Characterization of biodiesel obtained from atemoya (Annona squamosa x A. cherimola) seed oil
Autor(a) principal: | |
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Data de Publicação: | 2018 |
Outros Autores: | , , , , |
Tipo de documento: | Artigo |
Idioma: | eng |
Título da fonte: | Repositório Institucional da UFLA |
Texto Completo: | http://repositorio.ufla.br/jspui/handle/1/36051 |
Resumo: | Biodiesel is derived from renewable sources, such as vegetable oils, by means of a transesterification process in which triacylglycerols are transformed into smaller molecules of esters of fatty acids and glycerol. The transesterification reactions of ‘Gefner’ atemoya (Annona squamosa × A. cherimola) seed oil extracted by pressing (physical) and solvent (chemical) processes were studied, with analysis of the methyl esters produced. The reactions were monitored using gas chromatography coupled to mass spectrometry (GC-MS), as well as by hydrogen nuclear magnetic resonance spectroscopy (1H-NMR). The methyl esters formed during the transesterification reaction with methanol were determined for each oil. The major methyl esters (16:0, 18:0, 18:1 and 18:2) formed during 50 min of reaction were similar to those reported in the literature for other biodiesels; the peak areas and retention times were also similar. No changes in signal intensity over time were observed for the oils obtained by the two extraction methods. It was also noted that the extraction method had no influence on the types of methyl esters formed during biodiesel production. |
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Characterization of biodiesel obtained from atemoya (Annona squamosa x A. cherimola) seed oilAnnonaOil extractionTransesterificationBiodiesel is derived from renewable sources, such as vegetable oils, by means of a transesterification process in which triacylglycerols are transformed into smaller molecules of esters of fatty acids and glycerol. The transesterification reactions of ‘Gefner’ atemoya (Annona squamosa × A. cherimola) seed oil extracted by pressing (physical) and solvent (chemical) processes were studied, with analysis of the methyl esters produced. The reactions were monitored using gas chromatography coupled to mass spectrometry (GC-MS), as well as by hydrogen nuclear magnetic resonance spectroscopy (1H-NMR). The methyl esters formed during the transesterification reaction with methanol were determined for each oil. The major methyl esters (16:0, 18:0, 18:1 and 18:2) formed during 50 min of reaction were similar to those reported in the literature for other biodiesels; the peak areas and retention times were also similar. No changes in signal intensity over time were observed for the oils obtained by the two extraction methods. It was also noted that the extraction method had no influence on the types of methyl esters formed during biodiesel production.Academic Journals (AJ)2019-08-08T17:25:10Z2019-08-08T17:25:10Z2018-02-14info:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/articleapplication/pdfCRUZ, L. S. da et al. Characterization of biodiesel obtained from atemoya (Annona squamosa x A. cherimola) seed oil. African Journal of Biotechnology, [S.l.], v. 17, n. 7, p. 226-231, Feb. 2018. DOI: 10.5897/AJB2015.15126.http://repositorio.ufla.br/jspui/handle/1/36051African Journal of Microbiology Researchreponame:Repositório Institucional da UFLAinstname:Universidade Federal de Lavras (UFLA)instacron:UFLAAttribution 4.0 Internationalhttp://creativecommons.org/licenses/by/4.0/info:eu-repo/semantics/openAccessCruz, Luciana Soares daAraújo, Bárbara Lemes OuteiroAlbuquerque, Luiz Roberto MarquesCastro Neto, PedroCorrêa, Angelita DuartePinto, Luciana de Matos Alveseng2019-08-08T17:25:10Zoai:localhost:1/36051Repositório InstitucionalPUBhttp://repositorio.ufla.br/oai/requestnivaldo@ufla.br || repositorio.biblioteca@ufla.bropendoar:2019-08-08T17:25:10Repositório Institucional da UFLA - Universidade Federal de Lavras (UFLA)false |
dc.title.none.fl_str_mv |
Characterization of biodiesel obtained from atemoya (Annona squamosa x A. cherimola) seed oil |
title |
Characterization of biodiesel obtained from atemoya (Annona squamosa x A. cherimola) seed oil |
spellingShingle |
Characterization of biodiesel obtained from atemoya (Annona squamosa x A. cherimola) seed oil Cruz, Luciana Soares da Annona Oil extraction Transesterification |
title_short |
