQ)UFGBrasilInstituto de Química - IQ (RG)http://creativecommons.org/licenses/by-nc-nd/4.0/info:eu-repo/semantics/openAccessCastanha-do-BrasilBertholletia excelsaMacadâmiaMacadamia integrifoliaSimplex centroideVida útilReologiaExtrato HidrossolúvelBrazil nutBertholletia excelsaMacadâmiaMacadamia integrifoliaShelf lifeRheologyWater-soluble extractENGENHARIA QUIMICA::PROCESSOS INDUSTRIAIS DE ENGENHARIA QUIMICADesenvolvimento de extrato hidrossolúvel à base de castanha-do-brasil (bertholletia excelsa) e macadâmia (Macadamia integrifolia)Development of water-soluble extract produced by brazil nut (bertholletia excelsa) and macadamia (Macadamia integrifolia)info:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/masterThesis3481496501158460078600600600600782606674374119727888981387697583185912075167498588264571reponame:Repositório Institucional da UFGinstname:Universidade Federal de Goiás (UFG)instacron:UFGLICENSElicense.txtlicense.txttext/plain; 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dc.title.por.fl_str_mv Desenvolvimento de extrato hidrossolúvel à base de castanha-do-brasil (bertholletia excelsa) e macadâmia (Macadamia integrifolia)
dc.title.alternative.eng.fl_str_mv Development of water-soluble extract produced by brazil nut (bertholletia excelsa) and macadamia (Macadamia integrifolia)
title Desenvolvimento de extrato hidrossolúvel à base de castanha-do-brasil (bertholletia excelsa) e macadâmia (Macadamia integrifolia)
spellingShingle Desenvolvimento de extrato hidrossolúvel à base de castanha-do-brasil (bertholletia excelsa) e macadâmia (Macadamia integrifolia)
Machado, André Luiz Borges
Castanha-do-Brasil
Bertholletia excelsa
Macadâmia
Macadamia integrifolia
Simplex centroide
Vida útil
Reologia
Extrato Hidrossolúvel
Brazil nut
Bertholletia excelsa
Macadâmia
Macadamia integrifolia
Shelf life
Rheology
Water-soluble extract
ENGENHARIA QUIMICA::PROCESSOS INDUSTRIAIS DE ENGENHARIA QUIMICA
title_short Desenvolvimento de extrato hidrossolúvel à base de castanha-do-brasil (bertholletia excelsa) e macadâmia (Macadamia integrifolia)
title_full Desenvolvimento de extrato hidrossolúvel à base de castanha-do-brasil (bertholletia excelsa) e macadâmia (Macadamia integrifolia)
title_fullStr Desenvolvimento de extrato hidrossolúvel à base de castanha-do-brasil (bertholletia excelsa) e macadâmia (Macadamia integrifolia)
title_full_unstemmed Desenvolvimento de extrato hidrossolúvel à base de castanha-do-brasil (bertholletia excelsa) e macadâmia (Macadamia integrifolia)
title_sort Desenvolvimento de extrato hidrossolúvel à base de castanha-do-brasil (bertholletia excelsa) e macadâmia (Macadamia integrifolia)
author Machado, André Luiz Borges
author_facet Machado, André Luiz Borges
author_role author
dc.contributor.advisor1.fl_str_mv Cardoso, Cláudio Fernandes
dc.contributor.advisor1Lattes.fl_str_mv http://lattes.cnpq.br/5163369332806586
dc.contributor.advisor-co1.fl_str_mv Silva, Flávio Alves da
dc.contributor.advisor-co1Lattes.fl_str_mv http://lattes.cnpq.br/1713250447051507
dc.contributor.referee1.fl_str_mv Cardoso, Cláudio Fernandes
dc.contributor.referee2.fl_str_mv Silva, Flávio Alves da
dc.contributor.referee3.fl_str_mv Freitas, Fernanda Ferreira
dc.contributor.referee4.fl_str_mv Lima, Mayra Conceição Peixoto Martins
dc.contributor.authorLattes.fl_str_mv http://lattes.cnpq.br/4278774730558540
dc.contributor.author.fl_str_mv Machado, André Luiz Borges
contributor_str_mv Cardoso, Cláudio Fernandes
Silva, Flávio Alves da
Cardoso, Cláudio Fernandes
Silva, Flávio Alves da
Freitas, Fernanda Ferreira
Lima, Mayra Conceição Peixoto Martins
dc.subject.por.fl_str_mv Castanha-do-Brasil
Bertholletia excelsa
Macadâmia
Macadamia integrifolia
Simplex centroide
Vida útil
Reologia
Extrato Hidrossolúvel
topic Castanha-do-Brasil
Bertholletia excelsa
Macadâmia
Macadamia integrifolia
Simplex centroide
Vida útil
Reologia
Extrato Hidrossolúvel
Brazil nut
Bertholletia excelsa
Macadâmia
Macadamia integrifolia
Shelf life
Rheology
Water-soluble extract
ENGENHARIA QUIMICA::PROCESSOS INDUSTRIAIS DE ENGENHARIA QUIMICA
dc.subject.eng.fl_str_mv Brazil nut
Bertholletia excelsa
Macadâmia
Macadamia integrifolia
Shelf life
Rheology
Water-soluble extract
dc.subject.cnpq.fl_str_mv ENGENHARIA QUIMICA::PROCESSOS INDUSTRIAIS DE ENGENHARIA QUIMICA
description Brazil nut (Bertholletia excelsa) and Macadamia (Macadamia integrifolia) are rich feeds with excellent nutrients with higher quality. The main form of consumption of these nuts and almonds are in natura, but there are products which can be elaborated using these raw materials with high nutritional value and pleasant flavor. Water-soluble extracts are an alternative to consume them, which consist of fluid food of plant origin, that can be produced by nuts, oleaginous and even some grasses and they have great commercial appeal since they are free of animal’s fats, “lac free” (free of lactose) and have high rate of minerals. Thus, this research aimed to determine the best formulation, to accompany physical and microbiological stability, proximal composition, to estimate the shelf life and to determine the rheological behavior of a water-soluble extract made of Brazil nut and Macadamia. For the construction of mathematical models, with the purpose of knowing the effect of the variation of water, Brazil nut and Macadamia concentrations, basic components in the elaboration of the product on the proximal composition and physical aspects such as pH, titratable acidity and colorimetry, a simplex centroid design for mixtures was used and provided quadratic and cubic models showing excellent adjustment of experimental data. The Global Acceptance and Purchase Intention tests were performed for each experiment proposed by simplex centroid design and the Tukey test was used in order to determine the best proportion among the components of the ternary mixture. The formulation of water-soluble extract composed of 70% (w/w) water, 15% (w / w) Brazilian nut and 15% (w/w) Macadamia was considered to be the most preferred by tasters submitted to the sensory evaluations. In order to improve the product’s flavor, 10% (w/v) of sugar, expressed as sucrose, was added and the concentration of preservatives citric acid, potassium sorbate and sodium benzoate was reduced. The product was processed technologically under hygienic conditions and filled in 220 ml transparent glass bottles, hermetically sealed with metal crown cork, pasteurized at 80 °C/25 min, stored under refrigeration at 4 ° C and had its stability evaluated during 28 days. Growth of Thermotolerant Coliforms, Positive Coagulase Staphylococci, Salmonella sp, Molds and Yeasts during the evaluation period was not detected. There was a significant variation (p < 0.05) in pH in the first two weeks of storage, and remained without significant variation (p > 0.05) for the other weeks analyzed. The acidity remained constant throughout the lifetime. The product showed a yellowish-white color throughout the study, determined by the coordinates of the colorimetry. Sensory analysis scores for odor, color, taste and global impression averaged around 6, thus, concluding that the product has a 28 days of shelf life. The rheological profile of the beverage was evaluated at three different temperatures, at 25 °C (room temperature), at 45 °C (temperature of the disintegration stage of Brazil nut and Macadamia with water in blender), and at 80 °C, (pasteurization temperature). The Ostwald-de-Waele model was considered the best to describe the beverage flow and since the calculated flow rate of the model, was less than 1 at the temperatures studied, it had concluded that the beverage behaved as a fluid Non-Newtonian pseudoplastic. The apparent viscosity curves of the mixed drink were plotted and showed that the apparent viscosity decreased significantly (p < 0.05) with the increasing of temperature.
publishDate 2017
dc.date.accessioned.fl_str_mv 2017-04-04T10:15:52Z
dc.date.issued.fl_str_mv 2017-02-23
dc.type.status.fl_str_mv info:eu-repo/semantics/publishedVersion
dc.type.driver.fl_str_mv info:eu-repo/semantics/masterThesis
format masterThesis
status_str publishedVersion
dc.identifier.citation.fl_str_mv MACHADO, A. L. B. Desenvolvimento de extrato hidrossolúvel à base de castanha-do-brasil (bertholletia excelsa) e macadâmia (Macadamia integrifolia). 2017. 108 f. Dissertação (Mestrado em Engenharia Química) - Universidade Federal de Goiás, 2017.
dc.identifier.uri.fl_str_mv http://repositorio.bc.ufg.br/tede/handle/tede/7066
dc.identifier.dark.fl_str_mv ark:/38995/00130000048gm
identifier_str_mv MACHADO, A. L. B. Desenvolvimento de extrato hidrossolúvel à base de castanha-do-brasil (bertholletia excelsa) e macadâmia (Macadamia integrifolia). 2017. 108 f. Dissertação (Mestrado em Engenharia Química) - Universidade Federal de Goiás, 2017.
ark:/38995/00130000048gm
url http://repositorio.bc.ufg.br/tede/handle/tede/7066
dc.language.iso.fl_str_mv por
language por
dc.relation.program.fl_str_mv 3481496501158460078
dc.relation.confidence.fl_str_mv 600
600
600
600
dc.relation.department.fl_str_mv 7826066743741197278
dc.relation.cnpq.fl_str_mv 8898138769758318591
dc.relation.sponsorship.fl_str_mv 2075167498588264571
dc.rights.driver.fl_str_mv http://creativecommons.org/licenses/by-nc-nd/4.0/
info:eu-repo/semantics/openAccess
rights_invalid_str_mv http://creativecommons.org/licenses/by-nc-nd/4.0/
eu_rights_str_mv openAccess
dc.format.none.fl_str_mv application/pdf
dc.publisher.none.fl_str_mv Universidade Federal de Goiás
dc.publisher.program.fl_str_mv Programa de Pós-graduação em Engenharia Química (IQ)
dc.publisher.initials.fl_str_mv UFG
dc.publisher.country.fl_str_mv Brasil
dc.publisher.department.fl_str_mv Instituto de Química - IQ (RG)
publisher.none.fl_str_mv Universidade Federal de Goiás
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repository.name.fl_str_mv Repositório Institucional da UFG - Universidade Federal de Goiás (UFG)
repository.mail.fl_str_mv tasesdissertacoes.bc@ufg.br
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