Characterization of biodiesel obtained from atemoya (Annona squamosa x A. cherimola) seed oil |
title_full |
Characterization of biodiesel obtained from atemoya (Annona squamosa x A. cherimola) seed oil |
title_fullStr |
Characterization of biodiesel obtained from atemoya (Annona squamosa x A. cherimola) seed oil |
title_full_unstemmed |
Characterization of biodiesel obtained from atemoya (Annona squamosa x A. cherimola) seed oil |
title_sort |
Characterization of biodiesel obtained from atemoya (Annona squamosa x A. cherimola) seed oil |
author |
Cruz, Luciana Soares da |
author_facet |
Cruz, Luciana Soares da Araújo, Bárbara Lemes Outeiro Albuquerque, Luiz Roberto Marques Castro Neto, Pedro Corrêa, Angelita Duarte Pinto, Luciana de Matos Alves |
author_role |
author |
author2 |
Araújo, Bárbara Lemes Outeiro Albuquerque, Luiz Roberto Marques Castro Neto, Pedro Corrêa, Angelita Duarte Pinto, Luciana de Matos Alves |
author2_role |
author author author author author |
dc.contributor.author.fl_str_mv |
Cruz, Luciana Soares da Araújo, Bárbara Lemes Outeiro Albuquerque, Luiz Roberto Marques Castro Neto, Pedro Corrêa, Angelita Duarte Pinto, Luciana de Matos Alves |
dc.subject.por.fl_str_mv |
Annona Oil extraction Transesterification |
topic |
Annona Oil extraction Transesterification |
description |
Biodiesel is derived from renewable sources, such as vegetable oils, by means of a transesterification process in which triacylglycerols are transformed into smaller molecules of esters of fatty acids and glycerol. The transesterification reactions of ‘Gefner’ atemoya (Annona squamosa × A. cherimola) seed oil extracted by pressing (physical) and solvent (chemical) processes were studied, with analysis of the methyl esters produced. The reactions were monitored using gas chromatography coupled to mass spectrometry (GC-MS), as well as by hydrogen nuclear magnetic resonance spectroscopy (1H-NMR). The methyl esters formed during the transesterification reaction with methanol were determined for each oil. The major methyl esters (16:0, 18:0, 18:1 and 18:2) formed during 50 min of reaction were similar to those reported in the literature for other biodiesels; the peak areas and retention times were also similar. No changes in signal intensity over time were observed for the oils obtained by the two extraction methods. It was also noted that the extraction method had no influence on the types of methyl esters formed during biodiesel production. |
publishDate |
2018 |
dc.date.none.fl_str_mv |
2018-02-14 2019-08-08T17:25:10Z 2019-08-08T17:25:10Z |
dc.type.status.fl_str_mv |
info:eu-repo/semantics/publishedVersion |
dc.type.driver.fl_str_mv |
info:eu-repo/semantics/article |
format |
article |
status_str |
publishedVersion |
dc.identifier.uri.fl_str_mv |
CRUZ, L. S. da et al. Characterization of biodiesel obtained from atemoya (Annona squamosa x A. cherimola) seed oil. African Journal of Biotechnology, [S.l.], v. 17, n. 7, p. 226-231, Feb. 2018. DOI: 10.5897/AJB2015.15126. http://repositorio.ufla.br/jspui/handle/1/36051 |
identifier_str_mv |
CRUZ, L. S. da et al. Characterization of biodiesel obtained from atemoya (Annona squamosa x A. cherimola) seed oil. African Journal of Biotechnology, [S.l.], v. 17, n. 7, p. 226-231, Feb. 2018. DOI: 10.5897/AJB2015.15126. |
url |
http://repositorio.ufla.br/jspui/handle/1/36051 |
dc.language.iso.fl_str_mv |
eng |
language |
eng |
dc.rights.driver.fl_str_mv |
Attribution 4.0 International http://creativecommons.org/licenses/by/4.0/ info:eu-repo/semantics/openAccess |
rights_invalid_str_mv |
Attribution 4.0 International http://creativecommons.org/licenses/by/4.0/ |
eu_rights_str_mv |
openAccess |
dc.format.none.fl_str_mv |
application/pdf |
dc.publisher.none.fl_str_mv |
Academic Journals (AJ) |
publisher.none.fl_str_mv |
Academic Journals (AJ) |
dc.source.none.fl_str_mv |
African Journal of Microbiology Research reponame:Repositório Institucional da UFLA instname:Universidade Federal de Lavras (UFLA) instacron:UFLA |
instname_str |
Universidade Federal de Lavras (UFLA) |
instacron_str |
UFLA |
institution |
UFLA |
reponame_str |
Repositório Institucional da UFLA |
collection |
Repositório Institucional da UFLA |
repository.name.fl_str_mv |
Repositório Institucional da UFLA - Universidade Federal de Lavras (UFLA) |
repository.mail.fl_str_mv |
nivaldo@ufla.br || repositorio.biblioteca@ufla.br |
_version_ |
1815439170147975168 |